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At least 397 records · Page 22

Network Time Synchronization of the Readout Electronics for a New Radioactive Gas Detection System

In systems with multiple radiation detectors, time synchronization of the data collected from different detectors is essential to reconstruct multi-detector events such as scattering and coincidences. In cases where the number of detectors exceeds the readout channels in a single data acquisition electronics module, multiple modules have to be synchronized, which is traditionally accomplished by distributing clocks and triggers via dedicated connections. To eliminate this added cabling complexity in the case of a new radioactive gas detection system prototype under development at the French Atomic Energy Commission, we implemented time synchronization between multiple XIA Pixie-Net detector readout modules through the existing Ethernet network, based on the IEEE 1588 precision time protocol. The detector system is dedicated to the measurement of radioactive gases at low activity and consists of eight large silicon pixels and two NaI(Tl) detectors, instrumented with a total of three 4-channel Pixie-Net modules. Detecting NaI(Tl)/silicon coincidences will make it possible to identify each radioisotope present in the sample. To allow these identifications at low activities, the Pixie-Net modules must be synchronized to a precision well below the targeted coincidence window of 500-1000 ns. Being equipped with an Ethernet PHY compatible with IEEE 1588 and synchronous Ethernet that outputs a locally generated but system-wide synchronized clock, the Pixie-Net can operate its analog to digital converters and digital processing circuitry with that clock and match time stamps for captured data across the three modules. Depending on the network configuration and synchronization method, the implementation is capable to achieve timing precisions between 300 ns and 200 ps.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

SBND Calibration

The Short-Baseline Near Detector (SBND) is a 112-ton liquid argon time projection chamber (LArTPC) serving as the near detector of the Short-Baseline Neutrino Program at Fermilab. SBND aims to make precise measurements of neutrino-argon interactions, necessitating an extensive calibration program for the LArTPC to ensure precision/accuracy in these measurements. This talk describes the use of cosmogenic, radiogenic, and neutrino interaction activity with both Monte Carlo simulation and data in calibrating the SBND subsystems of the Time Projection Chamber, Photon Detection System, and Cosmic Ray Tagger. We will highlight some of SBND's first calibration results, including electronics calibrations, measurement of the electron lifetime, shower calibration, and studies of space charge effects in the detector.

Oh, Sungbin [Fermilab]↗

Automated High-Pressure Titration System with In Situ Infrared Spectroscopic Detection

A fully automated titration system with infrared detection was developed for investigating interfacial chemistry at high pressures. The apparatus consists of a high-pressure fluid generation and delivery system coupled to a high-pressure cell with infrared optics. A manifold of electronically actuated valves is used to direct pressurized fluids into the cell. Precise reagent additions to the pressurized cell are made with calibrated tubing loops that are filled with reagent and placed in-line with the cell and a syringe pump. The cell’s infrared optics facilitate both transmission and attenuated total reflection (ATR) measurements to monitor bulk-fluid composition and solid-surface phenomena such as adsorption, desorption, complexation, dissolution, and precipitation. Switching between the two measurement modes is accomplished with moveable mirrors that direct radiation from a Fourier transform infrared spectrometer into the cell along transmission or ATR light paths. The versatility of the high-pressure IR titration system is demonstrated with three case studies. First, we titrated water into supercritical CO2 (scCO2) to generate an infrared calibration curve and determine the solubility of water in CO2 at 50 °C and 90 bar. Next, we characterized the partitioning of water between a montmorillonite clay and scCO2 at 50 °C and 90 bar. Transmission-mode spectra were used to quantify changes in the clay’s sorbed water concentration as a function of scCO2 hydration, and ATR measurements provided insights into competitive residency of water and CO2 on the clay surface and in the interlayer. Finally, we demonstrated how time-dependent studies can be conducted with the system by monitoring the carbonation reaction of forsterite (Mg2SiO4) in water-bearing scCO2 at 50 °C and 90 bar. Immediately after water dissolved in the scCO2, a thin film of adsorbed water formed on the mineral surface, and the film thickness increased with time as the forsterite began to dissolve. However, after approximately 2.5 hours, the trend reversed, and a carbonate precipitate began to form on the forsterite surface, exposing dramatic chemical changes in the thin-water film. Collectively, these applications illustrate how the high-pressure IR titration system can provide molecular-level information about the interactions between variably wet scCO2 and minerals relevant to underground storage of CO2 (geologic carbon sequestration). The apparatus could also be utilized to study high-pressure interfacial chemistry in other areas such as catalysis, polymerization, food processing, and oil and gas recovery.

Environmental Molecular Sciences Laboratory↗

Pointing stabilization of a 1 Hz high-power laser via machine learning

Abstract High-power lasers are vital for particle acceleration, imaging, fusion and materials processing, requiring precise control and high-energy delivery. Laser plasma accelerators (LPAs) demand laser positional stability at focus to ensure consistent electron beams in applications such as X-ray free-electron lasers and high-energy colliders. Achieving this stability is especially challenging for the low-repetition-rate lasers in current LPAs. We present a machine learning method that predicts and corrects laser pointing instabilities in real-time using a high-frequency pilot beam. By preemptively adjusting a correction mirror, this approach overcomes traditional feedback limits. Demonstrated on the BELLA petawatt laser operating at the terawatt level (30 mJ amplification), our method achieved root mean square pointing stabilization of 0.34 and 0.59 $\unicode{x3bc} \mathrm{rad}$ in the x and y directions, reducing jitter by 65% and 47%, respectively. This is the first successful application of predictive control for shot-to-shot stabilization in low-repetition-rate laser systems, paving the way for full-energy petawatt lasers and transformative advances across science, industry and security.

Amodio, Alessio↗

Attosecond time-resolved photoelectron holography

Ultrafast strong-field physics provides insight into quantum phenomena that evolve on an attosecond time scale, the most fundamental of which is quantum tunneling. The tunneling process initiates a range of strong field phenomena such as high harmonic generation (HHG), laser-induced electron diffraction, double ionization and photoelectron holography—all evolving during a fraction of the optical cycle. Here we apply attosecond photoelectron holography as a method to resolve the temporal properties of the tunneling process. Adding a weak second harmonic (SH) field to a strong fundamental laser field enables us to reconstruct the ionization times of photoelectrons that play a role in the formation of a photoelectron hologram with attosecond precision. In conclusion, we decouple the contributions of the two arms of the hologram and resolve the subtle differences in their ionization times, separated by only a few tens of attoseconds.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Evolution of nanopores in hexagonal boron nitride

Abstract The engineering of atomically-precise nanopores in two-dimensional materials presents exciting opportunities for both fundamental science studies as well as applications in energy, DNA sequencing, and quantum information technologies. The exceptional chemical and thermal stability of hexagonal boron nitride (h-BN) suggest that exposed h-BN nanopores will retain their atomic structure even when subjected to extended periods of time in gas or liquid environments. Here we employ transmission electron microscopy to examine the time evolution of h-BN nanopores in vacuum and in air and find, even at room temperature, dramatic geometry changes due to atom motion and edge contamination adsorption, for timescales ranging from one hour to one week. The discovery of nanopore evolution contrasts with general expectations and has profound implications for nanopore applications of two-dimensional materials.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Introducing a Markov chain-based time calibration procedure for multi-channel particle detectors: application to the SuperFGD and ToF detectors of the T2K experiment

Inter-channel mis-synchronisation can be a limiting factor to the time resolution of high performance timing detectors with multiple readout channels and independent electronics units. In these systems, time calibration methods employed must be able to efficiently correct for minimal mis-synchronisation between channels and achieve the best detector performance. We present an iterative time calibration method based on Markov Chains, suitable for detector systems with multiple readout channels. Starting from correlated hit pairs alone, and without requiring an external reference time measurement, the method solves for fixed per-channel offsets, with precision limited only by the intrinsic single-channel resolution. A mathematical proof that the method is able to find the correct time offsets to be assigned to each detector channel in order to achieve inter-channel synchronisation is given, and it is shown that the number of iterations to reach convergence within the desired precision is controllable with a single parameter. Numerical studies are used to confirm unbiased recovery of true offsets. Finally, the application of the calibration method to the Super Fine-Grained Detector (SuperFGD) and the Time of Flight (TOF) detector at the upgraded T2K near detector (ND280) shows good improvement in overall timing resolution, demonstrating the effectiveness in a real-world scenario and scalability.

calibration and fitting methods↗

Single-Electron Tracking (SETI)

We present the results of the first experiments on 6-dimensional phase-space tracking of a single electron in a storage ring, using a linear multi-anode photomultiplier tube for simultaneously measuring transverse coordinates and arrival times of synchrotron-radiation pulses. This technology makes it possible to fully reconstruct turn-by-turn positions and momentums in all three planes for a single particle. Complete experimental particle tracking enables the first direct measurements of dynamical properties, including invariants, tunes dependence on amplitudes with exceptional precision.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Using Time Evolution of the Bunch Structure to Extract the Muon Momentum Distribution in the Fermilab Muon g-2 Experiment

Beam dynamics plays an important role in achieving the unprecedented precision on measurement of the muon anomalous magnetic moment in the Fermilab Muon g-2 Experiment. It needs to find the muon momentum distribution in the storage ring in order to evaluate the electric field correction to muon anomalous precession frequency. We will show how to use time evolution of the beam bunch structure to extract the muon momentum distribution by applying a fast rotation analysis on the decay electron signals.

43 PARTICLE ACCELERATORS↗

Using Time Evolution of the Bunch Structure to Extract the Muon Momentum Distribution in the Fermilab Muon g-2

Beam dynamics plays an important role in achieving the unprecedented precision on measurement of the muon anomalous magnetic moment in the Fermilab Muon g-2 Experiment. It needs to find the muon momentum distribution in the storage ring in order to evaluate the electric field correction to muon anomalous precession frequency. We will show how to use time evolution of the beam bunch structure to extract the muon momentum distribution by applying a fast rotation analysis on the decay electron signals.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Precision measurement of Compton scattering in silicon with a skipper CCD for dark matter detection

Experiments aiming to directly detect dark matter through particle recoils can achieve energy thresholds of $\mathcal{O}(1\,\mathrm{eV})$. In this regime, ionization signals from small-angle Compton scatters of environmental $\gamma$-rays constitute a significant background. Monte Carlo simulations used to build background models have not been experimentally validated at these low energies. We report a precision measurement of Compton scattering on silicon atomic shell electrons down to 23$\,$eV. A skipper charge-coupled device (CCD) with single-electron resolution, developed for the DAMIC-M experiment, was exposed to a $^{241}$Am $\gamma$-ray source over several months. Features associated with the silicon K, L$_{1}$, and L$_{2,3}$-shells are clearly identified, and scattering on valence electrons is detected for the first time below 100$\,$eV. We find that the relativistic impulse approximation for Compton scattering, which is implemented in Monte Carlo simulations commonly used by direct detection experiments, does not reproduce the measured spectrum below 0.5$\,$keV. The data are in better agreement with $ab$$initio$ calculations originally developed for X-ray absorption spectroscopy.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Rovibronic structure in slow photoelectron velocity-map imaging spectroscopy of CH{sub 2}CN{sup −} and CD{sub 2}CN{sup −}

We report high-resolution anion photoelectron spectra of the cryogenically cooled cyanomethide anion, CH{sub 2}CN{sup −}, and its isotopologue, CD{sub 2}CN{sup −}, using slow photoelectron velocity-map imaging (SEVI) spectroscopy. Electron affinities of 12 468(2) cm{sup −1} for CH{sub 2}CN and 12 402(2) cm{sup −1} for CD{sub 2}CN are obtained, demonstrating greater precision than previous experiments. New vibrational structure is resolved for both neutral species, especially activity of the ν{sub 5} hydrogen umbrella modes. The ν{sub 6} out-of-plane bending mode fundamental frequency is measured for the first time in both systems and found to be 420(10) cm{sup −1} for CH{sub 2}CN and 389(8) cm{sup −1} for CD{sub 2}CN. Some rotational structure is resolved, allowing for accurate extraction of vibrational frequencies. Temperature-dependent SEVI spectra show marked effects ascribed to controlled population of low-lying anion vibrational levels. We directly measure the inversion splitting between the first two vibrational levels of the anion ν{sub 5} umbrella mode in both species, finding a splitting of 130(20) cm{sup −1} for CH{sub 2}CN{sup −} and 81(20) cm{sup −1} for CD{sub 2}CN{sup −}. Franck-Condon forbidden activity is observed and attributed to mode-specific vibrational autodetachment from the CH{sub 2}CN{sup −} and CD{sub 2}CN{sup −} dipole bound excited states. We also refine the binding energy of the anion dipole bound states to 39 and 42 cm{sup −1}, respectively, for CH{sub 2}CN{sup −} and CD{sub 2}CN{sup −}.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Optical delay encoding for fast timing and detector signal multiplexing in PET

Purpose: The large number of detector channels in modern positron emission tomography (PET) scanners poses a challenge in terms of readout electronics complexity. Multiplexing schemes are typically implemented to reduce the number of physical readout channels, but often result in performance degradation. Novel methods of multiplexing in PET must be developed to avoid this data degradation. The preservation of fast timing information is especially important for time-of-flight PET. Methods: A new multiplexing scheme based on encoding detector interaction events with a series of extremely fast overlapping optical pulses with precise delays is demonstrated in this work. Encoding events in this way potentially allows many detector channels to be simultaneously encoded onto a single optical fiber that is then read out by a single digitizer. A two channel silicon photomultiplier-based prototype utilizing this optical delay encoding technique along with dual threshold time-over-threshold is demonstrated. Results: The optical encoding and multiplexing prototype achieves a coincidence time resolution of 160 ps full width at half maximum (FWHM) and an energy resolution of 13.1% FWHM at 511 keV with 3 × 3 × 5 mm{sup 3} LYSO crystals. All interaction information for both detectors, including timing, energy, and channel identification, is encoded onto a single optical fiber with little degradation. Conclusions: Optical delay encoding and multiplexing technology could lead to time-of-flight PET scanners with fewer readout channels and simplified data acquisition systems.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Precision Measurements of High-Energy Cosmic Gamma-Ray Emission with the GAMMA-400 Gamma-Ray Telescope

The GAMMA-400 γ-ray telescope installed at the Russian space observatory is intended for precision measurements in the energy range of 20 MeV–1000 GeV of γ-ray emission (with the angular and energy resolutions several times better than that of current γ-ray telescopes) from discrete sources; measurement of the energy spectra of Galactic and extragalactic diffuse γ-ray emission; studies of γ-ray emission from the active Sun; and measurements of fluxes of γ-ray emission and electron–positron cosmicray component, which are probably associated with the annihilation or decay of dark-matter particles.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Wideband precision stabilization of the -18.6kV retarding voltage for the KATRIN spectrometer

The Karlsruhe Tritium Neutrino Experiment (KATRIN) measures the effective electron anti-neutrino mass with an unprecedented design sensitivity of 0.2 eV (90 % C.L.). In this experiment, the energy spectrum of beta electrons near the tritium decay endpoint is analyzed with a highly accurate spectrometer. To reach the KATRIN sensitivity target, the retarding voltage of this spectrometer must be stable to the ppm (1 × 10 -6 ) level and well known on various time scales (μs up to months), for values around -18.6 kV. A custom-designed high-voltage regulation system mitigates the impact of interference sources in the absence of a closed electric shield around the large spectrometer vessel. In this article, we describe the regulation system and its integration into the KATRIN setup. Independent monitoring methods demonstrate a stability within 2 ppm, exceeding KATRIN's specifications.

47 OTHER INSTRUMENTATION↗

Multiscale Characterization of Additive Manufacturing Components with Computed Tomography, 3D X-ray Microscopy, and Deep Learning

Additive manufacturing (AM) facilitates the creation of complex-geometry parts, driving advancements in lightweight aerospace components, high-efficiency engine cooling channels, and customized medical implants. However, ensuring the quality and reliability of AM parts remains challenging due to internal defects, surface irregularities, porosity, and residual trapped powder, which are often inaccessible to traditional inspection methods. Recent developments in X-ray computed tomography (XCT) and 3D X-ray microscopy (XRM), particularly systems equipped with resolution-at-a-distance (RaaD™) capabilities, enable high-resolution, non-destructive evaluation of AM components across multiple scales, from sub-micrometer to macroscopic levels. This paper explores modern XCT and XRM techniques for multiscale characterization of AM parts, focusing on their ability to detect and analyze defects such as porosity, cracks, inclusions, and surface roughness, while offering insights into defect formation mechanisms, material properties, and process-induced variations. The integration of deep learning (DL) frameworks, including Simurgh, DeepRecon, and DeepScout, enhances XCT/XRM workflows by reducing scan times, improving resolution recovery, and enabling accurate defect detection even with limited projection data. These DL-based methods overcome limitations of traditional reconstruction techniques, enabling faster, more reliable characterization of dense materials like Inconel 718 and novel alloys such as AlCe. Applications include process parameter optimization, high-throughput quality control, and multistage AM process evaluation, with DL-enhanced workflows accelerating analysis times from weeks to days. Correlative imaging approaches further validate XCT and XRM data against scanning electron microscopy (SEM) images of physically sectioned samples, confirming the accuracy of DL-based reconstructions and enabling comprehensive defect analysis. While challenges remain in generalizing DL models to diverse materials and imaging conditions, improvements in resolution, noise reduction, and defect detection highlight the transformative potential of these methods. This multiscale and correlative approach enables precise identification and correlation of microstructural features with the overall performance of AM components. By integrating advanced XCT, XRM, and DL techniques, this paper demonstrates a significant leap forward in AM characterization, offering valuable insights into the relationships between processing parameters, microstructure, and part performance, and driving innovations that enhance the quality and reliability of AM products for demanding industrial applications.

Additive manufacturing↗

First beam tests of prototype silicon modules for the CMS High Granularity Endcap Calorimeter

The High Luminosity phase of the Large Hadron Collider will deliver 10 times more integrated luminosity than the existing collider, posing significant challenges for radiation tolerance and event pileup on detectors, especially for forward calorimetry. As part of its upgrade program, the Compact Muon Solenoid collaboration is designing a high-granularity calorimeter (HGCAL) to replace the existing endcap calorimeters. It will feature unprecedented transverse and longitudinal readout and triggering segmentation for both electromagnetic and hadronic sections. The electromagnetic section and a large fraction of the hadronic section will be based on hexagonal silicon sensors of 0.5–1 cm 2 cell size, with the remainder of the hadronic section being based on highly-segmented scintillators with silicon photomultiplier readout. The intrinsic high-precision timing capabilities of the silicon sensors will add an extra dimension to event reconstruction, especially in terms of pileup rejection. First hexagonal silicon modules, using the existing Skiroc2 front-end ASIC developed for CALICE, have been tested in beams at Fermilab and CERN in 2016. Here, we present results from these tests, in terms of system stability, calibration with minimum-ionizing particles and resolution (energy, position and timing) for electrons, and the comparisons of these quantities with GEANT4-based simulation.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Picosecond Timing Resolution Measurements of Low Gain Avalanche Detectors with a 120 GeV Proton Beam for the TOPSiDE Detector Concept

This paper presents results that take a critical step toward proving 10 ps timing resolution’s feasibility for particle identification in the TOPSiDE detector concept for the Electron-Ion Collider. Measurements of LGADs with a thickness of 35 μm and 50 μm are evaluated with a 120 GeV proton beam. The performance of the gain and timing response is assessed, including the dependence on the reverse bias voltage and operating temperature. The best timing resolution of UFSDs in a test beam to date is achieved using three combined planes of 35 μm thick LGADs at -30°C with a precision of 14.3 ± 1.5 ps.

Particle tracking detectors↗