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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 397 records · Page 22
All sourcesNASA NTRSDOE OSTI
NASA NTRS1984

Material growth and characterization for solid state devices

During the reporting period, InGaAs was grown on Fe-doped (semi-insulating) (100) InP substrates by current controlled liquid phase epitaxy (CCLPE) at 640 C and current densities of 2.5A sq/cm to 5 A/sq cm for periods from 5 to 30 minutes. Special efforts were made to reduce the background carrier concentration in the grown layers as much as possible. The best layers exhibited carrier concentrations in the mid-10 to the 15th power/cu cm range and up to 10,900 sq cm/V-sec room temperature mobility. InGaAsP quaternary layers of energy gap corresponding to wavelengths of approximately 1.5 microns and 1.3 microns were grown on (100) InP substrates by CCLPE. In the device fabrication area, work was directed toward processing MISFET's using InGaAs. SiO2, Si3N4 and Al2O3 were deposited by ion beam sputtering, electron beam evaporation and chemical vapor reaction on Si, GaAs, and InGaAs substrates. SiO2 and Si3N4 sputtered layers were found to possess a high density of pinhole defects that precluded capacitance-voltage analysis. Chemical vapor deposited Al2O3 layers on Si, GaAs and InGaAs substrates also exhibited a large number of pinhole defects. This prevented achieving good MIS devices over most of the substrate surface area.

Stefanakos, E. K.↗
NASA NTRS1986

Solid-State Detector for Trace Materials

Detector for trace chemicals senses as few as 10 to the 12th power molecules of given material on surface. Contains no moving parts, amenable to large-scale integration, and operates at room temperature. Potential applications in industrial process control and in environmental analysis. Characteristic signals indicate presence of certain chemicals.

Lambe, J. J.↗
NASA NTRS1984

Material growth and characterization for solid state devices

Manganese was used as the dopant for p-type InGaAs layers grown on semi-insulating (Fe-doped) and n-type (Sn-doped) InP substrates. Optical, electrical (Hall) and SIMS measurements were used to characterize the layers. Mn-diffusion into the substrate (during the growth of In GaAs) was observed only when Fe-doped substrates were used. Quaternary layers of two compositions corresponding to wavelengths (energy gaps) of approximated 1.52 micrometers were successfully grown at a constant temperature of 640 C and InP was grown in the temperature range of 640 C to 655 C. A study of the effect of pulses on the growth velocity of InP indicated no significant change as long as the average applied current was kept constant. A system for depositing films of Al2O3 by the pyrolysis of aluminum isopropoxide was designed and built. Deposited layers on Si were characterized with an ellipsometer and exhibited indices of refraction between 1.582 and 1.622 for films on the order of 3000 A thick. Undoped and p-type (Mn-doped) InGaAs epitaxial layers were also grown on Fe-doped InP substrates through windows in sputtered SiO2 (3200 A thick) layers.

Stefanakos, E. K.↗
NASA NTRS1985

Welding, Bonding and Fastening, 1984

A compilation of papers presented in a joint NASA, American Society for Metals, The George Washington University, American Welding Soceity, and Society of Manufacturing Engineers conference on Welding, Bonding, and Fastening at Langley Research Center, Hampton, VA, on October 23 to 25, 1984 is given. Papers were presented on technology developed in current research programs relevant to welding, bonding, and fastening of structural materials required in fabricating structures and mechanical systems used in the aerospace, hydrospace, and automotive industries. Topics covered in the conference included equipment, hardware and materials used when welding, brazing, and soldering, mechanical fastening, explosive welding, use of unique selected joining techniques, adhesives bonding, and nondestructive evaluation. A concept of the factory of the future was presented, followed by advanced welding techniques, automated equipment for welding, welding in a cryogenic atmosphere, blind fastening, stress corrosion resistant fasteners, fastening equipment, explosive welding of different configurations and materials, solid-state bonding, electron beam welding, new adhesives, effects of cryogenics on adhesives, and new techniques and equipment for adhesive bonding.

Buckley, J. D.↗
NASA NTRS1986

Primary magmatic carbon in ureilites - Evidence from cohenite-bearing metallic spherules

The compositions and mineralogy of metal-sulfide spherules trapped in ureilites are studied. Electron microprobe analyses of metallic phases and sulfides in spherules were conducted and backscattered electron images of metallic spherules in olivine and in ureilites are presented. It is observed that the spherules are composed of cohenite, Fe-Ni metal, troilite, and rare phosphorus-bearing minerals. The intergranular metal and graphite in the ureilites are analyzed. The phase relations of cohenite-bearing spherules are considered. Spherules represent Fe-Ni-C-S alloys that exist as immiscible metallic liquid droplets in the silicate magma from which ureilite olivine and pigeonite crystallized. The data reveal that graphite crystals occur as inclusions in olivine and ureilites and therefore graphite in ureilites is a primary magnetic component. It is hypothesized that graphite is a residue from the solid source materials that melted to produce the ureilite parent magma or crystallized from the magma.

Goodrich, C. A.↗
NASA NTRS1988

Direct solar-pumped iodine laser amplifier

A XeCl laser pumped iodine laser oscillator was developed which will be incorporated into the Master Oscillator Power Amplifier (MOPA) system. The developed XeCl laser produces output energy of about 60 mJ per pulse. The pulse duration was about 10 nsec. The kinetic model for the solar-pumped laser was refined and the algorithm for the calculation of a set of rate equations was improved to increase the accuracy and the efficiency of the calculation. The improved algorithm was applied to explain the existing experimental data taken from a flashlamp pumped iodine laser for three kinds of lasants, i-C3F7I, n-C4F9I, and t-C4F9I. Various solid laser materials were evaluated for solar-pumping. The materials studied were Nd:YAG, Nd:YLF, and Cr:Nd:GSGG crystals. The slope efficiency of 0.17 percent was measured for the Nd:YLF near the threshold pump intensity which was 211 solar constants (29W/sq cm). The threshold pump intensity of the Nd:YAG was measured to be 236 solar constants (32W/sq cm) and the near-threshold slope efficiency was 0.12 percent. True CW laser operation of Cr:Nd:GSGG was possible only at pump intensities less than or equal to 1,500 solar constants (203 W/sq cm). This fact was attributed to the high thermal focusing effect of the Cr:Nd:GSGG rod.

Han, Kwang S.↗
NASA NTRS1988

Titanium carbide coatings for aerospace ball bearings

In conventional ball bearings, steel to steel contacts between the balls and the raceways are at the origin of microwelds which lead to material transfer, surface roughening, lubricant breakdown, and finally to a loss in the bearing performances. To minimize the microwelding tendencies of the contacting partners it is necessary to modify their surface materials; the solid to solid collisions themselves are difficult to avoid. The use of titanium carbide coated steel balls can bring spectacular improvements in the performances and lifetimes of both oil-grease lubricated and oil-grease free bearings in a series of severe applications.

Boving, Hans J.↗
NASA NTRS1989

Grinding Si3N4 Powder In Si3N4 Equipment

Three methods of grinding compared. Report based on study of grinding silicon nitride powder in preparation for sintering into solid ceramic material. Attrition, vibratory, and ball mills lined with reaction-bonded silicon nitride tested. Rates of reduction of particle sizes and changes in chemical compositions of powders measured so grinding efficiences and increases in impurity contents from wear of mills and media evaluated for each technique.

Herbell, Thomas P.↗
NASA NTRS1988

Sensor technology

The objective is to provide necessary expertise and technology to advance space remote sensing of terrestrial, planetary, and galactic phenomena through the use of electromagnetic and electro-optic properties of gas, liquid, and solid state materials technology. The Sensor Technology Program is divided into two subprograms: a base research and development part and a Civil Space Technology Initiative (CSTI) part. The base research and development consists of research on artificially grown materials such as quantum well and superlattice structure with the potential for new and efficient means for detecting electromagnetic phenomena. Research is also being done on materials and concepts for detector components and devices for measuring high energy phenomena such as UV, X-, and gamma rays that are required observables in astrophysis and solar physics missions. The CSTI program is more mission driven and is balanced among four major disciplines: detector sensors; submillimeter wave sensors; LIDAR/DIAL sensors; and cooler technology.

Sokoloski, Martin M.↗
NASA NTRS1988

Material growth and characterization for solid state devices

During the period of this research grant, the process of liquid phase electroepitaxy (LPEE) was used to grow ternary and quaternary alloy III-V semiconductor thin films. Selective area growth of InGaAs was performed on InP substrates using a patterned sputtered quartz or spin-on glass layer. The etch back and growth characteristics with respect to substrate orientation were investigated. The etch back behavior is somewhat different from wet chemical etching with respect to the sidewall profiles which are observed. LPEE was also employed to grow epitaxial layers of InGaAsP alloys on InP substrates. The behavior of Mn as an acceptor dopant was investigated with low temperature Hall coefficient and photoluminescence measurements. A metal-organic vapor phase epitaxy system was partially complete within the grant period. This atmospheric pressure system will be used to deposit III-V compound and alloy semiconductor layers in future research efforts.

Collis, Ward J.↗
NASA NTRS1989

Electrochemical incineration of wastes

A low temperature electrolysis process has been developed for the treatment of solid waste material and urine. Experiments are described in which organic materials are oxidized directly at the surface of an electrode. Also, hypochlorite is generated electrochemically from chloride component of urine. Hypochlorite can act as a strong oxidizing agent in solution. The oxidation takes place at 30-60 C and the gaseous products from the anodic reaction are carbon dioxide, nitrogen, oxygen. Hydrogen is formed at the cathode. Carbon monoxide, and nitrogen oxides and methane were not detected in the off gases. Chlorine was evolved at the anode in relatively low amounts.

Kaba, L.↗
NASA NTRS1990

Inelastic transient dynamic analysis of three-dimensional problems by BEM

A general direct boundary element formulation and its numerical implementation for solving transient dynamic problems of three-dimensional isotropic homogeneous or piecewise homogeneous solids involving material nonlinearities are presented. The algorithm produces accurate results for static nonlinear problems by using large time steps. When a large value of yield stress is selected, the incremental inelastic transient algorithm produces results identical to those obtained by elastodynamic analysis.

Ahmad, S.↗
NASA NTRS1990

Piezoelectrostatic generator

A piezoelectrostatic generator includes a plurality of elongated piezoelectric elements having first and second ends, with the first ends fixedly mounted in a cylindrical housing and the second extending radially inwardly toward an axis. A shaft movable along the axis is connected to the inner ends of the elements to produce bending forces in piezoelectric strips within the elements. Each element includes a pair of strips mounted in surface contact and in electrical series to produce a potential upon bending. Electrodes spaced from the strips by a solid dielectric material act as capacitor plates to collect the potential charge.

Robertson, Glen A.↗
NASA NTRS1989

High resolution spectroscopy of the 11.3 micron emission band

High resolution spectra of the 11.3 micron emission band in M82 and NGC 7027 were obtained using the University of Texas IR echelle spectrometer on the IRTF in April 1988. The spectral resolution was 0.004 micron, with coverage from 11.0 to 11.6 microns. Spectra were measured at ten positions along a 10 min. long slit. Analysis of the data is still in progress, but initial results show no clear evidence of narrow structure within the feature. The analysis will involve comparison of the observed spectra to laboratory and predicted spectra of Polycylic Aromatic Hydrocarbons (PAHs) and Quenched Carbonaceous Composite (QCCs) to determine which may be responsible for the emission. The spectra will be examined with a goal of determining whether the emission is caused by molecular or solid state material. The data are also examined for evidence of variations in the shape and strength of the 11.3 micron feature with position on the sky. In NGC 7027 the 10 min. long slit went across the edge of the ionized nebulae, allowing comparison of emission from both ionized and neutral regions.

Achtermann, Jeff M.↗
NASA NTRS1989

The evolution of organic mantles on interstellar grains

By laboratory simulation of the chemical processes on dust grains it was investigated how solid organic materials can be produced in the interstellar medium. The ice mantles that accrete on grains in molecular clouds, consisting primarily of H2O, CO, H2CO, NH3, and O2, are irradiated by the internal UV field, resulting in the storage of radicals upon photodissociation of the original molecules. Transient heating events lead to the production of oxygen-rich organic species by recombination reactions. The experiments indicated that in this way the observed amount of organic material can be produced if a grain passes a few times through a molecular cloud during its life. After the destruction of the cloud the grains enter a more diffuse medium. Here they are subjected to the interstellar UV field as well as to collisions with atomic hydrogen. Experiments show that the intense photoprocessing results in the removal of small species like H2O and NH3 as well as in carbonization of the organic molecules. Contrary to this, the atomic H flux will maintain a certain hydrogen level in the mantle. These processes likely convert the original, oxygen-rich organics into an unsaturated hydrocarbon type material such as that observed towards IRS 7 and in Comet Halley grains.

Schutte, Willem A.↗
NASA NTRS1991

Impact processes in the Solar System: New understandings through numerical modeling

A collision of two rocky objects circling the sun in space, each roughly the size and mass of a large mountain range, was modeled. A fragmentation hydrocode was developed to perform dynamical computations of collisional outcomes. Explosive framentation and fluid dynamics were used and drawn together into a single application. To model a solid, certain material parameters, such as density, elasticity, rigidity, and energies of melting and vaporization were input. These parameters are well-known for a variety of important materials, such as ice, iron, granite, and basalt. Another important parameter used is the distribution of initial flaws within the material.

Asphaug, E.↗
NASA NTRS1991

Etching method for photoresists or polymers

A method for etching or removing polymers, photoresists, and organic contaminants from a substrate is disclosed. The method includes creating a more reactive gas species by producing a plasma discharge in a reactive gas such as oxygen and contacting the resulting gas species with a sacrificial solid organic material such as polyethylene or polyvinyl fluoride, reproducing a highly reactive gas species, which in turn etches the starting polymer, organic contaminant, or photoresist. The sample to be etched is located away from the plasma glow discharge region so as to avoid damaging the substrate by exposure to high energy particles and electric fields encountered in that region. Greatly increased etching rates are obtained. This method is highly effective for etching polymers such as polyimides and photoresists that are otherwise difficult or slow to etch downstream from an electric discharge in a reactive gas.

Lerner, Narcinda R.↗
NASA NTRS1990

Melt migration in a silicate liquid-olivine system - An experimental test of compaction theory

An experimentally derived melt migration profile is compared with those obtained from compaction theory. A couple is prepared in which a source-for-melt (a disk composed of a silicate glass and olivine) was placed in contact with a sink-for-melt (a disk of polycrystalline olivine) in order to induce melt migration under laboratory conditions. It is noted that melt infiltrates into the sink disk along triple junctions driven by capillary forces. In order to analyze the melt migration profile in terms of compaction theory, the equations developed by McKenzie (1984) to describe porous flow of a liquid in a deformable matrix were modified. The bouyancy force term is replaced with a capillary force term and governing equations are then solved numerically with the initial boundary conditions specified by the experimental design. Also, it is determined that compaction theory provides a good description of the experimental results provided that the permeability of these solid-liquid materials increases linearly with increasing liquid fraction.

Riley, G. N., Jr.↗