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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 397 records · Page 22
All sourcesNASA NTRSDOE OSTI
NASA NTRS2016

Imparting Barely Visible Impact Damage to a Stitched Composite Large-Scale Pressure Box

The Pultruded Rod Stitched Efficient Unitized Structure (PRSEUS) is a concept that was developed by The Boeing Company to address the complex structural design aspects associated with a pressurized hybrid wing body (HWB) aircraft configuration, which has been a focus of the NASA Environmentally Responsible Aviation Project. The NASA-Boeing structural development for the HWB aircraft culminated in testing of the multi-bay box, which is an 80%-scale representation of the pressurized center-body section. This structure was tested in the NASA Langley Research Center Combined Loads Test System facility. As part of this testing, barely visible impact damage was imparted to the interior and exterior of the test article to demonstrate compliance with a condition representative of the requirements for Category 1 damaged composite structure as defined by the Federal Aviation Regulations. Interior impacts were imparted using an existing spring-loaded impactor, while the exterior impacts were imparted using a newly designed, gravity-driven impactor. This paper describes the impacts to the test article, and the design of the gravitydriven guided-weight impactor. The guided-weight impactor proved to be a very reliable method to impart barely visible impact damage in locations which are not easily accessible for a traditional drop-weight impactor, while at the same time having the capability to be highly configurable for use on other aircraft structures.

Lovejoy, Andrew E.↗
DOE OSTI2020

Response of Pseudomonas putida to Complex, Aromatic-Rich Fractions from Biomass

There is strong interest in the valorization of lignin to produce valuable products; however, its structural complexity has been a conversion bottleneck. Chemical pretreatment liberates lignin-derived soluble fractions that may be upgraded by bioconversion. Here, cholinium ionic liquid pretreatment of sorghum produced soluble, aromatic-rich fractions that were converted by Pseudomonas putida (P. putida), a promising host for aromatic bioconversion. Growth studies and mutational analysis demonstrated that P. putida growth on these fractions was dependent on aromatic monomers but unknown factors also contributed. Proteomic and metabolomic analyses indicated that these unknown factors were amino acids and residual ionic liquid; the oligomeric aromatic fraction derived from lignin was not converted. A cholinium catabolic pathway was identified, and the deletion of the pathway stopped the ability of P. putida to grow on cholinium ionic liquid. This work demonstrates that aromatic-rich fractions obtained through pretreatment contain multiple substrates; conversion strategies should account for this complexity.

09 BIOMASS FUELS↗
NASA NTRS2012

Structural Analyses and Margins of Safety

There is an increasing reliance on modeling and simulation to verify, quantify, and certify designs of complex structures. The availability of a range of commercial modeling and simulations tools and packages with a variety of capabilities, in conjunction with increased computational resources, is allowing analysts to rapidly perform detailed analyses. However, care should be taken to understand specific tool limitations, assumptions, and boundary conditions as erroneous results can be generated without being recognized by the analysts. In addition, the reported margins of safety should be carefully interrogated to identify any false positive or negative margins and highlight any areas for structural concern.

Structural Analyses↗
DOE OSTI2025

Asymmetric loading of TnsE regulates Tn7 targeting of DNA replication structures

Abstract Tn7 transposable elements are known for their sophisticated target-site selection mechanisms. For the prototypical Tn7 element, dedicated transposon-encoded proteins direct insertions to either a conserved site in the chromosome or replicating DNA structures in conjugal plasmids, ensuring the vertical and horizontal spread of the element. While the pathway targeting the attTn7 site in the bacterial chromosome has been extensively studied, the pathway targeting DNA replication structures remains poorly understood. We have used an integrative structural biology approach to elucidate how the Tn7-encoded protein TnsE recognizes replication sites. Using native mass spectrometry, we found that TnsE forms 1:1 and 2:1 (TnsE:DNA) complexes on 3′-recessed DNA, with gain-of-function TnsE variants favoring the formation of 2:1 complexes. Structural characterization confirms that two TnsE molecules bind to DNA with the C-terminal domain of the protein recognizing duplex DNA, leaving the N-terminal domain to impose DNA substrate specificity and recruit the core transposition machinery. Collectively, our work is consistent with a model where TnsE-mediated target-site selection relies on the formation of an asymmetric TnsE:DNA complex to recruit the Tn7 transposase to DNA replication structures.

Biochemistry & Molecular Biology↗
DOE OSTI2023

Synchrotron x-Ray Study of Heterostructured Materials: A Review

Heterostructured materials (HSMs) have shown great potential for breaking the strength-ductility tradeoff. HSMs consist of heterogeneous zones that may have different sizes, shapes, compositions, structures, etc. Interactions and competitions among them often lead to unprecedented properties. However, due to the complex structures in a broad range of length scales, it is challenging to unravel deformation physics and strengthening mechanisms underlying extraordinary mechanical properties. Synchrotron x-rays provide powerful techniques and indispensable tools for investigating HSMs at various length scales. Here, we will present in situ high-energy x-ray diffraction and Laue x-ray microdiffraction techniques and their application in studying the HSMs. In this study, the principles of these techniques will be briefly introduced. We will focus on their application in studying stress partitioning and plastic accommodation during tensile deformation, thermo-driven and/or stress-driven phase transformations and various deformation microstructures like geometrically necessary dislocations and local stress/strain distributions, etc., in HSMs. Some important findings will be summarized. Challenging issues remain in studying HSMs and will be discussed.

36 MATERIALS SCIENCE↗
NASA NTRS1975

Experiences in using modal synthesis within project requirements

Modal synthesis methods were developed for use by engineers for cost-effective solutions of large structural dynamics problems. Different methods were proposed by various investigators based upon comparative solutions of relatively simple structures using different forms of displacement functions. The application of modal synthesis methods to a large complex structure in a project environment is described. The considerations include analysis, hardware interfaces, schedules, tests, resources, and other project requirements. Good technical results were obtained through the use of an integrated analysis/test modal synthesis on both substructures and systems.

Garba, J. A.↗
DOE OSTI2022

Controlling superconductivity of CeIrIn 5 microstructures by substrate selection

Superconductor/metal interfaces are usually fabricated in heterostructures that join these dissimilar materials. A conceptually different approach has recently exploited the strain sensitivity of heavy-fermion superconductors, selectively transforming regions of the crystal into the metallic state by strain gradients. The strain is generated by differential thermal contraction between the sample and the substrate. Here, we present an improved finite-element model that reliably predicts the superconducting transition temperature in CeIrIn 5 even in complex structures. Different substrates are employed to tailor the strain field into the desired shapes. Using this approach, both highly complex and strained as well as strain-free microstructures are fabricated to validate the model. This enables a high degree of control over the microscopic strain fields and forms the basis for more advanced structuring of superconductors as in Josephson junctions yet also finds natural use cases in any material class in which a modulation of the physical properties on a chip is desirable.

36 MATERIALS SCIENCE↗
NASA NTRS1972

Computerized multilevel analysis for multilayered fiber composites

A FORTRAN 4 computer code for the micromechanics, macromechanics, and laminate analysis of multilayered fiber composite structural components is described. The code can be used either individually or as a subroutine within a complex structural analysis/synthesis program. The inputs to the code are constituent materials properties, composite geometry, and loading conditions. The outputs are various properties for ply and composite; composite structural response, including bending-stretching coupling; and composite stress analysis, including comparisons with failure criteria for combined stress. The code was used successfully in the analysis and structural synthesis of flat panels, in the buckling analysis of flat panels, in multilayered composite material failure studies, and lamination residual stresses analysis.

Chamis, C. C.↗
NASA NTRS1972

Computerized multilevel analysis for multilayered fiber composites.

A FORTRAN IV computer code for the micromechanics, macromechanics, and laminate analysis of multilayered fiber composite structural components is described. The code can be used either individually or as a subroutine within a complex structural analysis/synthesis program. The inputs to the code are constituent materials properties, composite geometry, and loading conditions. The outputs are various properties for ply and composite; composite structural response, including bending-stretching coupling; and composite stress analysis, including comparisons with failure criteria for combined stress. The code was used successfully in the analysis and structural synthesis of flat panels, in the buckling analysis of flat panels, in multilayered composite material failure studies, and lamination residual stresses analysis.

Chamis, C. C.↗
NASA NTRS1980

Fabrication of a graphite/epoxy composite leading edge for laminar flow control

Lockheed, under NASA contract, has recently completed the first phase of a program to evaluate laminar flow control concepts for transport aircraft. Achievement of laminar flow over a wing surface requires a system of slots, metering holes, ducts and pumps to be used to remove the turbulent air adjacent to the surface. This requirement poses severe restrictions on conventional metallic structure. Graphite/epoxy composite with its unique properties appears to be the material that might solve the very complex structural problems associated with a laminar flow control aircraft. A six-foot span graphite/epoxy test article incorporating provisions for leading edge cleaning, deicing and laminar flow control was designed, fabricated and tested.

Beall, R. T.↗
NASA NTRS1984

Noise path identification using face-to-face and side-by-side microphone arrangements

In large complex structures, with several major sound transmission paths and high levels of background noise, it can be a complex task to locate and rank the contribution of an individual sound transmission path. The two microphone acoustic intensity techniques are investigated as a tool for path identification. Laboratory tests indicate that, if the intensity transmitted through a particular section of the fuselage is measured in the presence and absence of flanking paths using the face to face and side by side microphone arrangements, then no significant difference exists between the two measured intensities if the face to face microphone arrangement is used. However, if the side by side arrangement is used, then considerable difference exists between the two measured intensities.

Atwal, M.↗
NASA NTRS1986

A continuous record of tectonic evolution from 3.5 Ga to 2.6 Ga in Swaziland and northern Natal

The approx. 3.5 Ga-old bimodal suite underlying an extensive area in southwestern Swaziland comprises the oldest-dated sialic rocks in the Kaapvaal structural province. The suite consists of leucocratic, layered tonalitic-trondhjemitic gneisses and amphibolites characterized by the effects of repeated high strains. This suite is considered to represent a sialic basement on which metavolcanic and metasedimentary rocks, now preserved as scattered greenstone remnants, accumulated. Direct evidence to confirm this temporal relationship is lacking, but structural data from the Dwalile, Assegaai and Commondale areas indicate that (1) the bimodal gneisses experienced a complex structural history prior to the first recognizable deformation in the supracrustal rocks (i.e., D1 in the supracrustals is equivalent to Dn + 1 in the gneisses) and (2) scattered remnants of the Dwalile rocks infolded with the bimodal suite structurally overlie the gneisses and are preserved in synformal keels. Significant proportions of metaquartzites and metapelites are present in the Assegaai greenstone sequence, the presence of which implies the existence of felsic crust in the source area from which these sediments were derived, a conclusion that is consistent with the structural data.

Hunter, D. R.↗
NASA NTRS1992

Structural system reliability calculation using a probabilistic fault tree analysis method

The development of a new probabilistic fault tree analysis (PFTA) method for calculating structural system reliability is summarized. The proposed PFTA procedure includes: developing a fault tree to represent the complex structural system, constructing an approximation function for each bottom event, determining a dominant sampling sequence for all bottom events, and calculating the system reliability using an adaptive importance sampling method. PFTA is suitable for complicated structural problems that require computer-intensive computer calculations. A computer program has been developed to implement the PFTA.

Torng, T. Y.↗
NASA NTRS1990

Spacecraft dynamics characterization and control system failure detection

Two important aspects of the control of large space structures are studied: the modeling of deployed or erected structures including nonlinear joint characteristics; and the detection and isolation of failures of the components of control systems for large space structures. The emphasis in the first task is on efficient representation of the dynamics of large and complex structures having a great many joints. The initial emphasis in the second task is on experimental evaluation of FDI methodologies using ground-based facilities in place at NASA Langley Research Center and Marshall Space Flight Center. The progress to date on both research tasks is summarized.

Vandervelde, Wallace E.↗
DOE OSTI2024

Variation in Cation Adsorption Mechanism Controlled by Chemical and Structural Heterogeneities at the Quartz (101)–Water Interface

Mineral–water interfacial reactions are central to chemical processes that control the fate of nutrients and contaminants in natural environments. Mineral surfaces commonly have complex structures and compositions whose impact on interfacial reactivity is poorly understood. Here, in this work, we investigated the effects of surface heterogeneities on Rb + sorption at the quartz (101)–10 mM RbCl solution interface at pH 9.8 using in situ high-resolution X-ray reflectivity. Two surface locales (i.e., Spots A and B) having distinct interfacial structures were chosen: Spot A was characterized by its low defect density (≤20% topmost Si vacancies) and Rb + adsorption occurred predominantly as an inner-sphere complex. In comparison, Spot B had a higher defect density (~50% vacancies) and was covered with poorly crystalline SiO 2 . A substantially larger Rb + uptake (i.e., 7-times higher coverage) was observed on this defective surface where Rb + incorporated in the vacancy sites (confirmed by density functional tight binding-based molecular dynamics simulations) or adsorbed directly on the disordered film. These results provide a direct quantification of how surface heterogeneity influences the geochemical behavior of mineral–water interfaces, in particular highlighting the important role of chemical and structural defects on the sorbate speciation and coverage at silicate mineral surfaces.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2021

In Situ TEM Tensile Testing of Bicrystals with Tailored Misorientation Angles

Grain boundaries have complex structural features that influence strength, ductility and fracture in metals and alloys. Grain boundary misorientation angle has been identified as a key parameter that controls their mechanical behavior, but the effect of misorientation angle has been challenging to isolate in polycrystalline materials. Here, we describe the use of bicrystal Au thin films made using a rapid melt growth process to study deformation at a single grain boundary. Tensile testing is performed on bicrystals with different misorientation angles using in situ TEM, as well as on a single crystalline sample. Plastic deformation is initiated through dislocation nucleation from free surfaces. Grain boundary sliding is not observed, and failure occurs away from the grain boundary through plastic collapse in all cases. The failure behavior in these nanoscale bicrystals does not appear to depend on the misorientation angle or grain boundary energy but instead has a more complex dependence on sample surface structure and dislocation activity.

36 MATERIALS SCIENCE↗