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NASA NTRS2018

Aubrite and Impact Melt Enstatite Chondrite Meteorites as Potential Analogs to Mercury

The MESSENGER (MErcury Sur-face, Space ENvironment, GEochemistry and Ranging) orbiter measured the Mercurian surface abundances of key rock-forming elements to help us better understand the planet's surface and bulk geochemistry. A major discovery is that the Mercurian surface and interior are characterized by an extremely low oxygen fugacity (ƒO2; Iron-Wüstite (IW) -7.3 to IW-2.6. This is supported by low Fe and high S abundances on the surface. This low ƒO2 causes a different elemental partioning from what is observed on Earth. Using surface composition, it was shown that the Mercurian surface mainly consists of normative plagioclase, pyroxene, olivine, and exotic sulfides, such as niningerite ((Mg,Mn, Fe)S) and oldhamite (CaS).

Wilbur, Z. E.↗
NASA NTRS2018

Can Silicon-Smelting Contribute to the Low O/Si Ratio on the Surface of Mercury?

The MErcury Surface, Space ENvironment, GEochemistry, and Ranging (MESSENGER) spacecraft collected data that provided important insights into the structure, chemical makeup, and compositional diversity of Mercury. Among the many discoveries about Mercury made by MESSENGER, several surprising compositional characteristics of the surface were observed. These discoveries include elevated sulfur abundances (up to 4 wt.%), elevated abundances of graphitic carbon (0-4.1 wt.% across the surface with an additional 1-3 wt.% graphite above the global average in low reflectance materials), low iron abundances (less than 2 wt.%), and low oxygen abundances (O/Si weight ratio of 1.20+/-0.1). These exotic characteristics likely have important implications for the thermochemical evolution of Mercury and point to a planet that formed under highly reducing conditions. In the present study, we focus specifically on the low O/Si ratio of Mercury, which is anomalous compared to all other planetary materials. A recent study that considered the geochemical implications of the low O/Si ratio reported that 12-20% of the surface materials on Mercury are composed of Si-rich, Si-Fe alloys. They further postulated that the origin of the metal is best explained by a combination of space weathering and graphite-induced smelting that was facilitated by interaction of graphite with boninitic and komatiitic parental liquids. The goal of the present study is to assess the plausibility of smelting on Mercury through experiments run at the conditions that McCubbin et al. indicated would be favorable for Si-smelting.

McCubbin, F. M.↗
NASA NTRS2016

Simulating the Surface of Venus on Earth

The growing interest in comparative climatology among the terrestrial planets, the explosion of planets being discovered around other stars and the exciting results of recent orbital and remote observations of Venus provide evidence for a growing case to better understand Earths sister planet. The surface of Venus is quite unlike Earths surface conditions, and in fact is rather extreme. Science, technology, and planetary mission communities have a growing interest in the unique physiochemical properties and processes that occur under extreme temperature and pressure conditions in exotic and even hostile chemical environments such as Venus. The steadily growing catalog of exoplanets likely contains many examples of bodies with environments dramatically different than the surface of the Earth. Understanding these properties and processes will help us under-stand the history and present day state of inhospitable and even inaccessible regions of the Earth as well as other solar or extrasolar planets. Additionally, Venus and Saturn targets are prioritized in the current Planetary Decadal Survey, with reference missions that include in-situ investigations of these challenging environments. The fact that two of the five recent Discovery mission proposals selected by NASA for further development are Venus-focused adds additional priority and even urgency to laboratory-based extreme environment investigations. In addition to the importance of science-focused investigations, there is a current and future need for understanding the behavior of advanced technologies and materials in these extreme environments. The materials of course make up instruments and systems in missions and ultimately the success of planetary missions is dependent upon performance testing of instruments and systems in conditions that closely approximate those of the target. Until very recently, there was limited ability to accurately simulate Venus surface-like conditions, especially in vessels large enough to accommodate full-size instruments and components. This gap in capability is being addressed by NASA Glenn's Extreme Environment Rig, called GEER, located in Cleveland, Ohio. This large chamber allows for engineering tests of newly-developed as well as heritage instruments, while simultaneously affording opportunities for geochemical and materials-based science investigations.

Simulation↗
NASA NTRS2018

Exoplanet Biosignatures: Observational Prospects

Exoplanet hunting efforts have revealed the prevalence of exotic worlds with diverse properties, including Earth-sized bodies, which has fueled our endeavor to search for life beyond the Solar System. Accumulating experiences in astrophysical, chemical, and climatological characterization of uninhabitable planets are paving the way to characterization of potentially habitable planets. In this paper, we review our possibilities and limitations in characterizing temperate terrestrial planets with future observational capabilities through the 2030s and beyond, as a basis of a broad range of discussions on how to advance "astrobiology" with exoplanets. We discuss the observability of not only the proposed biosignature candidates themselves but also of more general planetary properties that provide circumstantial evidence, since the evaluation of any biosignature candidate relies on its context. Characterization of temperate Earth-sized planets in the coming years will focus on those around nearby late-type stars. The James Webb Space Telescope (JWST) and later 30-meter-class ground-based telescopes will empower their chemical investigations. Spectroscopic studies of potentially habitable planets around solar-type stars will likely require a designated spacecraft mission for direct imaging, leveraging technologies that are already being developed and tested as part of the Wide Field InfraRed Survey Telescope (WFIRST) mission. Successful initial characterization of a few nearby targets will be an important touchstone toward a more detailed scrutiny and a larger survey that are envisioned beyond 2030. The broad outlook this paper presents may help develop new observational techniques to detect relevant features as well as frameworks to diagnose planets based on the observables.

Characterization↗
NASA NTRS2018

Calculating the Modal Mineralogy of Aubrite Meteorites Using X-Ray Computed Tomography

The aubrites are a group of differentiated meteorites that formed in extremely reducing conditions, with oxygen fugacities (ƒO2) ranging from ~2 to ~6 log units below the Iron-Wüstite buffer. At these extreme conditions, elements that are lithophile (silica-loving) on Earth can behave as chalcophiles (sulfur-loving) or siderophiles (metal-loving), and FeO-poor silicates and exotic sulfides can form. Elemental partitioning among minerals at these conditions are still not well understood, thus studying aubrites could help better constrain elemental behavior. Only 30 aubrites exist; however, they display various textures, which can be difficult to identify in small samples. Identifying composite clasts can help in understanding the igneous history of the aubrite parent bodies. In order to distinguish different minerals and textures in larger samples, we use X-ray computed tomography (XCT), which is a useful, non-destructive analysis that can produce a 3D representation of a meteorite's textures, structures, and modal mineralogy. This study investigates the Norton County aubrite using XCT. Norton County is a fragmental impact breccia aubrite, and was an observed fall with a main mass of 1.1 tons. This large amount of material offers an opportunity to investigate a great volume of reduced, aubritic sample and study a more diverse variety of clasts. Here we report XCT results of two samples of Norton County (NC 15417) in order to constrain the 3D modal mineralogy of silicates, sulfides, and metals, and to identify unique clasts within the matrix.

Wilbur, Zoe↗
NASA NTRS2018

Potential Mercurian Analogues: Aubrite and Enstatite Chondrite Impact Melt Meteorites

The MESSENGER (MErcury Surface Space ENvironment GEochemistry and Ranging Spacecraft) mission provided new data that have helped us better constrain the surficial mineralogy and composition of Mercury. Mercury has an extremely low oxygen fugacity (f O2) (Iron Wustite (IW) -7.3 to IW -2.6), and at these unique conditions, elements, which usually exhibit lithophile behavior on Earth, can exhibit chalcophile or siderophile behavior on Mercury. No samples have been returned from Mercury; therefore, we must study candidate meteorite analogs to better understand the formation conditions of minerals inferred to be present at the Mercurian surface and Mercurian magmatic processes. In this study, we present a comprehensive analysis of a representative suite of eight aubrites and four enstatite chondrite impact melts (ECIM), which both have a similar f O2 to Mercury, and contain exotic sulfides that have been inferred to be present at the Mercurian surface. These characteristics allow us to assess their relevance for understanding the mineralogy and magmatic processes of Mercury. The ECIM were previously classified as aubrites, but we show that they are actually ECIM with a potential EH (high enstatite) parent body origin due to the presence of niningerite, Si-enriched kamacite, and uniform Ni in schreibersite. We propose that, with respect to the aubrites, the ECIM represent an ideal candidate for Mercurian studies due to their mineralogy and modal mineralogy. Compared to the aubrites, the ECIM samples do not contain forsterite or diopside, show a poorer sulfide diversity, contain graphite, and have a higher volume percentage of metal phases. Although the Mercurian surface contains forsterite and diopside, graphite and a similar amount of metal and sulfides as seen in the ECIM are inferred to be present on Mercury. According to the calculated normative Mercurian mineralogy, both candidate meteorites are most analogous to the Caloris Basin and Northern Plains Lower Mg regions.

Wilbur, Zoe E.↗
NASA NTRS2019

Experimental Insights into the Geochemistry of Mercury

With the recent estimate of Mercury's surface composition from the X-Ray Spectrometer and Gamma-Ray Spectrometer that were onboard NASA's MErcury Surface, Space ENvironment, Geochemistry and Ranging (MESSENGER) spacecraft, we now have our first opportunity to directly investigate the compositions of lavas from the planet Mercury and indirectly investigate the chemical make-up of its interior. Results from MESSENGER showed exotic surface compositions with more than 3 wt% sulfur in some lavas and relatively low amounts of iron (less than 3 wt%) across the surface. These striking features are consistent with magmatism occurring under highly reducing conditions which has an impact on the thermal and chemical evolution of a planetary body. Here we'll explore the geochemical evolution of Mercury through a series of experimental studies and discuss the implications of low oxygen fugacity on elemental behavior and magmatic processes.

Vander Kaaden, Kathleen E.↗
NASA NTRS2019

The Geochemistry of Aubrites: Investigating Reduced Parent Bodies

The aubrites (~30 known meteorites) are a unique group of differentiated meteorites that formed on asteroids with oxygen fugacities (ƒO2) from ~2 to ~6 log units below the iron-wüstite buffer [1–2]. At these highly reduced conditions, elements deviate from the geochemical behavior exhibited at terrestrial ƒO2, forming FeO-poor silicates, Si-bearing metals, and exotic sulfides [3]. Here we examine the 3D mineralogy and the geochemistry of fourteen aubrites, including mineral major element compositions, bulk-rock compositions, and oxygen isotopic compositions to understand their formation and evolution at extreme ƒO2 conditions. While previous studies have described the petrology and 2D modal abundances of aubrites, this work investigates the 3D modal mineralogies of silicate, metal, and sulfide phases in aubrite samples, which are then com-pared to the available 2D data. We utilize X-ray computed tomography (XCT) to non-destructively analyze the distribution and abundances of mineral phases in aubrites and locate composite clasts of sulfide grains for future analysis.

Wilbur, Z. E.↗
NASA NTRS2018

Novel Applications of Focused Ion Beam Technique for Planetary Sample Analyses

We are using innovative FIB techniques to prepare samples of planetary materials for different types of coordinated analyses using ion microprobes, synchrotron beamlines, and specialized transmission electron microscopy (TEM) techniques. In these cases, the FIB sample preparation is the critical step in enabling these specialized analyses. We discuss several examples below utilizing the FEI Quanta3D instrument at the NASA Johnson Space Center. Trace element analyses utilizing synchrotron x-ray fluorescence. The trace element content of mineral grains in comet dust provides important clues on their formation and processing in the early solar system. We preformed coordinated analyses of a comet dust particle that had been prepared using ultramicrotomy for TEM analysis. Following the TEM analyses, we extracted a 70 nm thick section from a region of the carbon (C) film of the TEM grid, for additional analyses. A carbon ring ~2-3 μm thick was deposited on top of the C film using the FIB. The C film on the outer rim of the ring was milled away using various patterns to uniformly release the stresses on the film, preventing rupture and collapse, and was attached to the micromanipulator needle. We then isolated the ring completely and transferred the section to a silicon sample holder for analysis using the HXN (hard X-ray nanoprobe) beamline at NSLSII at Brookhaven National Lab. Coordinated Analyses of Presolar Grains. Rare sub-m presolar grains that originate in evolved stars and supernovae, occur in primitive astromaterials and are identified by their exotic isotopic compositions. Coordinated analyses of these grains using NanoSIMS, TEM, and other techniques on the same grain is enabled by innovative FIB sample preparation. In order to obtain subsequent isotopic analyses of Mg and Fe, contributions from surrounding grains were minimized. We precisely deposited a protective cap of Pt on top of the grain to preserve the grain of interest and then milled away about 5 μm diameter of the surrounding material. Following the isotopic analyses, the spindle was extracted and thinned to electron transparency for TEM microstructural analyses. In situ heating TEM experiments on lunar samples. We extracted a FIB thin section from Apollo 17 lunar rock 76015. To avoid ion-beam damage, e-beam deposition was used to deposit the first 500 nm of the C strap, followed by ion beam-assisted deposition of ~3 μm carbon. We performed an ex situ lift-out of the section and placed the section on one of the elements of a microelectromechanical systems (MEMS) - specialized heating substrate and attached the section to the substrate by depositing small C straps with the FIB. The heating chips utilize silicon nitride windows to support the samples and provide uniform heating while enabling TEM imaging. The heating chip was loaded into a Hitachi “Blaze” heating holder and analyzed using a Hitachi HF5000 at the University of Arizona.

Rahman, Z.↗
NASA NTRS2019

Investigating the History of Aubrites Using X-Ray Computed Tomography and Bulk Partition Coefficients

The aubrites are a unique group of differentiated meteorites that formed on parent bodies with oxygen fugacities (ƒO2) from ~2 to ~6 log units below the iron-wustite buffer. At these highly reduced condi- tions, elements deviate from the geochemical behavior exhibited at terrestrial ƒO2, and may form FeO-poor silicates, Si-bearing metals, and exotic sulfides. Geochemical examinations of aubrites, such as mineral major-element compositions, bulk-rock compositions, O isotopes, and crystallization ages, are crucial to understand their formation and evolution at extreme ƒO2 conditions. In this study, we determine partitioning relationships of elements between bulk silicate, sulfide, and metal phases within aubrites, and compare the results to partition coefficients determined from petrologic experiments run under mercurian conditions. While previous studies have described the petrology and 2D modal abundances of aubrites, this work provides the first 3D view of aubritic mineralogies, which are com- pared to the available 2D data. Constraints of 3D modal abundances will increase the accuracy of computed bulk distribution coefficients; therefore, 3D scans of aubrite samples are imperative. We utilize X-ray computed tomogra- phy (XCT) to non-destructively analyze the distribution and abundances of mineral phases in aubrites and locate composite clasts of sulfide grains for future analysis.

Wilbur, Z. E.↗
NASA NTRS2019

MeV Emission from Pulsar Wind Nebulae: Understanding Extreme Particle Acceleration in Highly Relativistic Outflows

The Earth is constantly bombarded from outer space by energetic particles. Where and how these "cosmic rays" are produced is poorly understood, with various particle types and energies likely originating from different sources. Particularly mysterious is the source of high-energy e+/- produced in our Galaxy, especially those responsible for both the high fraction of e+ in the GeV cosmic ray lepton spectrum and the e+/- and observed excess of microwaves and gamma-rays detected towards the Galactic center and bulge. While these particles could be evidence for exotic forms of dark matter, they might also be produced by "normal" astrophysical sources such as pulsars the strongly magnetized, rapidly rotating neutron stars whose rotational energy powers an ultra-relativistic outflow (commonly referred to as a "pulsar wind") whose interaction with the surrounding medium creates a pulsar wind nebula .While the detection of TeV emission from numerous PWNe strongly suggest they contain e+/- with PeV or higher energies, how and to what energies these particles are produced is unknown, let alone their dependence on the properties of the pulsar, pulsar wind, and surrounding medium. A major reason for this uncertainty is the lack of information concerning their MeV properties, since the synchrotron emission from the highest energy e+/- peaks in this waveband. Only by combining the MeV spectrum of PWNe measured by proposed missions with that obtained at lower (primarily radio and X-ray) and higher (TeV) photon energies by current and hopefully future facilities is it possible to measure the full spectrum of e+/- in these sources. The resultant insights into the underlying acceleration mechanism would significantly impact many areas of astrophysics from indirect searches for dark matter to the origin of cosmic rays to the physics of relativistic outflows observed from active galactic nuclei, gamma-ray bursts, and some gravitational wave events.

Gelfand, Joseph D.↗
NASA NTRS2019

Magnetars as Astrophysical Laboratories of Extreme Quantum Electrodynamics: The Case for a Compton Telescope

A next generation of Compton and pair telescopes that improve MeV-band detection sensitivity by more than a decade beyond current instrumental capabilities will open up new insights into a variety of astrophysical source classes. Among these are magnetars, the most highly magnetic of the neutron star zoo, which will serve as a prime science target for a new mission surveying the MeV window. This paper outlines the core questions pertaining to magnetars that can be addressed by such a technology. These range from global magnetar geometry and population trends, to incisive probes of hard X-ray emission locales, to providing cosmic laboratories for spectral and polarimetric testing of exotic predictions of QED, principally the prediction of the splitting of photons and magnetic pair creation. Such fundamental physics cannot yet be discerned in terrestrial experiments. State of the art modeling of the persistent hard X-ray tail emission in magnetars is presented to outline the case for powerful diagnostics using Compton polarimeters. The case highlights an inter-disciplinary opportunity to seed discovery at the interface between astronomy and physics.

Wadiasingh, Zorawar↗
NASA NTRS2019

Negative Mass in Contemporary Physics, and Its Application to Propulsion

As first analyzed by Hermann Bondi in 1957, matter with negative mass is consistent with the structure of Einstein's general theory of Relativity. Although initially the concept was considered just a theoretical curiosity, negative mass, or "exotic matter," is now incorporated into the body of mainstream physics in a number of forms. Negative mass has a number of rather non-intuitive properties, which, as first noted by Bondi, and then later commented on by Forward (1990), Landis (1991), and others, results in possible applications for propulsion requiring little, or possibly no, expenditure of fuel. As pointed out by Morris and Thorne (1988) and others, negative mass (or, more strictly, a violation of the null energy condition) is also a requirement for any proposed faster than light travel. This paper presents the basic theory of negative mass, the ways by which it can manifest in contemporary physical theory, and the counterintuitive properties that result, including possible uses for interstellar propulsion. Although negative mass has moved from a theoretical curiosity to a concept fundamental to the contemporary understanding of physics, it is still not clear whether bulk negative mass can be manufactured, or if it is limited to only appearing at the cosmological scale (e.g., “dark energy:) or in the quantum (e.g., Casimir vacuum) limit. If it can be manufactured, the propulsion applications would be significant.

Landis, Geoffrey A.↗
NASA NTRS2019

Negative Mass in Contemporary Physics and its Application to Propulsion

As first analyzed by Hermann Bondi in 1957, matter with negative mass is consistent with the structure of Einstein's general theory of Relativity. Although initially the concept was considered just a theoretical curiosity, negative mass, or "exotic matter," is now incorporated into the body of mainstream physics in a number of forms. Negative mass has a number of rather non-intuitive properties, which, as first noted by Bondi, and then later commented on by Forward (1990), Landis (1991), and others, results in possible applications for propulsion requiring little, or possibly no, expenditure of fuel. As pointed out by Morris and Thorne (1988) and others, negative mass (or, more strictly, a violation of the null energy condition) is also a requirement for any proposed faster than light travel. This paper presents the basic theory of negative mass, the ways by which it can manifest in contemporary physical theory, and the counterintiutive properties that result, including possible uses for interstellar propulsion.Although negative mass has moved from a theoretical curiosity to a concept fundamental to the contemporary understanding of physics, it is still not clear whether bulk negative mass can be manufactured, or if it is limited to only appearing at the cosmological scale (e.g., "dark energy:) or in the quantum (e.g., Casimir vacuum) limit. If it can be manufactured, the propulsion applications would be significant.

Landis, Geoffrey A.↗
NASA NTRS2020

PHALANX: Expendable Projectile Sensor Networks for Planetary Exploration

Technologies enabling long-term, wide-ranging measurement in hard-to-reach areas are a critical need for planetary science inquiry. Phenomena of interest include flows or variations in volatiles, gas composition or concentration, particulate density, or even simply temperature. Improved measurement of these processes enables understanding of exotic geologies and distributions or correlating indicators of trapped water or biological activity. However, such data is often needed in unsafe areas such as caves, lava tubes, or steep ravines not easily reached by current spacecraft and planetary robots. To address this capability gap, we have developed miniaturized, expendable sensors which can be ballistically lobbed from a robotic rover or static lander - or even dropped during a flyover. These projectiles can perform sensing during flight and after anchoring to terrain features. By augmenting exploration systems with these sensors, we can extend situational awareness, perform long-duration monitoring, and reduce utilization of primary mobility resources, all of which are crucial in surface missions. We call the integrated payload that includes a cold gas launcher, smart projectiles, planning software, network discovery, and science sensing: PHALANX. In this paper, we introduce the mission architecture for PHALANX and describe an exploration concept that pairs projectile sensors with a rover “mothership.” Science use cases explored include reconnaissance using ballistic cameras, volatiles detection, and building timelapse maps of temperature and illumination conditions. Strategies to autonomously coordinate constellations of deployed sensors to self-discover and localize with peer ranging (i.e. a “local GPS”) are summarized, thus providing communications infrastructure beyond-line-of-sight (BLOS) of the rover. Capabilities were demonstrated through both simulation and physical testing with a terrestrial prototype. The approach to developing a terrestrial prototype is discussed, including design of the launching mechanism, projectile optimization, micro-electronics fabrication, and sensor selection. Results from early testing and characterization of commercial-off-the-shelf (COTS) components are reported. Nodes were subjected to successful burn-in tests over 48 hours at full logging duty cycle. Integrated field tests were conducted in the Roverscape, a half-acre planetary analog environment at NASA Ames, where we tested up to 10 sensor nodes simultaneously coordinating with an exploration rover. Ranging accuracy has been demonstrated to be within +/-10cm over 20m using commodity radios when compared to high-resolution laser scanner ground truthing. Evolution of the design, including progressive miniaturization of the electronics and iterated modifications of the enclosure housing for streamlining and optimized radio performance are described. Finally, lessons learned to date, gaps toward eventual flight mission implementation, and continuing future development plans are discussed.

Dille, Michael↗
NASA NTRSDate not supplied

3D Phase-Field Simulations of Pattern Formation During Freeze Casting

We present the results of a combined experimental and phase-field modeling study of pattern formation during freeze casting. Those studies use unidirectional freezing of simple binary liquid mixtures of water and sugars (sucrose and trehalose) in a temperature gradient, which suffice to produce hierarchical templated structures similar to those observed in more complex multi-component freeze-cast systems including lamellae, undulated ridges, and more exotic “jellyfish-like” substructures. Multiscale 3D phase-field simulations reproduce remarkably well those structures quantitatively and identify key properties of the ice-water interface that control their formation. They further reveal that lamellae form as a result of a novel symmetry-breaking secondary instability of partially faceted cellular structures and pinpoint additional secondary instability mechanisms giving rise to smaller-scale substructures.

Kaihua Ji↗
NASA NTRS2020

The NANOGrav 11 yr data set: Limits on Gravitational Wave Memory

The mergers of supermassive black hole binaries (SMBHBs) promise to be incredible sources of gravitational waves (GWs).While the oscillatory part of the merger gravitational waveform will be outside the frequency sensitivity range of pulsar timing arrays, the nonoscillatory GW memory effect is detectable. Further, any burst of GWs will produce GW memory, making memory a useful probe of unmodeled exotic sources and new physics. We searched the North American Nanohertz Observatory for Gravitational Waves (NANOGrav) 11 yr data set for GW memory. This data set is sensitive to very low-frequency GWs of ∼3 to 400 nHz (periods of ∼11 yr–1 month). Finding no evidence for GWs, we placed limits on the strain amplitude of GW memory events during the observation period. We then used the strain upper limits to place limits on the rate of GW memory causing events. At a strain of 2.5 × 10−14, corresponding to the median upper limit as a function of source sky position, we set a limit on the rate of GW memory events at <0.4 yr−1. That strain corresponds to an SMBHB merger with reduced mass of ηM ~2 × 1010Mmoonand inclination of ι = π/3 at a distance of 1 Gpc. As a test of our analysis, we analyzed the NANOGrav 9 yr data set as well. This analysis found an anomolous signal, which does not appear in the 11 yr data set. This signal is not a GW, and its origin remains unknown.

K Aggarwal↗