A comprehensive study of coupling agents in urethane and epoxy adhesives
Coupling agents in urethane and epoxy adhesives, discussing lap shear and T-peel tests on mild and stainless steels, Al and glass cloth substrates
Cassidy, P. E.↗
SEARCH · Search NASA
Results for “Adhesion Testing”
Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.
Processing study of a polyimidesulfone adhesive
An adhesive bonding process cycle study was performed for a polyimidesulfone (PISO2) recently developed as a promising structural adhesive. The high molecular weight, linear aromatic system possesses properties which make it attractive as a processable, low-cost material for elevated temperature applications. The results of a study to better understand the parameters that affect the adhesive properties of the polymer for titanium alloy adherends are detailed. These include the tape preparation, the use of a primer, and press and simulated autoclave processing conditions. The polymer was characterized using Fourier Transform Infrared Spectroscopy, glass transition temperature determination, flow measurements, and weight loss measurements. The adhesive's strength determined by lap shear strength tests was used to evaluate the effects of the bonding process variations. Higher lap shear strengths were obtained at room temperature when a primer (PISO2) was used; however, the results were the same at 232 C (450 F) with or without a primer. The use of a vacuum (simulated autoclave cycle) during titanium bonding produced similar lap shear strengths to those specimens bonded without a vacuum.
Progar, D. J.↗
Degradation of Dielectrics in Space
Effects of radiation (principally, electrons and protons) on dielectric materials summarized in report. Report based on radiation tests of optical coatings, temperature-control coatings, adhesives, radomes, thermal insulators, and light-control surfaces. Materials are primarily polymers and metal/organic coatings.
Bouquet, F. L.↗
Development of a reusable, flight-weight cryogenic foam insulation system
Attention is given to a light weight foam insulation system applicable to reusable cryogenic propellant tankage for hypersonic aircraft and space launch vehicles. The insulation system consists of nominally sized blocks of a high temperature-resistant polymethacrylimide foam that is wrapped with a vapor-impermeable membrane of Kapton-aluminum-Kapton laminate, which is adhesively bonded to the outer propellant tank wall. Test results are presented which indicate that this insulation system is capable of enduring a Mach 5 service environment without structural cracking, deterioration, or loss of performance.
Mcauliffe, P. S.↗
Evaluation results of the 700 deg C Chinese strain gages
There is a continuing interest and need for resistance strain gages capable of making static strain measurements on components located in the hot section of gas turbine engines. A paper by Tsen-tai Wu describes the development and evaluation of high temperature gauges fabricated from specially developed Fe-Cr-Al-V-Ti-Y alloy wire. Several of these gages and a quantity of P12-2 ceramic adhesive were purchased for evaluation. Nine members of the aircraft turbine engine community were invited to participate in an evaluation of these gages. Each participant was sent one strain gage, a small amount of ceramic adhesive, instructions for mounting the gage on a test beam, and a set of suggestions for the experiment. Data on gage factor variation with temperature, apparent strain, and drift are discussed.
Hobart, H. F.↗
International SAMPE Symposium and Exhibition, 37th, Anaheim, CA, Mar. 9-12, 1992, Proceedings
The present conference discusses the industrial and transportation markets for advanced composites, novel NASA and military applications of advanced materials, composite space structures, sandwich structures, composite tooling and processing, advanced epoxy compositions, composites repair, commercial applications of advanced resins, metal-matrix composites, adhesive compositions, ultrahigh-temperature composites, failure analyses, testing methods for composites, and bismaleimides and polyimides. Also discussed are composite structures design, innovations in composite reinforcement, nonautoclave-processed composites, molecular composites, design and manufacture processes with thermoplastics, automation in manufacturing, technologies for large component fabrication, damage-limitation design practices, thermoplastic-matrix composites, industrial applications of composites, and process controls in composites manufacturing.
Grimes, Glenn C.↗
Dust on Mars: An Aeolian Threat to Human Exploration?
The NASA HEDS Program is duly concerned for human explorers regarding the potential hazard posed by the ubiquitous dust mantle on Mars. To evaluate properties of dust that could be hazardous to humans, the MPS 2001 Lander payload will include the Mars Environmental Compatibility Assessment (MECA) experiment. This includes optical and atomic-force microscopy to evaluate soil grains for shape and size, wet chemistry to evaluate toxic substances, electrometry to evaluate triboelectric charging, and test-material palets to evaluate electrostatic and magnetic adhesion, and the hardness/abrasiveness of soil grains; these experimental subcomponents are delivered samples by the camera-equipped robotic arm of the lander which will acquire material from depths of 0.5 to 1.0 m in the soil. Data returned by MECA will be of value to both the BEDS and planetary/astrobiology communities. Dust poses a threat to human exploration because the martian system does not hydrologically or chemically remove fine particles that are being continuously generated by thermal, aeolian, and colluvial weathering, and by volcanism and impact over billions of years. The dust is extremely fine-grained, in copious quantities, ubiquitous in distribution, continually mobile, and a source of poorly-grounded static charges -- a suite of characteristics posing a particulate and electrical threat to explorers and their equipment. Dust is mobilized on global and regional scales, but probably also unpredictably and violently at local scales by dust devils. The latter might be expected in great abundance owing to near surface atmospheric instability (dust devils were detected by Pathfinder during its brief lifetime). Preliminary laboratory experiments suggest that space-suit materials subjected to windblown dust may acquire a uniform, highly adhesive dust layer that is also highly cohesive laterally owing to electrostatic forces. This layer will obscure visibility through the helmet visor, penetrate joints and fabrics, change the thermal properties of the suit, and possibly affect electronic/electrical suit functions. It is paramount that future missions address the issue of interparticle forces, and in particular, the role played by ionizing radiation in affecting these forces on Mars.
Marshall, J.↗
Dust on Mars: An Aeolian Threat to Human Exploration?
The NASA HEDS Program is duly concerned for human explorers regarding the potential hazard posed by the ubiquitous dust mantle on Mars. To evaluate properties of dust that could be hazardous to humans, the NMS 2001 Lander payload will include the Mars Environmental Compatibility Assessment (MECA) experiment. This includes optical and atomic-force microscopy to evaluate soil grains for shape and size, wet chemistry to evaluate toxic substances, electrometry to evaluate triboelectric charging, and test-material palets to evaluate electrostatic and magnetic adhesion, and the hardness/abrasiveness of soil grains; these experimental subcomponents are delivered samples by the camera-equipped robotic arm of the lander which will acquire material from depths of 0.5 to 1.0 m in the soil. Data returned by MECA will be of value to both the hEDS and planetary/astrobiology communities. Dust poses a threat to human exploration because the martian system does not hydrologically or chemically remove fine particles that are being continuously generated by thermal, aeolian, and colluvial weathering, and by volcanism and impact over billions of years. The dust is extremely fine-grained, in copious quantities, ubiquitous in distribution, continually mobile, and a source of poorly-grounded static charges -- a suite of characteristics posing a particulate and electrical threat to explorers and their equipment. Dust is mobilized on global and regional scales, but probably also unpredictably and violently at local scales by dust devils. The latter might be expected in great abundance owing to near surface atmospheric instability (dust devils were detected by Pathfinder during its brief lifetime). Preliminary laboratory experiments suggest that space-suit materials subjected to windblown dust may acquire a uniform, highly adhesive dust layer that is also highly cohesive laterally owing to electrostatic forces. This layer will obscure visibility through the helmet visor, penetrate joints and fabrics, change the thermal properties of the suit, and possibly affect electronic/electrical suit functions. It is paramount that future missions address the issue of interparticle forces, and in particular, the role played by ionizing radiation in affecting these forces on Mars.
Marshall, J.↗
UltraSail CubeSat Solar Sail Flight Experiment
UltraSail is a next-generation, highrisk, high-payoff sail system for the launch, deployment, stabilization, and control of very large (km2 class) solar sails enabling high payload mass fractions for interplanetary and deep space spacecraft. UltraSail is a non-traditional approach to propulsion technology achieved by combining propulsion and control systems developed for formation- flying microsatellites with an innovative solar sail architecture to achieve controllable sail areas approaching 1 km2, sail subsystem area densities approaching 1 g/m2, and thrust levels many times those of ion thrusters used for comparable deep space missions. UltraSail can achieve outer planetary rendezvous, a deep-space capability now reserved for high-mass nuclear and chemical systems. There is a twofold rationale behind the UltraSail concept for advanced solar sail systems. The first is that sail-andboom systems are inherently size-limited. The boom mass must be kept small, and column buckling limits the boom length to a few hundred meters. By eliminating the boom, UltraSail not only offers larger sail area, but also lower areal density, allowing larger payloads and shorter mission transit times. The second rationale for UltraSail is that sail films present deployment handling difficulties as the film thickness approaches one micrometer. The square sail requires that the film be folded in two directions for launch, and similarly unfolded for deployment. The film is stressed at the intersection of two folds, and this stress varies inversely with the film thickness. This stress can cause the film to yield, forming a permanent crease, or worse, to perforate. By rolling the film as UltraSail does, creases are prevented. Because the film is so thin, the roll thickness is small. Dynamic structural analysis of UltraSail coupled with dynamic control analysis shows that the system can be designed to eliminate longitudinal torsional waves created while controlling the pitch of the blades, while using solar photon pressure to slew the spin axis. Vacuum tests have also verified that electrostatic and molecular adhesion forces can substantially be eliminated by making the film electrically conductive, reducing the peel force of the film off the storage roll to levels of 100s of micro-N. The innovation demonstrated the capability of deploying a six-micron aluminum- coated film from a reel through a slit in vacuum. The innovation also demonstrated a spin-stabilized method for deploying a long reel of solar sail film using solar pressure to spin-up and orbit raise the satellite, and also a gravity gradient method for deploying a long reel of solar sail film using solar pressure to orbit raise the satellite. The solar sail mass fraction of 25% is consistent with high specific impulse ion systems, but without the added weight and cost of a power source and processing unit. The large sail area, coupled with low film density, is giving UltraSail a high payload fraction. The UltraSail deployment scheme unrolls a micrometerscale reflection-coated polyimide film from a storage mandrel to a maximum length of several kilometers with the aid of a blade tip satellite.
Carroll, David↗
Coldfinger Motion Suppression Using a Ceramic Applique
The development of a ceramic applique for the vibration suppression of a cryocooler coldfinger is a part of technology demonstration flight experiment.
bonding↗
Composites for Advanced Space Transportation Systems - (CASTS)
The CASTS Project initiated to develop graphite fiber/polyimide matrix (GR/PI) composite structures with 589K operational capability for aerospace vehicles is described. Near term tasks include screening composites and adhesives for 589K service, developing fabrication procedures and specifications, developing design allowables test methods and data, design and test of structural elements, and construction of a full scale aft body flap for the space shuttle orbiter vehicle for ground testing. Far term tasks include research efforts directed at new materials, manufacturing procedures and design/analysis methodology. Specific results discussed include: (1) identification of four GR/PI composites and three PI adhesives with 589K service potential for periods ranging from 125 to 500 hours; (2) development of an adhesive formulation suitable for bonding reusable surface insulation (RSI) titles to 589K (GR/PI) substructure; (3) the capability to fabricate and nondestructively inspect laminates, hat section shaped stiffeners, honeycomb sandwich panels, and chopped fiber moldings; and (4) test methods for measuring design allowables at 117K.
Davis, J. G., Jr.↗
Adhesive bonding for metal-lined filament-wound cryogenic pressure vessels.
Adhesives to bond metal linings to filament- wound cryogenic pressure vessels evaluated by test series simulating fabrication and service conditions
FILAMENT WINDING↗
Impact resistance of spar-shell composite fan blades
Composite spar-shell fan blades for a 1.83 meter (6 feet) diameter fan stage were fabricated and tested in a whirling arm facility to evaluate foreign object damage (FOD) resistance. The blades were made by adhesively bonding boron-epoxy shells on titanium spars and then adhesively bonding an Inconel 625 sheath on the leading edge. The rotating blades were individually tested at a tip speed of 800 feet per second. Impacting media used were gravel, rivets, bolt, nut, ice balls, simulated birds, and a real bird. Incidence angles were typical of those which might be experienced by STOL aircraft. The tests showed that blades of the design tested in this program have satisfactory impact resistance to small objects such as gravel, rivets, nuts, bolts, and two inch diameter ice balls. The blades suffered nominal damage when impacted with one-pound birds (9 to 10 ounce slice size). However, the shell was removed from the spar for a larger slice size.
Graff, J.↗
The Analysis of Adhesively Bonded Advanced Composite Joints Using Joint Finite Elements
The design and sizing of adhesively bonded joints has always been a major bottleneck in the design of composite vehicles. Dense finite element (FE) meshes are required to capture the full behavior of a joint numerically, but these dense meshes are impractical in vehicle-scale models where a course mesh is more desirable to make quick assessments and comparisons of different joint geometries. Analytical models are often helpful in sizing, but difficulties arise in coupling these models with full-vehicle FE models. Therefore, a joint FE was created which can be used within structural FE models to make quick assessments of bonded composite joints. The shape functions of the joint FE were found by solving the governing equations for a structural model for a joint. By analytically determining the shape functions of the joint FE, the complex joint behavior can be captured with very few elements. This joint FE was modified and used to consider adhesives with functionally graded material properties to reduce the peel stress concentrations located near adherend discontinuities. Several practical concerns impede the actual use of such adhesives. These include increased manufacturing complications, alterations to the grading due to adhesive flow during manufacturing, and whether changing the loading conditions significantly impact the effectiveness of the grading. An analytical study is conducted to address these three concerns. Furthermore, proof-of-concept testing is conducted to show the potential advantages of functionally graded adhesives. In this study, grading is achieved by strategically placing glass beads within the adhesive layer at different densities along the joint. Furthermore, the capability to model non-linear adhesive constitutive behavior with large rotations was developed, and progressive failure of the adhesive was modeled by re-meshing the joint as the adhesive fails. Results predicted using the joint FE was compared with experimental results for various joint configurations, including double cantilever beam and single lap joints.
Stapleton, Scott E.↗
Laser Surface Preparation and Bonding of Aerospace Structural Composites
Adhesive bonds are critical to the integrity of built-up structures. Disbonds can often be detected but the strength of adhesion between surfaces in contact is not obtainable without destructive testing. Typically the number one problem in a bonded structure is surface contamination, and by extension, surface preparation. Standard surface preparation techniques, including grit blasting, manual abrasion, and peel ply, are not ideal because of variations in their application. Etching of carbon fiber reinforced plastic (CFRP) panels using a neodymium-doped yttrium aluminum garnet (Nd:YAG) laser appears to be a highly precise and promising way to both clean a composite surface prior to bonding and provide a bond-promoting patterned surface akin to peel ply without the inherent drawbacks from the same (i.e., debris and curvature). CFRP surfaces prepared using laser patterns conducive to adhesive bonding were compared to typical prebonding surface treatments through optical microscopy, contact angle goniometry, and post-bonding mechanical testing.
Belcher, M. A.↗
The effect of low energy protons on silicon solar cells with simulated coverglass cracks
Results of a series of low-energy proton (LEP) tests are presented. The purpose of the tests was to investigate the effect of low-energy protons on the electrical performance of solar cells with simulated cracked covers. The results of the tests were then related to the space environment. A matrix of LEP tests was set up using solar cells with simulated cracks to determine the effect on electrical performance as a function of fluence, energy, crack width, coverglass adhesive shielding, crack location, and solar cell size. The results of the test were, for the most part, logical, and consistent.
Gasner, S.↗
Laser Surface Preparation for Adhesive Bonding of Aerospace Structural Composites
Adhesive bonds are critical to the integrity of built-up structures. Disbonds can often be detected but the strength of adhesion between surfaces in contact is not obtainable without destructive testing. Typically the number one problem in a bonded structure is surface contamination, and by extension, surface preparation. Standard surface preparation techniques, including grit blasting, manual abrasion, and peel ply, are not ideal because of variations in their application. Etching of carbon fiber reinforced plastic (CFRP) panels using a neodymium-doped yttrium aluminum garnet (Nd:YAG) laser appears to be a highly precise and promising way to both clean a composite surface prior to bonding and provide a bond-promoting patterned surface akin to peel ply without the inherent drawbacks from the same (i.e., debris and curvature). CFRP surfaces prepared using laser patterns conducive to adhesive bonding were compared to typical pre-bonding surface treatments through optical microscopy, contact angle goniometry, and post-bonding mechanical testing.
Belcher, M. A.↗
Tests of graphite/polyimide sandwich panels in uniaxial edgewise compression
The local and general buckling behavior of graphite/polyimide sandwich panels simply supported along all four edges and loaded in uniaxial edgewise compression were investigated. Material properties of sandwich panel constituents (adhesive and facings) were determined from flatwise tension and sandwich beam flexure tests. Buckling specimens were 30.5 by 33 cm, had quasi-isotropic, symmetric facings, and a glass/polyimide honeycomb core. Core thicknesses were varied and three panels of each thickness were tested at room temperature to investigate failure modes and corresponding buckling loads. Specimens 0.635 cm thick failed by overall buckling at loads close to the analytically predicted buckling load; all other panels failed by face wrinkling. Results of the wrinkling tests indicated that several buckling formulas were unconservative and therefore not suitable for design purposes; a recommended wrinkling equation is presented.
Camarda, C. J.↗