Arc jet tests of metallic TPS materials
Arc jets tests of thoria dispersed nickel base alloys and cobalt base alloys for space shuttle metallic thermal protection system
Centolanzi, F. J.↗
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Catalytic decomposition of sodium chlorate
Catalytic decomposition of sodium chlorate using cobalt oxide catalysts
Wydeven, T.↗
Promising catalyst for auto exhaust
Lanthanum cobalt oxide as potential auto exhaust catalyst from studies of activity in gas phase
Libby, W. F.↗
Advanced protective coating for superalloys
Superior oxidation protection for nickel-base alloys at temperatures up to 1367 K was obtained with cobalt-base alloy coating. Coating had 25 Cr, 14 Al, and 0.5 Y weight percent composition. Coating was applied by electron beam vapor deposition to thickness of 76 to 127 microns.
Elam, R. C.↗
The measurement of radiation exposure of astronauts by radiochemical techniques
The concentrations of 23 major, minor, and trace elements in the fecal samples from the Apollo 12 and 13 astronauts are reported. Most elemental excretion rates are comparable to rates reported for earlier missions. Exceptions are noted for calcium, iron, and tin. Body calcium and iron losses appear to be reduced during the Apollo 12 and 13 missions such that losses now seem to be insignificant. Refined measurements of tin excretion rates agree with normal dietary intakes. Earlier reported tin values are in error. A new passive dosimetry canister was designed which contains foils of tantalum, copper, titanium, iron, cobalt, aluminum, and scandium. By measuring the concentrations of the various products of nuclear reactions in these metals after space exposure, the characteristics of the incident cosmic particles can be determined.
Brodzinski, R. L.↗
Investigation of the fracture mechanics of boride composites
Fracture energies of WC-6Co, Boride 5 (ZrB2+SiC), Boride 8(ZrB2+SiC+C) and Boride 8-M2(ZrB2+SiC+C) were measured by slow bend and impact tests of notched charpy bars. Cobalt bonded tungsten carbide exhibited impact energies of 0.76 ft-lb or 73.9 in-lb/square inch. Boride 5 and the Boride 8 exhibit impact energies one third and one quarter of that observed for WC-6Co comparing favorably with measurements for SiC and Si3N4. Slow bend-notched bar-fracture energies for WC-6Co were near 2.6 in-lb/square inch or 1/20 the impact energies. Slow bend energies for Boride 8-M2, Boride 8 and Boride 5 were 58%, 42% and 25% of the value observed for WC-6Co. Fractograph showed differences for WC-6Co where slow bend testing resulted in smooth transgranular cleavage while samples broken by impact exhibited intergranular failures. By contrast the boride fractures showed no distinction based on testing method. Fabrication studies were conducted to effect alteration of the boride composites by alloying and introduction of graphite cloth.
Kaufman, L.↗
Use of radiation in preparative chemistry
A summary and updating of previous work on the use of radiation chemistry for the preparation of pure materials are presented. Work was chiefly concerned with the reduction of metal salts in solution to the free metal using 2 MeV electrons. Metals deposited from aqueous solution are copper, silver, zinc, cadmium, thallium, tin, lead, antimony, iron, nickel, cobalt, and palladium. Dry organic solvents were evaluated for the deposition of metals based on a study involving deposition of antimony from soltions of antimony (III) chloride. The use of organic liquids for the preparation of anhydrous metal halides is also presented. Reaction mechanisms for both organic liquids and aqueous system are discussed.
Philipp, W. H.↗
Exploratory screening tests of several alloys and coatings for automobile thermal reactors
A total of 23 materials (including uncoated ferritic and austenitic iron-base alloys, uncoated nickel and cobalt-base superalloys, and several different coatings on AISI 304 stainless steel) were screened as test coupons on a rack in an automobile thermal reactor. Test exposures were generally 51 hours including 142 thermal cycles of 10 minutes at 1010 + or - 30 C test coupon temperature and 7-minutes cool-down to about 510 C. Materials that exhibited corrosion resistance better than that of Hastelloy X include: a ferritic iron alloy with 6 weight percent aluminum; three nickel-base superalloys; two diffused-aluminum coatings on AISI 304; and a Ni-Cr slurry-sprayed coating on AISI 304. Preliminary comparison is made on the performance of the directly impinged coupons and a reactor core of the same material.
Oldrieve, R. E.↗
Permeameter for high-temperature magnetic measurements
A permeameter is described that measures the magnetizing force and the corresponding magnetic induction up to 1000 C. The two symmetrical yokes are made of an alloy of 9 percent iron, 91 percent cobalt. A coil surrounding the specimen supplies a magnetizing force of up to 100 oersteds. The instrument uses the magnetic potentiometer principle to cancel the effects of the reluctance of the yoke and the joint gaps. Very close agreement was obtained at room temperature when compared to an MH type permeameter. The effect of temperature on the normal induction curves for the yoke material is also presented.
Barranger, J. P.↗
Accelerator measurement of the energy spectra of neutrons emitted in the interaction of 3-GeV protons with several elements
The application of time of flight techniques for determining the shapes of the energy spectra of neutrons between 20 and 400 MeV is discussed. The neutrons are emitted at 20, 34, and 90 degrees in the bombardment of targets by 3 GeV protons. The targets used are carbon, aluminum, cobalt, and platinum with cylindrical cross section. Targets being bombarded are located in the internal circulating beam of a particle accelerator.
Nalesnik, W. J.↗
Solar cell radiation response near the interface of different atomic number materials
The response of cobalt 60 irradiated N/P silicon solar cells was measured as a function of the atomic number of the medium adjacent to the cell and the direction of the gamma ray beam. The interpositioning of various thicknesses of aluminum between the adjacent material and the cell had the effect of moving the cell to various locations in an approximate monatomic numbered medium. Using this technique the solar cell response was determined at various distances from the interface for gold and beryllium. The results were compared with predictions based upon ionization chamber measurements of dose perturbations in aluminum and found to agree within five percent. Ionization chamber data was then used to estimate the influence of various base contact materials.
Burke, E. A.↗
Evaluation, construction and endurance testing of compression sealed pyrolytic boron nitride slot insulation
A high-temperature statorette, consisting of an iron-27 percent cobalt magnetic lamination stack and nickel-clad silver conductors, was tested with pyrolytic boron nitride slot insulation. Temperatures were measured in each test to determine characteristics of slot linear heat conductance from statorette conductors. Testing was carried out to temperatures of approximately 1500 F in a vacuum environment of 10-8 torr. Three assemblies were built and tested, each having a different room temperature slot clearance. The final statorette assembly was subjected to a 100-hour vacuum aging test at 1400 F followed by 25 thermal cycles. Temperature data from the three assemblies showed that decreasing slot clearance and increasing compression loading did enhance heat transfer. The temperature difference between slot and lamination at 1400 F increased 4 F during the thermal aging and an additional 10 F during the 25 thermal cycles.
Grant, W. L.↗
High contrast cathode ray tube
A layer of material is described, which contains fine grains of phosphor material stimulated by electrons to produce visible radiation. The layer, which also contains fine grains of cobalt oxide, is deposited on the glass screen of a cathode ray tube to provide high contrast, by absorbing most of the visible radiation which is directed to the layer through the screen, while not materially affecting the visible light which the phosphor material produces in response to the electron stimulation.
Lisovicz, E. J.↗
Cyclic furnace oxidation of clad WI-52 systems at 1040 C and 1090 C
Cyclic furnace oxidation studies were conducted on the cobalt alloy WI-52 clad with Ni-30Cr, Fe-25Cr-4A1, and Ni-20Cr-4A1 foils (0.051 to 0.254 mm thick). Tests as long as 400 hours using 1- and 20-hour cycles showed that the Ni-Cr- and Fe-Cr-A1 claddings were about equally protective at both temperatures. The protective ability of these alloys was influenced by exposure temperature and cladding thickness. At both temperatures, they protected WI-52 about as well as, or better than, a widely used commercial aluminide coating. The Ni-Cr-Al claddings did not protect WI-52 nearly as well. Interdiffusion generally influenced the oxidation behavior of all clad WI-52 systems.
Gedwill, M. A.↗
Processing and plating helical metallic coils
The results of research efforts to develop an optimized nickel cobalt coating suitable as a recording medium are outlined. The coating is to be used directly on a BeCu helical coil substrate of a helical coil NASA recorder. Specifically, efforts were made to: optimize the coating thickness; establish processes and techniques adaptable for the production of finalized plated helical coils; design and fabricate the equipment required for production and testing of the coils; and deliver finalized helical coils to NASA.
Source record↗
Testing superalloys at 2000 (1367) and 2200 F (1478 K) in a Mach 4.6 airstream
Seven superalloy models were tested in a plasma arc tunnel facility. The test models were 3 in. (7.62cm) square flat surfaces (nominally 0.01 to 0.02 in. (0.0254 to 0.0508 cm) thick) held in a water-cooled wedge holder at a 60 deg (1.05 rad) angle of attack. The models were cycled 25 times (two were cycled 50 times) for 10 min each cycle in a Mach 4.6 test stream with the model leading edge temperature maintained at 2200 F (1478 K) (one at 2000 F (1367 K)). Backface temperatures were measured with four platinum-platinum 10% rhodium thermocouples and the front surface temperatures with an optical pyrometer. Four different nickel base alloy materials and one cobalt material were evaluated.
Land, D. W.↗
On the cyclic stress-strain behavior and low cycle fatigue of aerospace materials
The elastic-plastic deformation behavior under cyclic stress of a number of different engineering materials was experimentally investigated with the aid of high-precision methods of measuring, some of which had been newly developed. Experiments made with a variety of steels, the titanium alloy Ti-A16-V4, a cobalt (tungsten) alloy, the high-temperature material Nimonic 90 and Dural (A1-Cu) are reported. The theory given in an attempt to explain these experiments is aimed at finding general formulas for the cyclic stress-strain behavior materials.
Burbach, J.↗
Quantitative X-ray diffraction analysis of oxides formed on superalloys
Methods were developed for quantitative analysis by X-ray diffraction of the oxides Al2O3, NiO, Cr2O3, CoO, and CoCr2O4 within a standard deviation of about 10 percent of the weight fraction reported or within 1 percent absolute. These error limits assume that the sample oxides are well characterized and that the physiochemical structure of the oxides in the samples are identical with those in the synthesized standards. Results are given for the use of one of the techniques in the analysis of spalls from a series of oxidation tests of the cobalt base alloy WI-52.
Garlick, R. G.↗