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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 415 records · Page 23

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NASA NTRS2005

Growing Aligned Carbon Nanotubes for Interconnections in ICs

A process for growing multiwalled carbon nanotubes anchored at specified locations and aligned along specified directions has been invented. Typically, one would grow a number of the nanotubes oriented perpendicularly to a silicon integrated-circuit (IC) substrate, starting from (and anchored on) patterned catalytic spots on the substrate. Such arrays of perpendicular carbon nanotubes could be used as electrical interconnections between levels of multilevel ICs. The process (see Figure 1) begins with the formation of a layer, a few hundred nanometers thick, of a compatible electrically insulating material (e.g., SiO(x) or Si(y)N(z) on the silicon substrate. A patterned film of a suitable electrical conductor (Al, Mo, Cr, Ti, Ta, Pt, Ir, or doped Si), having a thickness between 1 nm and 2 m, is deposited on the insulating layer to form the IC conductor pattern. Next, a catalytic material (usually, Ni, Fe, or Co) is deposited to a thickness between 1 and 30 nm on the spots from which it is desired to grow carbon nanotubes. The carbon nanotubes are grown by plasma-enhanced chemical vapor deposition (PECVD). Unlike the matted and tangled carbon nanotubes grown by thermal CVD, the carbon nanotubes grown by PECVD are perpendicular and freestanding because an electric field perpendicular to the substrate is used in PECVD. Next, the free space between the carbon nanotubes is filled with SiO2 by means of CVD from tetraethylorthosilicate (TEOS), thereby forming an array of carbon nanotubes embedded in SiO2. Chemical mechanical polishing (CMP) is then performed to remove excess SiO2 and form a flat-top surface in which the outer ends of the carbon nanotubes are exposed. Optionally, depending on the application, metal lines to connect selected ends of carbon nanotubes may be deposited on the top surface. The top part of Figure 2 is a scanning electron micrograph (SEM) of carbon nanotubes grown, as described above, on catalytic spots of about 100 nm diameter patterned by electron-beam lithography. These and other nanotubes were found to have lengths ranging from 2 to 10 m and diameters ranging from 30 to 200 nm, the exact values of length depending on growth times and conditions and the exact values of diameter depending on the diameters and thicknesses of the catalyst spots. The bottom part of Figure 2 is an SEM of an embedded array of carbon nanotubes after CMP.

Li, Jun↗

DOE OSTI2020

Two-Dimensional Molecular Charge Density Waves in Single-Layer-Thick Islands of a Dirac Fermion System

Charge density waves have been intensely studied in inorganic materials such as transition metal dichalcogenides however its counterpart in organic materials has yet to be explored in detail. Here we report the finding of a robust two dimensional charge density waves in molecular layers formed by α-(BEDT-TTF) 2 -I 3 on a Ag(111) surface. Low temperature scanning tunnelling microscopy images of a multi-layer thick α-(BEDT-TTF) 2 -I 3 on Ag(111) substrate reveal coexistence of 5a0 x 5a0 and √31 a0 x √31 a0 R9° charge density wave patterns commensurate with the underlying molecular lattice at 80 K. Both charge density wave patterns remain in nano-size molecular islands with just a single constituent molecular-layer thickness at 80 K and 5 K. Local tunneling spectroscopy measurements reveal the variation of the gap from 244 meV to 288 meV between the maximum and minimum charge density wave locations. Density functional theory calculations further confirm a vertical positioning of BEDT-TTF molecules in the molecular layer. While the observed charge density wave patterns are stable for the defect sites, they can be reversely switched for one molecular lattice site by means of inelastic tunnelling electron energy transfer with the electron energies exceeding 400 meV using a scanning tunneling microscope manipulation scheme.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS1972

Scanning technique for tracking small eye-movements

Scanning technique images spot of blue light on fundus, measures variations in reflectance of spot and compares reflectance pattern with a stored reference pattern. Method then converts the difference from stored pattern into infrared eye motion.

Kelly, D. H.↗

NASA NTRS1977

New features of global climatology revealed by satellite-derived oceanic rainfall maps

Quantitative rainfall maps over the oceanic areas of the globe were derived from the Nimbus 5 Electrically Scanning Microwave Radiometer (ESMR) data. Analysis of satellite derived oceanic rainfall maps reveal certain distinctive characteristics of global patterns for the years 1973-74. The main ones are (1) the forking of the Intertropical Convergence Zone in the Pacific, (2) a previously unrecognized rain area in the South Atlantic, (3) the bimodal behavior of rainbelts in the Indian Ocean and (4) the large interannual variability in oceanic rainfall. These features are discussed.

Rao, M. S. V.↗

NASA NTRS1981

Auroral arc electrodynamic parameters measured by AE-C and the Chatanika radar

Auroral arc electrodynamic parameters are studied using coordinated measurements between the AE-C satellite and the Chatanika radar. On January 4, 1978, the spacecraft twice crossed an east-west aligned auroral arc at widely spaced longitudes, spanning more than 3 hours in local time. The Chatanika radar was scanning in elevation at a magnetic longitude equidistant from the two AE-C crossings. The electric field pattern around this arc was remarkably similar at the three longitudes. Equatorward of the arc the north-south field was very intense (greater than approximately 60 mV/m), whereas poleward of the arc it was small (approximately 10 mV/m). The east-west field was small and almost constant across the arc. The same arc was observed by the radar for about 1 hour, and this electric field pattern did not change, even though the arc location, intensity, and width changed substantially. For a given electric field the AE-C measured ion temperature was substantially different during each of the arc crossings. This dissimilarity is attributed to differences in the F region neutral wind at the two longitudes. It is shown that the electric field variations are consistent with the existence of polarization charges within the arc, even though the electric field remained small poleward of the arc.

Beaujardiere, O. D. L.↗

NASA NTRS1989

Observation and analysis for the bidirectional reflectance of stratus clouds at near-infrared wavelengths

Results are presented from observations of the spectral reflectance of marine stratocumulus clouds acquired during the First ISCCP Regional Experiment in June and July, 1987. The data were obtained with aircraft-mounted cross track scanning radiometers. The radiance data show persistent and significant scattering features. The characteristics of the observed NIR reflectance patterns are examined and compared with model calculations based on in situ particle measurements.

Spinhirne, J. D.↗

NASA NTRS1993

Final-Approach Spacing Aids (FASA) evaluation for terminal-area, time-based air traffic control

A jointly funded (NASA/FAA) real-time simulation study was conducted at NASA Langley Research Center to gather comparative performance data among three candidate final-approach spacing aid (FASA) display formats. Several objective measures of controller performance and their display eye-scan behavior as well as subjective workload and rating questionnaires were used. For each of two representative pattern-speed procedures (a 170-knot procedure and a 210-knot procedure with speed control aiding), data were gathered, via twelve FAA controllers, using four final-controller display format conditions (manual/ARTS 3, graphic marker, DICE countdown, and centerline slot marker). Measured runway separations were more precise with both the graphic marker and DICE countdown formats than with the centerline slot marker and both (graphic and DICE) improved precision relative to the manual/ARTS 3 format. For three separate rating criteria, the subject controllers ranked the FASA formats in the same order: graphic marker, DICE countdown, and centerline slot marker. The increased precision measured with the 210-knot pattern-speed procedure may indicate the potential for the application of speed-control aiding where higher pattern speeds are practical after the base-to-final turn. Also presented are key FASA issues, a rationale for the formats selected for testing, and their description.

Credeur, Leonard↗

DOE OSTI2026

Combustion-assisted ink-jet printing of nuclear targets

Advances in target fabrication are critical to high-precision measurements in nuclear physics. This work details the preparation of patterned CeO 2 and ThO 2 architectures and thin-film targets via ink-jet deposition of combustible solutions. The produced targets were characterized by scanning electron microscopy (SEM), and by alpha-particle spectroscopy for radioactive targets to determine densities. Ink jet printing of the targets, used both ethanol and 2-methoxyethanol as solvents, with cerium or thorium nitrate as the oxidizer and acetylacetone as the fuel. Additionally, we found that the distance between each droplet dispersion (step size) played the most significant role in determining the final pattern uniformity and thickness. A 50 μm step size leads to relatively thick targets with a density of 350 μg/cm 2 . Significant overlap in droplet sizes leads to a heterogeneous target with an undesirable cracked surface structure. In contrast, 150 μm spacing yields thinner (20 μg/cm 2 ) patterned structures with excellent surface coverage. This method of Ink-jet printing provides a straightforward, scalable, and high-efficiency pathway to prepare custom made, high-quality targets for nuclear physics experiments.

CeO2↗

NASA NTRS2019

Impact Damage Tolerance of Composite Laminates with Through-The-Thickness Stitches

The ability of through-the-thickness stitches to contain damage during a low-velocity impact event and increase the residual strength of stitched panels was investigated in this research. The impact response, spread of interlaminar delaminations, dent depth, surface damage, and static residual strength after impact were studied for carbon-epoxy specimens fabricated from HTS40 TohoTenax standard modulus fibers, stitched together with Vectran 1200 denier thread and infused with API 1078 resin after through-the-thickness stitching. Three different stitch patterns were used to explore the ability to arrest impact damage during and after impact. Simply supported boundary conditions were maintained during the impact testing. Non-destructive evaluations were performed using ultrasonic C-scans and X-ray computed tomography (CT) imaging to determine the shape, size, and location of delaminations. Results indicate that while the dynamic response during the impact event was almost the same for the unstitched specimens and all stitch patterns considered, the extent of delamination and the compression strength after impact varied greatly. For both the 60 J and 80 J impact energies, the delamination area was significantly less for the stitched specimens than for the unstitched specimens, but the range of delamination areas among the stitch patterns was much larger for the lower impact energy than for the greater impact energy. Similarly, while the presence of stitching influenced the compression after impact strength, the strength values for all stitch patterns were very similar. These results are a step toward quantifying the influence of through-the-thickness stitching.

Ranatunga, Vipul↗

NASA NTRS2006

Pattern-Recognition Algorithm for Locking Laser Frequency

A computer program serves as part of a feedback control system that locks the frequency of a laser to one of the spectral peaks of cesium atoms in an optical absorption cell. The system analyzes a saturation absorption spectrum to find a target peak and commands a laser-frequency-control circuit to minimize an error signal representing the difference between the laser frequency and the target peak. The program implements an algorithm consisting of the following steps: Acquire a saturation absorption signal while scanning the laser through the frequency range of interest. Condition the signal by use of convolution filtering. Detect peaks. Match the peaks in the signal to a pattern of known spectral peaks by use of a pattern-recognition algorithm. Add missing peaks. Tune the laser to the desired peak and thereafter lock onto this peak. Finding and locking onto the desired peak is a challenging problem, given that the saturation absorption signal includes noise and other spurious signal components; the problem is further complicated by nonlinearity and shifting of the voltage-to-frequency correspondence. The pattern-recognition algorithm, which is based on Hausdorff distance, is what enables the program to meet these challenges.

Karayan, Vahag↗

DOE OSTI2024

Random forest prediction of crystal structure from electron diffraction patterns incorporating multiple scattering

Diffraction is the most common method to solve for unknown or partially known crystal structures. However, it remains a challenge to determine the crystal structure of a new material that may have nanoscale size or heterogeneities. Here, in this study, we train an architecture of hierarchical random forest models capable of predicting the crystal system, space group, and lattice parameters from one or more unknown two-dimensional electron diffraction patterns. Our initial model correctly identifies the crystal system of a simulated electron diffraction pattern from a 20-nm-thick specimen of arbitrary orientation 67% of the time. We achieve a topline accuracy of 79% when aggregating predictions from ten patterns of the same material but different zone axes. The space group and lattice predictions range from 70% to 90% accuracy and median errors of 0.01-0.5Å, respectively, for cubic, hexagonal, trigonal, and tetragonal crystal systems while being less reliable on orthorhombic and monoclinic systems. We apply this architecture to a four-dimensional scanning transmission electron microscopy scan of gold nanoparticles, where it accurately predicts the crystal structure and lattice constants. These random forest models can be used to significantly accelerate the analysis of electron diffraction patterns, particularly in the case of unknown crystal structures. Additionally, due to the speed of inference, these models could be integrated into live transmission electron microscopy experiments, allowing real-Time labeling of a specimen.

36 MATERIALS SCIENCE↗

DOE OSTI2024

Power Electronics Materials and Bonded Interfaces - Reliability and Lifetime

The need for reliable bonded interface materials is critical to realize the performance benefits of wide-bandgap devices in power electronic modules, especially in operating temperatures greater than 150 degrees Celsius. In this paper, we investigate the thermomechanical performance of sintered copper (Cu) as a large-area attachment, bonded between Cu baseplates and active-metal-bonded substrates, under accelerated thermal shock (-40 degrees Celsius to 200 degrees Celsius) conditions. In the fabrication phase of the samples, we used different stencil patterns and found out that the grid and stripe patterns resulted in a better outgassing of the residual organics during the sintering process, thereby ensuring a substantially improved bond quality than a full-area print. The paste consisted of Cu microflakes and we performed sintering using a Budatec SP300 sintering press at 275 degrees Celsius with 15 MPa of bonding pressure for 5 minutes in a nitrogen atmosphere. Under accelerated experiments, we monitored the degradation of the sintered Cu bond in the samples through C-mode scanning acoustic microscope (C-SAM) images. To quantify the defect percentage in C-SAM images, we investigated image denoising techniques to exclude the pattern prints. Finally, we cross-sectioned a sample and obtained digital microscope images, which revealed adhesive fracture as the dominant failure mechanism.

ADVANCED PROPULSION SYSTEMS↗

NASA NTRS1975

Vertical velocity structure and geometry of clear air convective elements

The paper discusses observations of individual convective elements with a high-power narrow-beam scanning radar, an FM-CW radar, and an acoustic sounder, including the determination of the vertical air velocity patterns of convective structures with the FM-CW radar and acoustic sounder. Data are presented which link the observed velocity structure and geometrical patterns to previously proposed models of boundary layer convection. It is shown that the high-power radar provides a clear three-dimensional picture of convective cells and fields over a large area with a resolution of 150 m, where the convective cells are roughly spherical. Analysis of time-height records of the FM-CW radar and acoustic sounder confirms the downdraft-entrainment mechanism of the convective cell. The Doppler return of the acoustic sounder and the insect-trail slopes on FM-CW radar records are independent but redundant methods for obtaining the vertical velocity patterns of convective structures.

Rowland, J. R.↗

NASA NTRS1980

30/20 GHz demonstration system for improving orbit utilization

To guard against severe rain losses at 30 and 20 GHz, techniques are being developed which provide the high antenna gain needed to increase communications margins and frequency reuse capability through beam isolation, while providing complete coverage of the U.S. Effective bandwidths from a single satellite location may then reach tens of gigahertz, with capacity tailored to match nonuniform geographic demand patterns. Satellite onboard processing which includes forward-error-correction and the routing of channels to terminals will reduce scanning antenna requirements and increase rain margins, through the adaptive use of system margins to support those terminals experiencing rain. These antenna and onboard processing techniques are adaptable to C-band and Ku-band, in addition to Ka-band.

Holmes, W. M., Jr.↗

NASA NTRS1984

Satellite derived atmosphere water vapor as a tracer of large scale interactions between the atmosphere and ocean

Two water-vapor distributions and the accompanying circulation patterns which occurred over the North and South Atlantic Ocean during February 1979 are described. It is shown that scanning multichannel microwave radiometer observations from the Nimbus-7 satellite are used to remotely sense the vertically integrated atmospheric water vapor and liquid water, and the surface wind speed over the ocean and that they provide information on the ocean-atmosphere interaction. To provide evidence of the events revealed in the satellite observations, FGGE data are used.

Short, D. A.↗

NASA NTRS1990

Experiment K-6-01. Distribution and biochemistry of mineral and matrix in the femurs of rats

Previous analyses of the composition of mineral and matrix in the bone of young rats following space flight has revealed deficits in calcium, phosphorus, and osteocalcin, a non-collagenous protein, without an associated decrease in collagen. To characterize the location and nature of this mineralization defect in a weight bearing long bone, the femur, researchers attempted to relate the spatial distribution of mineral in situ in the proximal, central and distal thirds of the femoral diaphysis to the biochemical composition of bone from the same area. Biochemical analyses revealed lower concentrations of calcium, phosphorus and osteocalcin but not collagen only in the central third of the diaphysis of the flight animals (F) compared to synchronous controls (S). Collagen concentration was reduced only in the proximal third of the diaphysis, where all 3 crosslinks, expressed as nM/mol collagen were higher in F than S. A new technique, x ray microtomography, with a resolution of 26 microns, was used to obtain semi-quantitative data on mineral distribution in reconstructed sections of wet whole bone. To improve the resolution of the mineral density distribution, images of the surfaces of cut sections were analyzed by backscattered electrons in a scanning electron microscope (BSE). There was good agreement between the results of the two stereochemical techniques which revealed distinct patterns of mineralization in transverse and longitudinal directions of the diaphysis. The novel methodology developed for this flight experiment shows considerable promise in elucidating the biochemical nature of what appear to be regional alterations in the mineralization of long bones of animals exposed to spaceflight.

Arnaud, S.↗

NASA NTRSDate not supplied

Laser Ablative Patterning of B4C and MoAlB Ceramics for Hydrophobic Surfaces

Through a novel laser ablative patterning (LAP) process, the present work reports the increase in wetting contact angle of molybdenum aluminum boride (MoAlB) and the reduction of dust adhesion. The LAP technique employed picosecond laser pulses to form a crosshatch pattern with micropillars on ceramic surfaces. The wetting behavior was successfully transitioned from hydrophilic (θ < 90°) to hydrophobic (θ > 90°), which may be related to Wenzel or Cassie-Baxter mechanisms. Parameters such as laser fluence and number of laser scans were varied to study their effects on ceramic surface characteristics. Dust adhesion experiments were performed on these hydrophobic ceramic surfaces, which showed that the adhesion of lunar soil simulant dust particles was significantly reduced in the patterned MoAlB surface. The patterned MoAlB samples were further examined using the surveying lunar dust influence on device efficacy (SLIDE) testbed to evaluate the wear performance.

Bai Cui↗

DOE OSTI2023

Exploration of non-resonant divertor features on the Compact Toroidal Hybrid

Abstract Non-resonant divertors (NRDs) separate the confined plasma from the surrounding plasma facing components (PFCs). The resulting striking field line intersection pattern on these PFCs is insensitive to plasma equilibrium effects. However, a complex scrape-off layer (SOL), created by chaotic magnetic topology in the plasma edge, connects the core plasma to the PFCs through varying magnetic flux tubes. The Compact Toroidal Hybrid (CTH) serves as a test-bed to study this by scanning across its inductive current. Simulations observe a significant change of the chaotic edge structure and an effective distance between the confined plasma and the instrumented wall targets. The intersection pattern is observed to be a narrow helical band, which we claim is a resilient strike line pattern. However, signatures of finger-like structures, defined as heteroclinic tangles in chaotic domains, within the plasma edge connect the island chains to this resilient pattern. The dominant connection length field lines intersecting the targets are observed via heat flux modeling with EMC3-EIRENE. At low inductive current levels, the excursion of the field lines resembles a limited plasma wall scenario. At high currents, a private flux region is created in the area where the helical strike line pattern splits into two bands. These bands are divertor legs with distinct SOL parallel particle flow channels. The results demonstrate the NRD strike line pattern resiliency within CTH, but also show the underlying chaotic edge structure determining if the configuration is diverted or limited. This work supports future design efforts for a mechanical structure for the NRD.

Physics↗