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At least 433 records · Page 24

Laser velocimetry applied to transonic and supersonic aerodynamics

As a further demonstration of the capabilities of laser velocity in compressible aerodynamics, measurements obtained in a Mach 2.9 separated turbulent boundary layer and in the transonic flow past a two-dimensional airfoil section are presented and compared to data realized by conventional techniques. In the separated-flow study, the comparisons were made against pitot-static pressure data. Agreement in mean velocities was realized where the pressure measurements could be considered reliable; however, in regions of instantaneous reverse velocities, the laser results were found to be consistent with the physics of the flow whereas the pressure data were not. The laser data obtained in regions of extremely high turbulence suggest that velocity biasing does not occur if the particle occurrence rate is low relative to the turbulent fluctuation rate. Streamwise turbulence intensities are also presented. In the transonic airfoil study, velocity measurements obtained immediately outside the upper surface boundary layer of a 6-inch chord MACA 64A010 airfoil are compared to edge velocities inferred from surface pressure measurements. For free-stream Mach numbers of 0.6 and 0.8, the agreement in results was very good. Dual scatter optical arrangements in conjunction with a single particle, counter-type signal processor were employed in these investigations. Half-micron-diameter polystyrene spheres and naturally occurring condensed oil vapor acted as light scatterers in the two respective flows. Bragg-cell frequency shifting was utilized in the separated flow study.

Johnson, D. A.↗

Subgrid-scale horizontal and vertical variation of cloud water in stratocumulus clouds: a case study based on LES and comparisons with in situ observations

Abstract. Stratocumulus clouds in the marine boundary layer cover a large fraction of ocean surface and play an important role in the radiative energy balance of the Earth system. Simulating these clouds in Earth system models (ESMs) has proven to be extremely challenging, in part because cloud microphysical processes such as the autoconversion of cloud water into precipitation occur at scales much smaller than typical ESM grid sizes. An accurate autoconversion parameterization needs to account for not only the local microphysical process (e.g., the dependence on cloud water content qc and cloud droplet number concentration Nc) but also the subgrid-scale variability of the cloud properties that determine the process rate. Accounting for subgrid-scale variability is often achieved by the introduction of a so-called enhancement factor E. Previous studies of E for autoconversion have focused more on its dependence on cloud regime and ESM grid size, but they have largely overlooked the vertical dependence of E within the cloud. In this study, we use a large-eddy simulation (LES) model, initialized and constrained with in situ and surface-based measurements from a recent airborne field campaign, to characterize the vertical dependence of the horizontal variation of qc in stratocumulus clouds and the implications for E. Similar to our recent observational study (Zhang et al., 2021), we found that the inverse relative variance of qc, an index of horizontal homogeneity, generally increases from cloud base upward through the lower two-thirds of the cloud and then decreases in the uppermost one-third of the cloud. As a result, E decreases from cloud base upward and then increases towards the cloud top. We apply a decomposition analysis to the LES cloud water field to understand the relative roles of the mean and variances of qc in determining the vertical dependence of E. Our analysis reveals that the vertical dependence of the horizontal qc variability and enhancement factor E is a combined result of condensational growth throughout the lower portion of the cloud and entrainment mixing at cloud top. The findings of this study indicate that a vertically dependent E should be used in ESM autoconversion parameterizations.

54 ENVIRONMENTAL SCIENCES↗

Infiltrated electrodes for metal supported solid oxide electrolysis cells

Metal-supported solid oxide cells (MSOCs) are an alternative to conventional solid oxide cells (SOCs) based on ceramic cermets, offering lower material costs and higher operational flexibility. In this study symmetric MSOCs with infiltrated electrodes are explored for steam electrolysis operation to understand the underlying operation and degradation principles and suggest a direction for future MSOCs development. Two different fuel electrode backbones are used: an electronically-conductive lanthanum strontium co-doped iron nickel titanate (LSFNT) infiltrated with cerium-gadolinium oxide (CGO), or an ionic conductive zirconia based backbone (10ScYSZ) infiltrated with Ni:CGO. At the oxygen side, the backbone is 10ScYSZ, which is infiltrated with lanthanum-strontium co-doped cobalt oxide (LSC), or praseodymium oxide as cobalt-free alternative for comparison. This study suggests that the backbone electronic conductivity is key for good electrochemical performance as well as for boosting cell durability. Highly electronically conductive nanoparticles, especially nickel, were observed to irreversibly agglomerate driven by thermal conditions, whereas CGO proved to be a very stable electrocatalyst. At the fuel side, CGO (LSFNT) electrode showed lower ASR and degradation rate than Ni:CGO(ScYSZ) configuration with measured values of 0.50 Ω cm2 and 11 %/1000 h (at 0.60 A/cm2), and 0.70 Ω cm2 and 26 %/1000 h (at 0.50 A/cm2) at 1.30 V, respectively (700 °C, 50 % steam in hydrogen at the fuel side and air at the oxygen electrode side, LSC(ScYSZ) oxygen electrode).

25 ENERGY STORAGE↗

A finalized determinant for complete lignocellulose enzymatic saccharification potential to maximize bioethanol production in bioenergy Miscanthus

Miscanthus is a leading bioenergy crop with enormous lignocellulose production potential for biofuels and chemicals. However, lignocellulose recalcitrance leads to biomass process difficulty for an efficient bioethanol production. Hence, it becomes essential to identify the integrative impact of lignocellulose recalcitrant factors on cellulose accessibility for biomass enzymatic hydrolysis. In this study, we analyzed four typical pairs of Miscanthus accessions that showed distinct cell wall compositions and sorted out three major factors that affected biomass saccharification for maximum bioethanol production. Among the three optimal (i.e., liquid hot water, H 2 SO 4 and NaOH) pretreatments performed, mild alkali pretreatment (4% NaOH at 50 °C) led to almost complete biomass saccharification when 1% Tween-80 was co-supplied into enzymatic hydrolysis in the desirable Miscanthus accessions. Consequently, the highest bioethanol yields were obtained at 19% (% dry matter) from yeast fermentation, with much higher sugar–ethanol conversion rates by 94–98%, compared to the other Miscanthus species subjected to stronger pretreatments as reported in previous studies. By comparison, three optimized pretreatments distinctively extracted wall polymers and specifically altered polymer features and inter-linkage styles, but the alkali pretreatment caused much increased biomass porosity than that of the other pretreatments. Based on integrative analyses, excellent equations were generated to precisely estimate hexoses and ethanol yields under various pretreatments and a hypothetical model was proposed to outline an integrative impact on biomass saccharification and bioethanol production subjective to a predominate factor (CR stain) of biomass porosity and four additional minor factors (DY stain, cellulose DP, hemicellulose X/A, lignin G-monomer). Using four pairs of Miscanthus samples with distinct cell wall composition and varied biomass saccharification, this study has determined three main factors of lignocellulose recalcitrance that could be significantly reduced for much-increased biomass porosity upon optimal pretreatments. It has also established a novel standard that should be applicable to judge any types of biomass process technology for high biofuel production in distinct lignocellulose substrates. Hence, this study provides a potential strategy for precise genetic modification of lignocellulose in all bioenergy crops.

09 BIOMASS FUELS↗

The microbiome of a Pacific moon jellyfish Aurelia coerulea

The impact of microbiome in animal physiology is well appreciated, but characterization of animal-microbe symbiosis in marine environments remains a growing need. This study characterizes the microbial communities associated with the moon jellyfish Aurelia coerulea, first isolated from the East Pacific Ocean and has since been utilized as an experimental system. We find that the microbiome of this Pacific Aurelia culture is dominated by two taxa, a Mollicutes and Rickettsiales. The microbiome is stable across life stages, although composition varies. Mining the host sequencing data, we assembled the bacterial metagenome-assembled genomes (MAGs). The bacterial MAGs are highly reduced, and predict a high metabolic dependence on the host. Analysis using multiple metrics suggest that both bacteria are likely new species. We therefore propose the names Ca. Mariplasma lunae (Mollicutes) and Ca. Marinirickettsia aquamalans (Rickettsiales). Finally, comparison with studies of Aurelia from other geographical populations suggests the association with Ca. Mariplasma lunae occurs in Aurelia from multiple geographical locations. The low-diversity microbiome of Aurelia provides a relatively simple system to study host-microbe interactions.

59 BASIC BIOLOGICAL SCIENCES↗

Bonneville Dam Powerhouse 2 Gatewell Improvement Post Construction Evaluation (Final Report)

Modifications to vertical barrier screens (VBS) and the addition of concrete corbels to improve passage conditions for juvenile salmonids in the gatewells of Bonneville Dam’s second powerhouse (B2) were completed prior to the 2024 passage season. To evaluate the effectiveness of those modifications, PNNL carried out a post construction evaluation to contrast fish condition and mortality between two turbine unit operational ranges within the peak efficiency range. A block-treatment study design was implemented in 2024 to contrast descaling and mortality of juvenile salmonids sampled in the juvenile fish facility following exposure to turbine operations (middle versus upper 1% peak efficiency range) during spring and summer passage periods. In spring, 1.96% of juvenile salmonids sampled during mid-1% operations were descaled and 0.46% were mortalities. Of those sampled during upper 1% unit operations in spring, 2.90% were descaled and 0.95% were mortalities. Although these differences appeared to be meaningful, substantial exceedances of the upper 1% limit occurred during two treatment blocks of the spring study period. Fish collected during the upper 1% treatment of these two blocks experienced substantially higher rates of descaling and mortality compared to those collected during mid-1% treatments. Censoring these two upper 1% samples from the spring study period resulted in upper 1% descaling and mortality rates that were statistically similar to those from the mid-1% treatment. During the summer study period, 0.99% of juveniles sampled during mid-1% operations were descaled and 0.33% suffered mortality; these rates were significantly lower than the descaling (2.80%) and mortality (1.73%) rates observed during upper 1% treatments. Comparing the results from the 2024 study to those from the historical (2008–2013) baseline of unmodified units revealed that the descaling and mortality rates observed during upper 1% operations in spring 2024 were near the upper end of the historic range observed for mid-1% operations. Spring 2024 upper 1% descaling and mortality rates were below, or well below the median of historical mid and upper 1% (combined) rates, which suggests that the modifications have had a positive effect. Summer 2024 upper 1% descaling and mortality rates were at or above the top of the range of historical mid 1% and above or well above the median of historical mid and upper 1% (combined) rates. It is important to keep in mind that 2024 is a single year when considering these comparisons. Additional study could help confirm these results or seek a level of operation that achieves the desired outcomes for fish.

13 HYDRO ENERGY↗

Exclusive measurements of mean pion multiplicities in 4He-nucleus reactions from 200 to 800 MeV/nucleon

Mean multiplicities of pi+ and pi- in 4He collisions with C, Cu, and Pb at 200, 600, and 800 MeV/u, and with C and Pb at 400 MeV/u have been measured using the large solid angle detector Diogene. The independence of pion multiplicity on projectile incident energy, target mass and proton multiplicity is studied in comparison with intra-nuclear cascade predictions. The discrepancy between experimental results and theory is pointed out and discussed.

NASA Discipline Radiation Health↗

S-NPP and N20 VIIRS RSB Bands Detector-to-Detector Calibration Differences Assessment Using a Homogeneous Ground Target

The S-NPP and N20 satellites have successfully operated since their launches on October 28, 2011 and November 18, 2017, respectively. This paper provides an assessment of the detector calibration stability for the reflective solar bands (RSBs) observed from both S-NPP and N20 VIIRS. Top-of-atmosphere radiances from near-nadir observations over the homogeneous Libya 4 desert site are extracted from the S-NPP VIIRS Collection 1 and N20 Collection 2 Level-1B products. The radiances from individual detectors per Half‐angle Mirror side are studied. The comparisons of the normalized radiance to all detector average values indicate that the detector calibration differences are wavelength dependent. The S-NPP detector differences have been slowly increasing in the past 8.5 years and bands M1-M4 have 1.3%- 2.2% detector differences in 2019. N20 detector differences are stable and small in the past two years except SWIR M bands. N20 M10 and M11 have 1.3% and 2.1% detector differences, respectively. S-NPP DNB detector differences are about 0.8% and N20 DNB detector differences are about 0.5%. Most bands HAM side differences are less than 0.25% in the past years except N20 VIIRS M1 HAM side differences are 0.57% in 2018 and 0.54% in 2019. The Libya 4 images have small but noticeable striping in S-NPP M1-M4 data as well as in N20 M1, M8, M10, and M11 data. These study results have been applied in the S-NPP Collection 2 new algorithm to remove the detector differences. This research help scientists and VIIRS users better understand detector calibration differences in different version VIIRS products.

Libya 4↗

Residential agricultural pesticide exposures and risks of preeclampsia

Highlights: • Pesticides and preeclampsia have been rarely investigated. • Studied were >200,000 births and exposures to >500 pesticides. • There was a general lack of association between pesticide exposures and preeclampsia. • It is possible that unobserved early fetal loss may have biased risk estimates. We investigated risks of preeclampsia phenotypes from potential residential pesticide exposures, including 543 individual chemicals and 69 physicochemical groupings that were applied in the San Joaquin Valley of California during the study period, 1998–2011. The study population was derived from birth certificate data linked with Office of Statewide Health Planning and Development maternal and infant hospital discharge data. The following numbers of women with preeclampsia phenotypes were identified: 1045 with superimposed (pre-existing hypertension with preeclampsia) preeclampsia (265 with gestational weeks 20–31 and 780 with gestational weeks 32–36); 3471 with severe preeclampsia (824 with gestational weeks 20–31 and 2647 with gestational weeks 32–36); and 2780 with mild preeclampsia (207 with gestational weeks 20–31 and 2573 with gestational weeks 32–36). The reference population for these groups was 197,461 women who did not have diabetes (gestational or pre-existing), did not have any hypertensive disorder, and who delivered at 37 weeks or later. The frequency of any exposure was lower or about the same in each preeclampsia case group (further delineated by gestational age), and month time period, relative to the frequency in reference population controls. Nearly all odds ratios were below 1.0 for these any vs no exposure comparisons. This study showed a general lack of increased risks between a range of agriculture pesticide exposures near women's residences and various preeclampsia phenotypes.

60 APPLIED LIFE SCIENCES↗

Performance of traffic-alert collision avoidance (TCAS) antennas in the presence of scatterers

The performance of two TCAS systems is studied in the presence of electromagnetic scatterers. TCAS is an aircraft mounted angle of arrival (AOA) system, which estimates the bearing of a signal transmitted from a mode-S transponder on another nearby aircraft (intruder). Two systems are studied: (1) Comparison of Relative Amplitude system (CRA), and (2) Spiral Phase Antenna (SPA). The CRA antenna receives the reply via four switched beams. The bearing is estimated by comparing the amplitudes of the received signal. The SPA is based on the phase interferometer, which utilizes the received phase via sum and difference beams. The AOA is computed by comparing the reply with similar values on a calibration table, which is generated by modeling the TCAS antenna on the bare fuselage of a Boeing 727-200. The antenna patterns for the TCAS are found via high frequency methods based on the Uniform Geometric theory of Diffraction (UTD). By minimizing the standard deviation of the bearing error in a specified angular sector, optimal locations for top and bottom mounted TCAS antennas are found on the Boeing 727-200, 737-300 and 747-200 airframes. It will be shown that the overall bearing errors of the amplitude system are consistently smaller than the spiral phase TCAS. The effect of two types of nearby scatterers--antennas, and engine inlets--is studied. The AT741 L-band blade, DMC60-1 VHF Communication antenna were chosen as being representative antenna interference examples. Models are derived for the blades via a moment method analysis followed by a least squares procedure to synthesize the scattering patterns. Studies were conducted to estimate the minimum separation between the two antennas for acceptable operation. It will be shown that the spiral phase TCAS is adversely affected by the presence of a blade antenna. The amplitude system does not suffer from this limitation, especially for the forward look angles which are of most interest here. A model to represent the inlet scattering is based on the multiple scattering method and UTD. The engine on top of the B727-200 fuselage is modeled by a terminated circular waveguide. Then, the effect of moving the antenna forward on the fuselage is studied. It is again shown that the performance of the amplitude system is superior.

Sampath, K. S.↗

Quantifying Climate Change Effects of Bioenergy and BECCS: Critical Considerations and Guidance on Methodology

Bioenergy is a critical element in many national and international climate change mitigation efforts, including as a carbon dioxide removal strategy combined with the capture and durable geological storage of flue gas emissions (BECCS). However, divergent results on the effectiveness of bioenergy as a climate change mitigation measure are reported in the scientific literature. Climate impacts of bioenergy depend on case-specific factors, primarily biophysical features of the biomass production system, and the design and efficiency of conversion and capture processes. Estimates of climate impacts are also strongly affected by methodological choices and assumptions, and much of the divergence between studies derives from differences in the assumed alternate use of the land or feedstock, the alternate energy source and the system boundaries applied. We present a methodology to support robust estimates of the climate change effects of bioenergy systems, updating the standard methodology developed by the International Energy Agency's Technology Collaboration Program on Bioenergy. We provide guidance on the key choices including the reference land use and energy system that bioenergy is assumed to displace, spatial and temporal system boundaries, co-product handling, climate forcers considered, metrics applied and time horizon of impact assessment. Researchers should consider the whole bioenergy system including all life cycle stages, and choose system boundaries, reference systems and treatment of co-products that are consistent with the intended application of the results. The assessment should be normalised to a functional unit that can be compared with other systems delivering an equivalent quantity of the same function. All significant climate forcers should be included, and climate effects should be quantified using appropriate impact assessment methods that distinguish the impact of time. Consistency in methodology and interpretation will facilitate comparison between studies of different bioenergy systems.

09 BIOMASS FUELS↗

Spreading Characteristics and Thrust of Jets from Asymmetric Nozzles

The spreading characteristics of jets from several asymmetric nozzles are studied in comparison to those of an axisymmetric jet, over the Mach number (M(sub J)) range of 0.3 to 1.96. The effect of tabs in two cases, the axisymmetric nozzle fitted with four tabs and a rectangular nozzle fitted with two large tabs, is also included in the comparison. Compared to the axisymmetric jet, the asymmetric jets spread only slightly faster at subsonic conditions, while at supersonic conditions, when screech occurs, they spread much faster. Screech profoundly increases the spreading of all jets. The effect varies in the different stages of screech, and the corresponding unsteady flowfield characteristics are documented via phase-averaged measurement of the fluctuating total pressure. An organization and intensification of the azimuthal vortical structures under the screeching condition is believed to be responsible for the increased spreading. Curiously, the jet from a 'lobed mixer' nozzle spreads much less at supersonic conditions compared to all other cases. This is due to the absence of screech with this nozzle. Jet spreading for the two tab configurations, on the other hand, is significantly more than any of the no-tab cases. This is true in the subsonic regime, as well as in the supersonic regime in spite of the fact that screech is essentially eliminated by the tabs. The dynamics of the streamwise vortex pairs produced by the tabs cause the most efficient jet spreading thus far observed in the study.

Zaman, K. B. M. Q.↗

Estimation of Thermodynamic and Dynamic Contributions to Sea Ice Growth in the Central Arctic Using ICESat-2 and MOSAiC SIMBA Buoy Data

The fine spatial resolution of the ICESat-2 (IS2) satellite altimeter allows monitoring the evolution of sea ice thickness with detailed dynamic information (e.g. ridges and leads). In this study, we first assess the ability of IS2 to estimate thermodynamic ice growth and dynamic thickening during the ice-growing season in the central Arctic Ocean. As an indicator of the thermodynamic ice growth, we use 10 thermistor string-based sea ice mass balance array (SIMBA) buoys deployed at a scale of ~ 50 km from the Icebreaker Polarstern during the Multidisciplinary drifting Observatory for the Study of Arctic Climate (MOSAiC) expedition. We collect IS2 data within 20 km buffer distance from the individual buoys, and calculate the mode, median, and mean of the IS2-derived ice thickness. The IS2 modal thickness shows the least bias (−0.169 m) with the buoy ice thickness, representing level ice thickness. In addition, the increasing rate of the IS2 modal thickness is close to the thermodynamic ice growth with a small bias of −0.054 cm/day. However, the increasing rates of the IS2 median and mean thickness are greater than the thermodynamic ice growth by about 0.114 cm/day and 0.198 cm/day, respectively, because they also include ice growth caused by thickness redistribution during dynamic deformation. The dynamic contributions may account for 26.1 ± 10.3% and 34.4 ± 10.1% of the total increase of the IS2 median and mean thickness, respectively. Within a ~ 50 km radius area from the MOSAiC Central Observatory, IS2 measurements exhibit that the ridge fraction increased from <2% in November to ~ 4% in March (~0.029%/day of average increasing rate) and ridge height increased about 0.047 cm/day during the same period. However, lead formation does not show significant contributions to the dynamic ice thickening because leads are temporary features lasting only 2–3 days. Although there are considerable uncertainties in IS2 ice thickness estimation and IS2-buoy thickness comparison, this study emphasizes the importance of combining measurements by IS2 and SIMBA buoys to explain the regional sea ice mass balance with separating the thermodynamic and dynamic contributions.

satellite altimeter↗

Stability analysis and trend study of a balloon tethered in a wind, with experimental comparisons

A stability analysis and trend study for a balloon tethered in a steady wind are presented. The linearized, stability-derivative type analysis includes balloon aerodynamics, buoyancy, mass (including apparent mass), and static forces resulting from the tether cable. The analysis has been applied to a balloon 7.64 m in length, and the results are compared with those from tow tests of this balloon. This comparison shows that the analysis gives reasonable predictions for the damping, frequencies, modes of motion, and stability boundaries exhibited by the balloon. A trend study for the 7.64-m balloon was made to illustrate how the stability boundaries are affected by changes in individual stability parameters. The trends indicated in this study may also be applicable to many other tethered-balloon systems.

Redd, L. T.↗

Eddy Current Probe Parameters Identification Using a Genetic Algorithm and Simultaneous Perturbation Stochastic Approximation

This study tries to identify the coil parameters using numerical methods. The eddy current testing (ECT) is used for evaluation of a crack with the aid of numerical simulations by utilizing the identification of these parameters. In this study, a comparison of the performance of the GA and SPSA algorithms to identify the parameter values of the coil sensors are presented. So, the optimization probe geometry is introduced in the simulation with Three-dimensional finite element simulations (FLUX finite element code) were conducted to obtain eddy current signals resulting from a crack in a plate made of aluminium. The simulation results are compared with experimental measurements for the defect present in a plate.

42 ENGINEERING↗

Highly sensitive SPR PCF biosensors based on Ag/TiN and Ag/ZrN configurations

We numerically present and analyze a surface plasmon resonance (SPR) bimetallic photonic crystal fiber (PCF) biosensor using full vectorial finite element method. The bimetallic configuration is based on Silver and (TiN or ZrN) as alternative plasmonic materials. The reported design relies on PCF with an external channel to house the analyte. The inner surface of the channel is coated by a silver layer followed by TiN or ZrN to protect the silver layer from oxidation. The proposed biosensor can be implemented to detect the unknown analytes, organic chemicals, biological analytes, and biomolecules via the sensitive resonant peaks to the analyte refractive index variations for both polarized modes with high linearity. In this study, a comparison is made between the Ag/TiN configuration and the Ag/ZrN counterpart in terms of sensitivity, losses, and linearity. The geometrical parameters are optimized to achieve high refractive index sensitivities of 7000 nm/RIU for quasi-transverse electric (TE) mode and 6900 nm/RIU for quasi-transverse magnetic (TM) mode, respectively for the Ag/TiN configuration. However, the quasi TE and quasi TM modes achieve high sensitivity of 5300 and 5400 nm/RIU, respectively using the Ag/ZrN configuration. The standard PCF fabrication technologies can be used to fabricate the proposed SPR PCF biosensors.

36 MATERIALS SCIENCE↗

In Situ Neutron Diffraction Study of the Influence of Microstructure on the Mechanical Response of Additively Manufactured 304L Stainless Steel

In situ neutron diffraction measurements were completed for this study during tensile and compressive deformation of stainless steel 304L additively manufactured (AM) using a high power directed energy deposition process. Traditionally produced wrought 304L material was also studied for comparison. The AM material exhibited roughly 200 MPa higher flow stress relative to the wrought material. Crystallite size, crystallographic texture, dislocation density, and lattice strains were all characterized to understand the differences in the macroscopic mechanical behavior. The AM material’s initial dislocation density was about 10 times that of the wrought material, and the flow strength of both materials obeyed the Taylor equation, indicating that the AM material’s increased yield strength was primarily due to greater dislocation density. Finally, a ~50 MPa flow strength tension/compression asymmetry was observed in the AM material, and several potential causes were examined.

36 MATERIALS SCIENCE↗

Performance of Nd-Fe-B Magnets Fabricated by Hot Isostatic Pressing and Low-Temperature Sintering

Magnetic properties and microstructure of Nd-Fe-B sintered magnets fabricated by hot isostatic pressing (HIP) were studied. For comparison, magnets were also fabricated by vacuum sintering. The density reached 7.58 g/cm{sup 3} for the magnets HIP-sintered at 1123 K. The density of the magnets vacuum-sintered at 1123 K was much lower, which is of about 6.92 g/cm{sup 3}. While the density of magnets vacuum-sintered at 1318 K was the same as the HIP-sintered magnets, the sintering temperature was significantly decreased to 1123 K. In addition, the average grain size decreased from 9 to 6 μm, which has enhanced coercivity. Therefore, the coercivity increased from 1067.7 to 1238.5 kA/m, which is 16% higher than the vacuum-sintered magnets. HIP is a promising method to obtain high density and high coercivity Nd-Fe-B sintered magnets.

36 MATERIALS SCIENCE↗