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At least 433 records · Page 24

Thermal environment effects on strength and impact properties of boron-aluminum composites

A systematic study was conducted regarding the degradation of fracture strength and impact energy in commercial B-Al composites in both static and cyclic thermal environments. The composites used in the study contained approximately 50 vol % boron fibers, unidirectionally aligned in either a 6061 Al or 1100 Al matrix. The tensile strengths of the composites after 3000 thermal cycles as a function of upper cycle temperature are presented in graphs. The temperature at which the strengths of 6061 Al matrix, B-Al composites were significantly degraded after 3000 cycles was noticeably higher than that for the 1100 Al matrix composites. Static heating at 420 C resulted in no significant strength degradation for the 6061 Al matrix composites. In the case of 1100 matrix composites, some degradation was observed at 420 C but markedly less than in the composites cycled to 420 C.

Grimes, H. H.↗

Exploration of Failure and Potential Damage Markers in Ti-6Al-4V

To improve prognostics for predicting component life, coupon tests were conducted on Ti-6Al-4V to investigate the development of damage. Various test types were employed (tension, creep, stress relaxation, and fatigue) under a wide range of temperatures and loading rates to engage various amounts of time-dependent and damage behavior. Both stiffness degradation and Poisson’s ratio were monitored to see if they were useful in indicating the initiation and accumulation of damage and subsequently the onset of failure. Stiffness exhibited large decreases with increasing strain when calculated using engineering stress and strain. However, minimal stiffness change was observed when using the true-stress and true- strain values. Detailed microscopy and image analysis were performed to document the actual physical damage that occurred within the various specimens. Two types of damage were observed: shallow surface cracks and internal pores. The severity of damage was greater in the region of localized necking and diminished further away from the neck. The area fraction of pores was higher in the necked region, yet even there it did not exceed more than a few percent and, in most cases, was significantly lower. It was observed that conditions that induced more time-dependent deformation (e.g., slower strain rate testing) resulted in a larger number of pores and larger pore sizes. The pores were always found to occur in the softer β-phase. The severity of observed damage was inconsistent with the large drop in engineering stiffness, but was more aligned with stiffness changes from the true-stress and -strain values. Poisson’s ratio was monitored on every test and showed promise as a damage indicator. It was found to be more sensitive than either the ultimate tensile strength or the inception of tertiary creep. However, calculation of Poisson’s ratio was found to be more involved than expected because of anisotropy and the presence of strain gradients along the specimen at large applied strains. First, the material had a moderate texture and resulted in anisotropy of the strains. Second, the evolution of Poisson’s ratio as a function of axial strain showed strange and unexpected behaviors, which necessitated more extensive analyses of its development. This led to an investigation on the use of small versus large strain approaches and the importance of making consistent measurements; that is, axial and transverse strain measurements over the same volume of material. Additionally, finite element analysis of a tensile sample indicated that non- uniform strain occurred in the sample prior to attaining the maximum strength. This, along with the location at which transverse strain was measured, had a significant influence on the resulting values of Poisson’s ratio. Based on this, lessons learned are offered for future testing.

Ti-6Al-4V↗

Direction of crack growth in fibrous composites

A model for predicting the direction of crack growth in resin matrix composite materials is presented. The model is based upon the normal stress and the anisotropic tensile strength on arbitrary planes about the tip of a crack. The model is incorporated into a finite element solution which predicts energy release rates in addition to the direction of crack growth. Results are obtained for cracks in unidirectional off-axis slotted tensile coupons. Comparisons are made with other theories and experimental results.

Buczek, M. B.↗

Status of High-Strength Nanotube Composites at Johnson Space Center

Single-wall carbon nanotubes offer extraordinary mechanical properties that could start a revolution in materials science. The combination of very high strength and modulus with high strain to failure makes nanotubes an ideal fiber for strengthening in composites. Because of the scale of these fibers, new challenges exist for processing of composite materials and materials characterization. Our project includes aspects of nanotube materials from production and characterization to purification and incorporation into composites for mechanical testing. Early results show that some new techniques will be necessary for the strength of single wall nanotubes to be fully utilized. Current research at JSC focuses on structural polymeric materials to attempt to lower the weight of spacecraft necessary for interplanetary missions. Studies show good nanotube dispersion and wetting by the epoxy materials. Results of tensile strength tests will also be reported. This presentation will focus on current research into polymer nanotube composites and the next steps toward this revolution in aerospace materials.

Files, Bradley S.↗

Laser Machining of Melt Infiltrated Ceramic Matrix Composite

As interest grows in considering the use of ceramic matrix composites for critical components, the effects of different machining techniques, and the resulting machined surfaces, on strength need to be understood. This work presents the characterization of a Melt Infiltrated SiC/SiC composite material system machined by different methods. While a range of machining approaches were initially considered, only diamond grinding and laser machining were investigated on a series of tensile coupons. The coupons were tested for residual tensile strength, after a stressed steam exposure cycle. The data clearly differentiated the laser machined coupons as having better capability for the samples tested. These results, along with micro-structural characterization, will be presented.

Jarmon, D. C.↗

Properties of splat-quenched 7075 aluminum type alloys

The 7075 alloy belonging to the Al-Zn-Mg-Cu system, prepared by powder metallurgy techniques, was used in a study of alloys prepared from splat-quenched foils consolidated into bar material by hot extrusion. Ni and Fe were included in one alloy specimen, producing a fine dispersion of FeAl3 type particles which added to the strength of the aged alloy but did not coarsen upon heat treatment. Fine oxide films showing up on air-splatted foils induce finely dispersed oxide stringers (if the foils are not hot-worked subsequently) which in turn promote axial cracking (but longitudinal tensile strength is not seriously impaired). Splatting in a protective atmosphere, or thermomechanical processing, is recommended to compensate for this.

Durand, J. P. H. A.↗

Modeling the Thermostructural Stability of Melt-infiltrated Sic/sic Composites

SiC/SiC composites developed by NASA with Sylramic-iBN fibers and melt-infiltrated (MI) SiC-Si matrices have demonstrated 1000-hour rupture life in air at 100 MPa and 1315OC. Recently it has been determined that a major factor controlling the long-term rupture life of these composites is not environment or stress, but an intrinsic microstructural and strength instability caused by a thermally-induced silicon attack of the Sic fibers. The objective of this paper is to present a simple diffusion-based analytical model which predicts well the observed effects of stress-free thermal exposure on the residual tensile strength of Sylramic-iBN/SiC-Si composites. The practical implications of the model for SiC/SiC composites with MI matrices are discussed.

DiCarlo, James A.↗

Fatigue Damage in Notched Composite Laminates Under Tension-Tension Cyclic Loads

The results are given of an investigation to determine the damage states which develop in graphite epoxy laminates with center holes due to tension-tension cyclic loads, to determine the influence of stacking sequence on the initiation and interaction of damage modes and the process of damage development, and to establish the relationships between the damage states and the strength, stiffness, and life of the laminates. Two quasi-isotropic laminates were selected to give different distributions of interlaminar stresses around the hole. The laminates were tested under cyclic loads (R=0.1, 10 Hz) at maximum stresses ranging between 60 and 95 percent of the notched tensile strength.

Stinchcomb, W. W.↗

Progress toward a tungsten alloy wire/high temperature alloy composite turbine blade

A tungsten alloy wire reinforced high temperature alloy composite is being developed for potential application as a hollow turbine blade for advanced rocket engine turbopumps. The W-24Re-HfC alloy wire used for these composite blades provides an excellent balance of strength and wire ductility. Preliminary fabrication, specimen design, and characterization studies were conducted by using commercially available W218 tungsten wire in place of the W-24Re-Hfc wire. Subsequently, two-ply, 50 vol pct composite panels using the W-24Re-HfC wire were fabricated. Tensile tests and metallographic studies were performed to determine the material viability. Tensile strengths of a Waspaloy matrix composite at 870 C were 90 pct of the value expected from rule-of-mixtures calculations. During processing of this Waspaloy matrix composite, a brittle phase was formed at the wire/matrix interface. Circumferential wire cracks were found in this phase. Wire coating and process evaluation efforts were performed in an attempt to solve the reaction problem. Although problems were encountered in this study, wire reinforced high temperature alloy composites continue to show promise for turbopump turbine blade material improvement.

Ritzert, F. J.↗

Elevated temperature tensile and creep behavior of a SiC fiber-reinforced titanium metal matrix composite

In this research program, the tensile properties and creep behavior in air of (0)(sub 4), (0/90)(sub s) and (90)(sub 4) SCS-9/Beta 21S composite layups with 0.24 volume fraction fiber were evaluated. Monotonic tensile tests at 23, 482, 650 and 815 C yielded the temperature dependence of the elastic modulus, proportional limit, ultimate tensile strength and total strain at failure. At 650 C, the UTS of the (0)(sub 4) and (0/90)(sub s) layups decreases by almost 50 percent from the room temperature values, indicating that operating temperatures should be less than 650 C to take advantage of the specific tensile properties of these composites.

Thurston, Rita J.↗

Weldability of Weldalite (tm) 049 with and without TiB2 reinforcement

The effects are assessed of TiB2 reinforcement and parent alloy Li content on the weldability of Weldalite (tm) 049 type alloys. Welding trials were performed using either AC or DC polarity gas tungsten arc (GTA) welding according to described procedures. The welding was performed under conditions of high restraint on 5 cm (2 in) wide x 25.4 cm (10 in) long plates machined from the 0.952 cm (0.375 in) extruded bar parallel to the extrusion direction. A 37.5 deg bevel was machined on the center edge of the extruded bar. Cut rod filler wire was machined from three alloys, and one commercially available 2319 filler wire was also used. The preliminary assessment of the weldability revealed no propensity for hot cracking under conditions of high restraint. This result is significant, because hot cracking has been reported for all other leading aluminum lithium alloys welded with certain conventional filler alloys. The strengths for Weldalite parent welded with parent filler obtained were higher than those for alloys used in launch systems, such as 2219 and 2014 welded with 2319 and 4043 fillers, respectively. Even higher values were obtained by variable polarity plasma arc welding (e.g., 54 ksi (372 MPa) mean tensile strength).

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Laser Heated Oxide Fiber Growth Using Melt Modulation Technique

As a reinforcement for structural composites, single crystal alumina fibers offer low density, high modulus, and high creep resistance. In this study, the laser heated float zone approach was employed to grow c-axis Al2O3 continuous fibers of high purity and high strength. A new melt modulation technique, laser scanning, avoids the formation of surface induced ripples and allows the growth of 50 micro-m diameter sapphire fibers with strengths (approx. 7 GPa) significantly greater than either commercially available fibers grown by the edge-defined film growth process (approx. 2-3 GPa) or laboratory fibers grown by stationary laser heating (approx. 5 GPa). The present work suggests that surface striations are the predominant defects controlling the tensile strength of laser-scanned fibers at room temperature. Several possible mechanisms for inducing surface striations are systematically discussed for several oxide fiber compositions.

Sayir, Ali↗

Life Modeling and Design Analysis for Ceramic Matrix Composite Materials

The primary research efforts focused on characterizing and modeling static failure, environmental durability, and creep-rupture behavior of two classes of ceramic matrix composites (CMC), silicon carbide fibers in a silicon carbide matrix (SiC/SiC) and carbon fibers in a silicon carbide matrix (C/SiC). An engineering life prediction model (Probabilistic Residual Strength model) has been developed specifically for CMCs. The model uses residual strength as the damage metric for evaluating remaining life and is posed probabilistically in order to account for the stochastic nature of the material s response. In support of the modeling effort, extensive testing of C/SiC in partial pressures of oxygen has been performed. This includes creep testing, tensile testing, half life and residual tensile strength testing. C/SiC is proposed for airframe and propulsion applications in advanced reusable launch vehicles. Figures 1 and 2 illustrate the models predictive capabilities as well as the manner in which experimental tests are being selected in such a manner as to ensure sufficient data is available to aid in model validation.

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Tensile Properties of Some Structural Sheet Materials Under Rapid-Heating Conditions

The results of the NACA tests to determine the tensile strength of some structural sheet materials heated to failure at temperature rates from 0.2 deg. F to 100 deg F per second under constant load conditions are reviewed . Yield and rupture stresses obtained under rapid-heating conditions are compared with the results of conventional elevated-temperature tensile tests. The relation between rapid-heating tests, short-time creep tests, and conventional creep tests is discussed . The application of a phenomenological theory for calculating rapid-heating curves is shown. Methods are given for predicting yield and rupture stresses and temperatures from master curves and temperature-rate parameters

Heimerl, George J.↗

Effect of Cristobalite on the Mechanical Properties of Silica RSI Materials

The strength of various silica surface insulation materials was measured after high temperature heat treatment to develop substantial crystalline phases, and after low temperature thermal cycling through the alpha-beta cristobalite transformation. It appears that the presence of cristobalite in the structural elements (the fibers) is highly detrimental to tensile strength. When crystallization does not occur in silica material, the strength improves with heat treatment.

Khandelwal, P. K.↗

Identification of strengthening phases in Al-Cu-Li alloy Weldalite (tm) 049

Microstructure property relationships were determined for a family of ultrahigh strength weldable Al-Cu-Li based alloys referred to as Weldalite (tm) alloys. The highest strength variant of this family, Weldalite 049, has a high Cu/Li wt pct. ratio with a nominal composition of Al-6.3Cu-1.3Li-0.4Ag-0.4Mg-0.14Zr. Increasing the alloy's lithium content above 1.3 wt pct. resulted in a decrease in both yield and ultimate tensile strength. Strength was shown to be strongly dependent on lithium content, with a maximum in strength occurring in the range of about 1.1 to 1.4 wt pct. lithium. The strengthening phases present in Weldalite 049 (1.3Li) and an Al-6.3Cu-1.9Li-0.4Mg-0.14Zr alloy were identified using transmission electron microscopy (TEM).

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Thermal barrier coating life prediction model

This is the first report of the first phase of a 3-year program. Its objectives are to determine the predominant modes of degradation of a plasma sprayed thermal barrier coating system, then to develop and verify life prediction models accounting for these degradation modes. The first task (Task I) is to determine the major failure mechanisms. Presently, bond coat oxidation and bond coat creep are being evaluated as potential TBC failure mechanisms. The baseline TBC system consists of an air plasma sprayed ZrO2-Y2O3 top coat, a low pressure plasma sprayed NiCrAlY bond coat, and a Rene'80 substrate. Pre-exposures in air and argon combined with thermal cycle tests in air and argon are being utilized to evaluate bond coat oxidation as a failure mechanism. Unexpectedly, the specimens pre-exposed in argon failed before the specimens pre-exposed in air in subsequent thermal cycles testing in air. Four bond coats with different creep strengths are being utilized to evaluate the effect of bond coat creep on TBC degradation. These bond coats received an aluminide overcoat prior to application of the top coat to reduce the differences in bond coat oxidation behavior. Thermal cycle testing has been initiated. Methods have been selected for measuring tensile strength, Poisson's ratio, dynamic modulus and coefficient of thermal expansion both of the bond coat and top coat layers.

Hillery, R. V.↗

Predicting the time-temperature dependent axial failure of B/A1 composites

Experimental and theoretical studies were conducted in order to understand and predict the effects of time, temperature, and stress on the axial failure modes of boron fibers and B/A1 composites. Due to the anelastic nature of boron fiber deformation, it was possible to determine simple creep functions which can be employed to accurately describe creep and fracture stress of as-produced fibers. Analysis of damping and strength data for B/6061 A1 composites indicates that fiber creep effects of creep on fiber fracture are measurably reduced by the composite fabrication process. The creep function appropriate for fibers with B/Al composites was also determined. A fracture theory is presented for predicting the time-temperature dependence of the axial tensile strength for metal matrix composites in general and B/A1 composites in particular.

Dicarlo, J. A.↗