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At least 433 records · Page 24

Research study on materials processing in space experiment M512

A study program was conducted to clarify the role of gravity in the fluid mechanics of certain molten metal processes of potential significance to manufacturing in space. In particular, analyses were conducted of the M551 Metals Melting Experiment and the M553 Sphere Forming Experiment to be conducted in the M512 Facility onboard Skylab. The M551 experiment consisted of a study of electron beam welding of various metals, and the M553 experiment studied the formation of molten metal spheres by free-floating in a near zero-gravity environment. The analyses of these experiments and a comparison with ground-based and KC135 experimental results are presented.

Brashears, M. R.↗

Research study on materials processing in space experiment number M512

Conclusions of the team of specialists can be generalized as: (1) Brazing and welding of metal structures in an orbital near zero gravity condition are quite feasible. (2) Design of joints for fabrication in zero gravity will place less emphasis on the tolerances and proximity of the adjacent structures than on the quantity of liquid metal available. (3) Brazing of metallic joints has many advantages over electron beam welding for practical reasons: simplicity, launch weight, development costs, joint design tolerances, remotization, etc. (4) No evidence of different physical or mechanical properties of liquid metals in zero gravity was observed. However, many differences in liquid behavior were observed. Many of these effects have been called adhesion-cohesion phenomena.

Tobin, J. M.↗

Research study on materials processing in space experiment number M512

Adhesion of the melted metals to the adjacent solid metals, and cohesion of the liquid metal to itself appeared to be equally as strong in zero gravity as on earth. Similar cut edge bead periodicity in cut thin plate, and similar periodic chevron patterns in full penetration welds were seen. The most significant practical result is that the design of braze joints for near zero gravity can be very tolerant of dimensional gaps in the joint. This conclusion is based on a comparison of narrow, wide and variable gap widths. Brazing is very practical as a joining or repairing technique for metal structures at zero gravity. The operation of the hardware developed to locate successive small (0.6 cm) diameter cylinders in the focus of the battery powered EB unit, melt the various metal specimens and deploy some liquid metal drops to drift in space, was generally successful. However, the sphericity and surface roughness were far from those of ball bearings.

Tobin, J. M.↗

Flat-plate collector research area: Silicon material task

Silane decomposition in a fluidized-bed reactor (FBR) process development unit (PDU) to make semiconductor-grade Si is reviewed. The PDU was modified by installation of a new heating system to provide the required temperature profile and better control, and testing was resumed. A process for making trichlorosilane by the hydrochlorination of metallurgical-grade Si and silicon tetrachloride is reported. Fabrication and installation of the test system employing a new 2-in.-dia reactor was completed. A process that converts trichlorosilane to dichlorosilane (DCS), which is reduced by hydrogen to make Si by a chemical vapor deposition step in a Siemens-type reactor is described. Testing of the DCS PDU integraled with Si deposition reactors continued. Experiments in a 2-in.-dia reactor to define the operating window and to investigate the Si deposition kinetics were completed.

Lutwack, R.↗

Fatigue and fracture research in composite materials

The fatigue, fracture, and impact behavior of composite materials are investigated. Bolted and bonded joints are included. The solutions developed are generic in scope and are useful for a wide variety of structural applications. The analytical tools developed are used to demonstrate the damage tolerance, impact resistance, and useful fatigue life of structural composite components. Standard tests for screening improvements in materials and constituents are developed.

T. Kevin O'Brien↗

Safety research of insulating materials of cable for nuclear power generating station

The polymers PE, EPR, PVC, Neoprene, CSP, CLPE, EP and other similar substances are frequently used as insulation and protective covering for cables used in nuclear power generating stations. In order to test these materials for flame retardation, environmental resistance, and cable specifications, they were given the cable normal test, flame test, chemical tests, and subjected to design analysis and loss of coolant accident tests. Material was collected on spark tests and actual experience standards were established through these contributions and technology was accumulated.

Lee, C. K.↗

NDE of ceramics and ceramic composites

Although nondestructive evaluation (NDE) techniques for ceramics are fairly well developed, they are difficult to apply in many cases for high probability detection of the minute flaws that can cause failure in monolithic ceramics. Conventional NDE techniques are available for monolithic and fiber reinforced ceramic matrix composites, but more exact quantitative techniques needed are still being investigated and developed. Needs range from flaw detection to below 100 micron levels in monolithic ceramics to global imaging of fiber architecture and matrix densification anomalies in ceramic composites. NDE techniques that will ultimately be applicable to production and quality control of ceramic structures are still emerging from the lab. Needs are different depending on the processing stage, fabrication method, and nature of the finished product. NDE techniques are being developed in concert with materials processing research where they can provide feedback information to processing development and quality improvement. NDE techniques also serve as research tools for materials characterization and for understanding failure processes, e.g., during thermomechanical testing.

Vary, Alex↗

NDE of ceramics and ceramic composites

Although nondestructive evaluation (NDE) techniques for ceramics are fairly well developed, they are difficult to apply in many cases for high probability detection of the minute flaws that can cause failure in monolithic ceramics. Conventional NDE techniques are available for monolithic and fiber reinforced ceramic matrix composites, but more exact quantitative techniques needed are still being investigated and developed. Needs range from flaw detection to below 100 micron levels in monolithic ceramics to global imaging of fiber architecture and matrix densification anomalies in ceramic composites. NDE techniques that will ultimately be applicable to production and quality control of ceramic structures are still emerging from the lab. Needs are different depending on the processing stage, fabrication method, and nature of the finished product. NDE techniques are being developed in concert with materials processing research where they can provide feedback information to processing development and quality improvement. NDE techniques also serve as research tools for materials characterization and for understanding failure processes, e.g., during thermomechanical testing.

Vary, Alex A.↗

Ground based research in microgravity materials processing

The core activities performed during this time period have been concerned with tracking the TEMPEST experiments on the shuttle with drops of Zr, Ni, and Nb alloys. In particular a lot of Zr drops are being made to better define the recalescence characteristics of that system so that accurate comparisons of the drop tube results with Tempest can be made. A new liner, with minimal reflectivity characteristics, has been inserted into the drop tube in order to improve the recalescence measurements of the falling drops. The first installation to make the geometric measurements to ensure a proper fit has been made. The stovepipe sections are currently in the shop at MSFC being painted with low reflectivity black paint. Work has also continued on setting up the MEL apparatus obtained from Oak Ridge in the down stairs laboratory at the Drop Tube Facilities. Some ground-based experiments on the same metals as are being processed on TEMPEST are planned for the MEL. The flight schedules for the KC-135 experiments are still to be determined in the near future.

Workman, Gary L.↗

Cryogenic Thermal Performance Testing of Bulk-Fill and Aerogel Insulation Materials

The research testing and demonstration of new bulk-fill materials for cryogenic thermal insulation systems was performed by the Cryogenics Test Laboratory at NASA Kennedy Space Center. Thermal conductivity testing under actual-use cryogenic conditions is a key to understanding the total system performance encompassing engineering, economics, and materials factors. A number of bulk fill insulation materials, including aerogel beads, glass bubbles, and perlite powder, were tested using a new cylindrical cryostat. Boundary temperatures for the liquid nitrogen boil-off method were 293 K and 78 K. Tests were performed as a function of cold vacuum pressure from high vacuum to no vacuum conditions. Results are compared with other complementary test methods in the range of 300 K to 20 K. Various testing techniques are shown to be required to obtain a complete understanding of the operating performance of a material and to provide data for answers to design engineering questions.

Scholtens, B. E.↗

Smart Materials and Structures Applications at the NASA Langley Research Center

This overview of the presentation covers Langley's smart materials infrastructure, materials research, applications, and summary. Langley's infrastructure consists of fabrication and characterization of smart structures. Materials researched include ceramics, polymers, and polymer-ceramic composites. Applications include interior aircraft noise suppression, aircraft engine noise reduction, active flutter damping of aircraft wings for better performance, active shape control of polymeric reflectors, and aircraft wing distortion to eliminate control surfaces.

Horner, Garnett↗