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At least 433 records · Page 24

Automation and Upgrade of Thermal System for Large 38-Year-Young Test Facility

The Goddard Space Flight Center's Space Environment Simulator (SES) facility has been improved by the upgrade of its thermal control hardware and software. This paper describes the preliminary design process, funding constraints, and the proposed enhancements as well as the installation details, the testing difficulties, and the overall benefits realized from this upgrade. The preliminary design process was discussed in a paper presented in October 1996 and will be recapped in this paper to provide background and comparison to actual product. Structuring the procurement process to match the funding constraints allowed Goddard to enhance its capabilities in an environment of reduced budgets. The installation of the new system into a location that has been occupied for over 38 years was one of the driving design factors for the size of the equipment. The installation was completed on time and under budget. The tuning of the automatic sequences for the new thermal system to the existing shroud system required more time and ultimately presented some setbacks to the vendor and the final completion of the system. However, the end product and its benefits to Goddard's thermal vacuum test portfolio will carry the usefulness of this facility well into the next century.

Webb, Andrew T.↗

Automation and Upgrade of Thermal System for Large 38-Year Young Test Facility

The Goddard Space Flight Center's Space Environment Simulator (SES) facility has been improved by the upgrade of its thermal control hardware and software. This paper describes the preliminary design process, funding constraints, and the proposed enhancements as well as the installation details, the testing difficulties, and the overall benefits realized from this upgrade. The preliminary design process was discussed in a paper presented in October 1996 and will be recapped in this paper to provide background and comparison to actual product. Structuring the procurement process to match the funding constraints allowed Goddard to enhance its capabilities in an environment of reduced budgets. The installation of the new system into a location that has been occupied for over 38-years was one of the driving design factors for the size of the equipment. The installation was completed on-time and under budget. The tuning of the automatic sequences for the new thermal system to the existing shroud system required more time and ultimately presented some setbacks to the vendor and the final completion of the system. However, the end product and its benefits to Goddard's thermal vacuum test portfolio will carry the usefulness of this facility well into the next century.

Webb, Andrew↗

Vapor Growth of Binary and Ternary Chalcogenides in Preparation for Microgravity Experiments

In the bulk crystal growth of some technologically important semiconducting chalcopyrites, such as ZnTe, CdS, ZnSe and ZnS, vapor growth techniques have significant advantages over melt growth techniques due to the high melting points of these materials. The realization of routine production of high-quality single crystals of these semiconductors requires a fundamental, systematic and in-depth study on the PVT growth process and crystal growth by vapor transport in low gravity offers a set of unique conditions for this study. Previously, two reasons have been put forward to account for this. The first is weight-related reductions in crystal strain and defects. These are thought to be caused by the weight of the crystals during processing at elevated temperatures and retained on cooling, particularly for materials with a low yield strength. The second, and more general, reason is related to the reduction in density-gradient driven convection. The PVT crystal growth process consists of essentially three processes: sublimation of the source material, transport of the vapor species and condensation of the vapor species to form the crystal. The latter two processes can be affected by the convection caused by gravitational accelerations on Earth. Reductions in such convection in low gravity is expected to yield a nearly diffusion-limited growth condition which results in more uniform growth rates (on the microscopic scale) and hence greater crystalline perfection and compositional homogeneity. The reduction of convective contamination by performing flight experiments in a reduced gravity environment will help to understand the relation between fluid phase processes (growth parameters) and defect and impurity incorporation in grown crystals.

Su, C.↗

Microgravity and Macromolecular Crystallography

Macromolecular crystal growth has been seen as an ideal experiment to make use of the reduced acceleration environment provided by an orbiting spacecraft. The experiments are small, simply operated and have a high potential scientific and economic impact. In this review we examine the theoretical reasons why microgravity should be a beneficial environment for crystal growth and survey the history of experiments on the Space Shuttle Orbiter, on unmanned spacecraft, and on the Mir space station. Finally we outline the direction for optimizing the future use of orbiting platforms.

Kundrot, Craig E.↗

Ground Based Experiments in Support of Microgravity Research Results-Vapor Growth of Organic Nonlinear Optical Thin Film

This work is specifically focused on explaining previous results obtained for the crystal growth of an organic material in a reduced gravity environment. On STS-59, in April 1994, two experiments were conducted with N,N-dimethyl-p-(2,2-dicyanovinyl) aniline (DCVA), a promising nonlinear optical (NLO) material. The space experiments were set to reproduce laboratory experiments that yielded small, bulk crystals of DCVA. The results of the flight experiment, however, were surprising. Rather than producing a bulk single crystal, the result was the production of two high quality, single crystalline thin films. This result was even more intriguing when it is considered that thin films are more desirable for NLO applications than are bulk single crystals. Repeated attempts on the ground to reproduce these results were fruitless. A second set of flight experiments was conducted on STS-69 in September 1995. This time eight DCVA experiments were flown, with each of seven experiments containing a slight change from the first reference experiment. The reference experiment was programmed with growth conditions identical to those of the STS-59 mission. The slight variations in each of the other seven were an attempt to understand what particular parameter was responsible for the preference of thin film growth over bulk crystal growth in microgravity. Once again the results were surprising. In all eight cases thin films were grown again, albeit with varying quality. So now we were faced with a phenomenon that not only takes place in microgravity, but also is very robust, resisting all attempts to force the growth of bulk single crystals.

Zugrav, M. Ittu↗

Sixth International Microgravity Combustion Workshop

This conference proceedings document is a compilation of papers presented orally or as poster displays to the Sixth International Microgravity Combustion Workshop held in Cleveland, Ohio on May 22-24, 2001. The purpose of the workshop is to present and exchange research results from theoretical and experimental work in combustion science using the reduced-gravity environment as a research tool. The results are contributed by researchers funded by NASA throughout the United States at universities, industry and government research agencies, and by researchers from international partner countries that are also participating in the microgravity combustion science research discipline. These research results are intended for use by public and private sector organizations for academic purposes, for the development of technologies needed for Human Exploration and Development of Space, and to improve Earth-bound combustion and fire-safety related technologies.

Sacksteder, Kurt↗

Bi-Component Droplet Combustion in Reduced Gravity

This research deals with reduced-gravity combustion of bi-component droplets initially in the mm size range or larger. The primary objectives of the research are to study the effects of droplet internal flows, thermal and solutal Marangoni stresses, and species volatility differences on liquid species transport and overall combustion phenomena (e.g., gas-phase unsteadiness, burning rates, sooting, radiation, and extinction). The research program utilizes a reduced-gravity environment so that buoyancy effects are rendered negligible. Use of large droplets also facilitates visualization of droplet internal flows, which is important for this research. In the experiments, droplets composed of low- and high-volatility species are burned. The low-volatility components are initially present in small amounts. As combustion of a droplet proceeds, the liquid surface mass fraction of the low-volatility component will increase with time, resulting in a sudden and temporary decrease in droplet burning rates as the droplet rapidly heats to temperatures close to the boiling point of the low-volatility component. This decrease in burning rates causes a sudden and temporary contraction of the flame. The decrease in burning rates and the flame contraction can be observed experimentally. Measurements of burning rates as well as the onset time for flame contraction allow effective liquid-phase species diffusivities to be calculated, e.g., using asymptotic theory. It is planned that droplet internal flows will be visualized in future flight and ground-based experiments. In this way, effective liquid species diffusivities can be related to droplet internal flow characteristics. This program is a continuation of extensive ground based experimental and theoretical research on bi-component droplet combustion that has been ongoing for several years. The focal point of this program is a flight experiment (Bi-Component Droplet Combustion Experiment, BCDCE). This flight experiment is under development. However, supporting studies have been performed. Because of space limitations, only some of the research performed over the last two years (since the 5th Microgravity Combustion Workshop) is summarized here.

Shaw, B. D.↗

Vapor Growth of Binary and Ternary Chalcogenides in Preparation for Microgravity Experiments

In the bulk crystal growth of some technologically important semiconducting chalcopyrites, such as ZnTe, CdS, ZnSe and ZnS, vapor growth techniques have significant advantages over melt growth techniques due to the high melting points of these materials. The realization of routine production of high-quality single crystals of these semiconductors requires a fundamental, systematic and in-depth study on the PVT growth process and crystal growth by vapor transport in low gravity offers a set of unique conditions for this study. Previously, two reasons have been put forward to account for this. The first is weight-related reductions in crystal strain and defects. These are thought to be caused by the weight of the crystals during processing at elevated temperatures and retained on cooling, particularly for materials with a low yield strength. The second, and more general, reason is related to the reduction in density-gradient driven convection. The PVT crystal growth process consists of essentially three processes: sublimation of the source material, transport of the vapor species and condensation of the vapor species to form the crystal. The latter two processes can be affected by the convection caused by gravitational accelerations on Earth. Reductions in such convection in low gravity is expected to yield a nearly diffusion-limited growth condition which results in more uniform growth rates (on the microscopic scale) and hence greater crystalline perfection and compositional homogeneity. The reduction of convective contamination by performing flight experiments in a reduced gravity environment will help to understand the relation between fluid phase processes (growth parameters) and defect and impurity incorporation in grown crystals.

Su, Ching-Hua↗

Nucleation of Quantized Vortices from Rotating Superfluid Drops

The long-term goal of this project is to study the nucleation of quantized vortices in helium II by investigating the behavior of rotating droplets of helium II in a reduced gravity environment. The objective of this ground-based research grant was to develop new experimental techniques to aid in accomplishing that goal. The development of an electrostatic levitator for superfluid helium, described below, and the successful suspension of charged superfluid drops in modest electric fields was the primary focus of this work. Other key technologies of general low temperature use were developed and are also discussed.

Donnelly, Russell J.↗

Free-falling Crystals: Biological Macromolecular Crystal Growth Studies in Low Earth Orbit

Spacecraft orbiting the earth experience a reduced acceleration environment due to being in a state of continuous free-fall. This state colloquially termed microgravity, has produced improved X-ray diffraction quality crystals of biological macromolecules. Improvements in X-ray diffraction resolution (detail) or signal to noise, provide greater detail in the three-dimensional molecular structure providing information about the molecule, how it works, how to improve its function or how to impede it. Greater molecular detail obtained by crystallization in microgravity, has important implications for structural biology. In this article we examine the theories behind macromolecule crystal quality improvement in microgravity using results obtained from studies with the model protein, chicken egg white lysozyme.

Judge, Russell A.↗

The Microgravity Science Glovebox

The Microgravity Science Glovebox (MSG) provides scientific investigators the opportunity to implement interactive experiments on the International Space Station. The facility has been designed around the concept of an enclosed scientific workbench that allows the crew to assemble and operate an experimental apparatus with participation from ground-based scientists through real-time data and video links. Workbench utilities provided to operate the experiments include power, data acquisition, computer communications, vacuum, nitrogen. and specialized tools. Because the facility work area is enclosed and held at a negative pressure with respect to the crew living area, the requirements on the experiments for containment of small parts, particulates, fluids, and gasses are substantially reduced. This environment allows experiments to be constructed in close parallel with bench type investigations performed in groundbased laboratories. Such an approach enables experimental scientists to develop hardware that more closely parallel their traditional laboratory experience and transfer these experiments into meaningful space-based research. When delivered to the ISS the MSG will represent a significant scientific capability that will be continuously available for a decade of evolutionary research.

Baugher, Charles R.↗

Dynamics of a Finite Liquid Oxygen (LOX) Column in a Pulsed Magnetic Field

It is well known that liquid oxygen has a sufficient paramagnetic susceptibility that a strong magnetic field gradient can lift it in the earth's gravitational field. The movement of liquid oxygen is vital to the space program since it one of the primary oxidizers used for propulsion. Transport of liquid oxygen (LOX) via direct interaction of the magnetic fields (B field) with the fluid is a current topic of research and development at Kennedy Space Center, FL. This method of transporting (i.e. pumping) LOX may have particular advantages on Mars and other reduced gravitational environments, namely safety and reliability. This paper will address transport of a magnetic fluid, LOX, via phased-pulsed electromagnets acting on the edge of the column of fluid. The authors have developed a physical model from first-principles for the motion of a magnetic fluid in a particular U-tube geometry subjected to a pulsed magnetic field from an arbitrary solenoidal electromagnet. Experimental data that have been collected from the analogous geometry correlate well to that of the ab-initio calculations.

Youngquist, Robert↗

Space Rose Pleases the Senses

International Flavors and Fragrances (IFF), Inc., discovered a new scent by flying a miniature rose plant aboard NASA's Space Shuttle Discovery Flight STS-95. IFF and the Wisconsin Center for Space Automation and Robotics (WCSAR) partnered to fly the rose plant in the commercial plant research facility, ASTROCULTURE(TM), for reduced-gravity environment research. IFF commercialized the space rose note, which is now a fragrance ingredient in a perfume developed by Shiseido Cosmetics (America), Ltd. In addition to providing a light crisp scent, the oil from the space rose can also serve as a flavor enhancer. ASTROCULTURE(TM) is a trademark of the Wisconsin Center for Space Automation and Robotics.

Source record↗

Experimental Methods in Reduced-gravity Soldering Research

The National Center for Microgravity Research, NASA Glenn Research Center, and NASA Johnson Space Center are conducting an experimental program to explore the influence of reduced gravity environments on the soldering process. An improved understanding of the effects of the acceleration environment is important to application of soldering during current and future human space missions. Solder joint characteristics that are being considered include solder fillet geometry, porosity, and microstructural features. Both through-hole and surface mounted devices are being investigated. This paper focuses on the experimental methodology employed in this project and the results of macroscopic sample examination. The specific soldering process, sample configurations, materials, and equipment were selected to be consistent with those currently on-orbit. Other apparatus was incorporated to meet requirements imposed by operation onboard NASA's KC-135 research aircraft and instrumentation was provided to monitor both the atmospheric and acceleration environments. The contingent of test operators was selected to include both highly skilled technicians and less skilled individuals to provide a population cross-section that would be representative of the skill mix that might be encountered in space mission crews.

Pettegrew, Richard D.↗

Comparison of the Oxidation Rates of Some New Copper Alloys

Copper alloys were studied for oxidation resistance and mechanisms between 550 and 700 C, in reduced-oxygen environments expected in rocket engines, and their oxidation behaviors compared to that of pure copper. They included two dispersion-strengthened alloys (precipitation-strengthened and oxide-dispersion strengthened, respectively) and one solution-strengthened alloy. In all cases the main reaction was oxidation of Cu into Cu2O and CuO. The dispersion-strengthened alloys were superior to both Cu and the solution-strengthened alloy in oxidation resistance. However, factors retarding oxidation rates seemed to be different for the two dispersion-strengthened alloys.

Ogbuji, Linus U. J. Thomas↗

Wire Insulation Flammability Experiment: USML-1 One Year Post Mission Summary

Herein we report the results from the Wire Insulation Flammability (WIF) Experiment performed in the Glovebox Facility on the USML-1 mission. This experiment explored various aspects of electrically induced fire scenarios in a reduced gravity environment. Under quiescent microgravity conditions, heat and mass transfer are dominated by diffusive and radiative transport; while in normal-gravity buoyancy induced convection often dominates. Of considerable scientific and practical interest is the intermediate situation of combustion occurring in the presence of imposed gas flows, with lower characteristic velocities than those induced by buoyancy in noma1 gravity. Two distinct cases naturally arise: flow direction opposed to, or concurrent with, the flame spread direction. Two tests of each kind were conducted in the WIF experiment, providing the first controlled demonstration of flame spreading in forced convection ever conducted in space. Four test modules were flown. The wire insulation, 1.5 mm in diameter, was polyethylene, extruded onto nichrome wire. Temperatures of the wh3 cores and insulation heated in quiescent and flowing environments were measured. Video and still-camera images of the samples, burning in air flowing at approximately 10 cm/sec, were recorded to obtain flame characteristics including spread rate, structure and temperature. Flame spread rates in concurrent flow were approximately twice those in opposed flow. In concurrent and opposed flow regimes, the spreading flames stabilized around a bead of molten insulation material, within which bubble nucleation was observed. An ignition attempt without flow mated a quiescent cloud of vaporized fuel which ignited dramatically yet failed to sustain normal flame spread. Finally, all tests produced substantial soot agglomerates, particularly the concurrent flow tests; and the collected soot has a morphology very distinct from soot formed in normal gravity flames. Several unexpected and unique microgravity combustion phenomena were observed.

Greenberg, Paul S.↗

Creation and Distribution of CAIs in the Protoplanetary Nebula

CaAl rich refractory mineral inclusions (CAIs) found at 1 - 10% mass fraction in primitive chondrites appear to be several million years older than the dominant (chondrule) components in the same parent bodies. A prevalent concern is that it is difficult to retain CAIs for this long against gas-drag-induced radial drift into the sun. We assess a hot inner (turbulent) nebula context for CAI formation, using analytical models of nebula evolution and particle diffusion. We show that outward radial diffusion in a weakly turbulent nebula can prevent significant numbers of CAI-size particles from being lost into the sun for times of 1 - 3 x 10(exp 6) years. To match the CAI abundances quantitatively, we advocate an enhancement of the inner hot nebula in silicate-forming material, due to rapid inward migration of very primitive, silicate and carbon rich, meter-sized objects. 'Combustion' of the carbon into CO would make the CAI formation environment more reduced than solar, as certain observations imply. Abundant CO might also play a role in mass-independent chemical fractionation of oxygen isotopes as seen in CAIs and associated primitive, high-temperature condensates.

Cuzzi, J. N.↗

Quantitative Studies on the Propagation and Extinction of Near-Limit Premixed Flames Under Normal and Microgravity

The main objective of this research is to introduce accurate fluid mechanics measurements diagnostics in the 2.2-s drop tower for the determination of the detailed flow-field at the states of extinction. These results are important as they can then be compared with confidence with detailed numerical simulations so that important insight is provided into near-limit phenomena that are controlled by not well-understood kinetics and thermal radiation processes. Past qualitative studies did enhance our general understanding on the subject. However, quantitative studies are essential for the validation of existing models that subsequently be used to describe near-limit phenomena that can initiate catastrophic events in micro- and/or reduced gravity environments.

Dong, Y.↗