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At least 451 records · Page 25

Development of aircraft brake materials

The requirements of brake materials were outlined and a survey made to select materials to meet the needs of high temperature brakes. A number of metals and ceramic materials were selected and evaluated in sliding tests which simulated aircraft braking. Nickel, molybdenum tungsten, Zr02, high temperature cements and carbons were tested. Additives were then incorporated into these materials to optimize their wear or strength behavior with particular emphasis on nickel and molybdenum base materials and a high temperature potassium silicate cement. Optimum materials were developed which improved wear behavior over conventional brake materials in the simulated test. The best materials are a nickel, aluminum oxide, lead tungstate composition containing graphite or molybdenum disulphite; a molybdenum base material containing LPA100 (an intermetallic compound of cobalt, molybdenum, and silicon); and a carbon material (P5).

Ho, T. L.↗

Determination of copper, scandium, molybdenum, tin, lead, and iron group elements in lunar surface materials

Distribution regularities of copper, scandium, molybdenum, tin, lead, and iron group elements were investigated in basaltoid rocks of lunar and terrestrial origin. Samples of various regolith zones taken in the area of the Sea of Fertility were analyzed, along with samples of basic and ultrabasic rocks of the East African Rift for their content of the trace admixtures listed. Data obtained on the abundance of copper, scandium, molybdenum, tin, lead, cobalt, nickel, chromium, and vanadium in Luna 16 lunar surface material were compared with the abundance of these elements in samples of lunar rocks returned by Apollo 11, Apollo 12, and Apollo 14, with the exception of scandium; its content in the latter samples was considerably higher.

Pavlenko, L. I.↗

Metallographic study of metallic fragment of lunar surface material

A high precision investigation of a metallic fragment from the lunar material returned by the Soviet Luna 16 automatic station revealed three characteristic temperature intervals with different kinetics of solid solution decomposition. The following were found in the structure of the iron-nickel-cobalt alloy: (1) delta-phase and alpha-ferrite of diffusional, displacement origin in the grain boundary and acicular forms; and (2) martensite of isothermal and athermal nature, acicular, lamellar, massive, and dendritic. The diversity of the shapes of structural constituents is associated with the effect on their formation of elastic distortions and various mechanisms of deformation relaxation processes.

Mints, R. I.↗

Design, construction and evaluation of a 12.045 GHz, 2.0 kW-cw permanent-magnet focused klystron amplifier

An analytical and experimental program to demonstrate the technical feasibility of a lightweight, high-efficiency, 1-2 kW cw, permanent magnet focused klystron operating at 12.0 GHz was described. The design is based on use of a samarium-cobalt permanent magnet for focusing of the electron beam and choice of the most optimum parameters for maximum efficiency. A filter-loaded output circuit is used for the required bandwidth. The design incorporates a collector which is demountable from the tube to facilitate multistage depressed collector experiments, permitting replacement with a NASA-designed axisymmetric, electrostatic collector for linear beam microwave tubes. A further requirement is that the focusing field between the last interaction gap and the collector decay in a prescribed manner referred to as adiabatic expansion.

Nishida, J. M.↗

Oxygen reduction of several gold alloys in 1-molar potassium hydroxide

With rotated disk-and-ring equipment, polarograms and other electrochemical measurements were made of oxygen reduction in 1-molar potassium hydroxide on an equiatomic gold-copper (Au-Cu) alloy and a Au-Cu alloy doped with either indium (In) or cobalt (Co) and on Au doped with either nickel (Ni) or platinum (Pt). The results were compared with those for pure Au and pure Pt. The two-electron reaction dominated on all Au alloys as it did on Au. The polarographic results at lower polarization potentials were compared, assuming exclusively a two-step reduction. A qualified ranking of cathodic electrocatalytic activity on the freshly polished reduced disks was indicated: anodized Au Au-Cu-In Au-Cu Au-Cu-Co is equivalent or equal to Au-Pt Au-Ni. Aging in distilled water improved the electrocatalytic efficiency of Au-Cu-Co, Au-Cu, and (to a lesser extent) Au-Cu-In.

Miller, R. O.↗

Shock-induced melting in anorthositic rock 60015 and a fragment of anorthositic breccia from the 'picking pot' /70052/

Microscopic and chemical evidence are presented to support the contention that shock-generated incipient grain-boundary melting of plagioclase occurred in an anorthositic lunar rock and that shock-generated plagioclase liquid was present along grain boundaries during post-shock adiabatic expansion in a fragment of anorthositic breccia. The first contention is supported by microtextural relationships in the rock, the composition of its metal particles (most iron with some cobalt and less nickel), and glass inclusions with vapor bubbles. The second contention is supported by angular irregular voids in the fragment as well as the occurrence of oriented glass filaments in some of the voids. It is shown that shock-generation of 'cataclastic anorthosite' and high-temperature plagioclase liquids can explain the exceptionally young lead and argon ages of the anorthositic rock. The results of the breccia study indicate that shock lithification of plagioclase-rich particulate material from the highland regolith is due to grain-boundary melting of plagioclase.

Sclar, C. B.↗

Comparison of isothermal and cyclic oxidation behavior of twenty-five commercial sheet alloys at 1150 C

Twenty-five commercial nickel-, iron-, and cobalt-base sheet alloys incorporating chromium or chromium and aluminum additions for oxidation resistance were tested at 1150 C in air for 100 hr in both isothermal and 1-hr cyclic furnace exposures. The alloys were evaluated by sample specific weight change, by type of scale formed, by amount and type of spall, and by sample thickness change and microstructure.-

Barrett, C. A.↗

Na-22, Ne-E, extinct radioactive anomalies and unsupported Ar-40

The possibility that the origin of extinct radioactivities depended on their living long enough for grains to form in the expanding nucleosynthetic envelope, rather than on their living long enough for meteorites to form, is examined. As an example, the interpretation of Na-22 as a detectable extinct radioactivity, with a half life of only 2.6 years, is explored and related to Ne-22 occurrence. Similar arguments involving He-4, Ar-40, K-40, K-41, and calcium, titanium, chromium, manganese, iron, nickel, and cobalt isotopes are briefly presented.

Clayton, D. D.↗

Comparative thermal fatigue resistance

Nineteen cast nickel-base alloys, five cast cobalt-base alloys, and two wrought nickel-base alloys are included in study. Five nickel-base alloys have directionally-solidified polycrystalline grain structure. Three diffusion coatings and vapor-deposited overlay coating are also included in investigation.

Bizon, P. T.↗

Universal solar-cell terminal

Terminal, which replaces stakes or lugs in conventional design with loop receptacles for wires from cell and harness, uses dissimilar bonding properties (metal-to-glass and/or ceramics) of iron-nickel-cobalt alloy in conjunction with standard termination.

Bashin, S.↗

Ironless-armature brushless motor

Device uses 12-pole samarium cobalt permanent-magnet rotor and three Hall-effect sensors for commutation. In prototype motor, torque constant (3-phase delta) is 65 oz-in/amp; electrical time constant (L/R) is 0.2 x 0.001 sec, and armature resistance is 20 ohms.

Fisher, R. L.↗

Work function determination of promising electrode materials for thermionic energy converters

The work function determinations of candidate materials for low temperature (1400 K) thermionics through vacuum emission tests are discussed. Two systems, a vacuum emission test vehicle and a thermionic emission microscope are used for emission measurements. Some nickel and cobalt based super alloys were preliminarily examined. High temperature physical properties and corrosion behavior of some super alloy candidates are presented. The corrosion behavior of sodium is of particular interest since topping cycles might use sodium heat transfer loops. A Marchuk tube was designed for plasma discharge studies with the carbide and possibly some super alloy samples. A series of metal carbides and other alloys were fabricated and tested in a special high temperature mass spectrometer. This information coupled with work function determinations was evaluated in an attempt to learn how electron bonding occurs in transition alloys.

Jacobson, D.↗

Selected fretting-wear-resistant coatings for titanium - 6-percent-aluminum - 4-percent-vanadium alloy

A titanium - 6-percent-aluminum - 4-percent-vanadium alloy (Ti-6Al-4V) was subjected to fretting-wear exposures against uncoated Ti-6Al-4V as a baseline and against various coatings and surface treatments applied to Ti-6Al-4V. The coatings evaluated included plasma-sprayed tungsten carbide with 12 percent cobalt, aluminum oxide with 13 percent titanium oxide, chromium oxide, and aluminum bronze with 10 percent aromatic polyester; polymer-bonded polyimide, polyimide with graphite fluoride, polyimide with molybdenum disulfide (MoS2), and methyl phenyl silicone bonded MoS2, preoxidation surface treatment, a nitride surface treatment, and a sputtered MoS2 coating. Results of wear measurements on both the coated and uncoated surfaces after 300,000 fretting cycles indicated that the polyimide coating was the most wear resistant and caused the least wear to the uncoated mating surface.

Bill, R. C.↗

Zero-G processing of magnets experiment MA-070

Solidification of magnetic materials in the low gravity orbital environment was studied. The magnetic compounds under study, manganese bismuth and copper cobalt cerium ((Cu, Co)5Ce), both have the potential for the development of high coercive strength. Preliminary results indicate that static fluid configurations, in the absence of the gravitational body force, differ substantially from the documented terrestrial behavior. Chemical homogeneity is substantially enhanced on a macroscopic and microscopic level. Single crystal matrices have been grown in the coordinated growth regions of the flight samples. Primary crystals one order of magnitude greater than those grown terrestrially have been noted and are limited in size by the ampoule dimensions.

Larson, D. J., Jr.↗

Irradiate-anneal screening of total dose effects in semiconductor devices

An extensive investigation of irradiate-anneal (IRAN) screening against total dose radiation effects was carried out as part of a program to harden the Mariner Jupiter/Saturn 1977 (MJS'77) spacecraft to survive the Jupiter radiation belts. The method consists of irradiating semiconductor devices with Cobalt-60 to a suitable total dose under representative bias conditions and of separating the parts in the undesired tail of the distribution from the bulk of the parts by means of a predetermined acceptance limit. The acceptable devices are then restored close to their preirradiation condition by annealing them at an elevated temperature. IRAN was used when lot screen methods were impracticable due to lack of time, and when members of a lot showed a diversity of radiation response. The feasibility of the technique was determined by testing of a number of types of linear bipolar integrated circuits, analog switches, n-channel JFETS and bipolar transistors. Based on the results of these experiments a number of device types were selected for IRAN of flight parts in the MJS'77 spacecraft systems. The part types, screening doses, acceptance criteria, number of parts tested and rejected as well as the program steps are detailed.

Stanley, A. G.↗

Prediction and verification of creep behavior in metallic materials and components for the space shuttle thermal protection system

A method of analysis was developed for predicting permanent cyclic creep deflections in stiffened panel structures. This method uses creep equations based on cyclic tensile creep tests and a computer program to predict panel deflections as a function of mission cycle. Four materials were investigated - a titanium alloy (Ti-6Al-4V), a cobalt alloy (L605), and two nickel alloys (Rene'41 and TDNiCr). Steady-state and cyclic creep response data were obtained by testing tensile specimens fabricated from thin gage sheet (0.025 and 0.63 cm nominal). Steady-state and cyclic creep equations were developed which describe creep as a function of time, temperature and load. Tests were also performed on subsize (6.35 x 30.5 cm) rib and corrugation stiffened panels. These tests were used to correlate creep responses between elemental specimens and panels. The panel response was analyzed by use of a specially written computer program.

Davis, J. W.↗

Influence of gaseous hydrogen on the mechanical properties of high temperature alloys

Tensile tests of six nickel-base and one cobalt-base alloy were conducted in 34.5 MN/sq m helium and hydrogen environments at temperatures from 297 K to 1,088 K. Mechanical properties tests of the nickel-base alloy MAR M-246 (Hf modified), in two cast conditions, were conducted in gaseous environments at temperatures from 297 K to 1,144 K and pressures from one atmosphere to 34.5 MN/sq m. The objective of this program was to obtain the mechanical properties of the various alloys proposed for use in space propulsion systems in a pure hydrogen environment at different temperatures and to compare with the mechanical properties in helium at the same conditions. All testing was conducted on solid specimens exposed to external gaseous pressure. Smooth and notched tensile properties were determined using ASTM tensile testing techniques, and creep-rupture life was determined using ASTM creep-rupture techniques. Low-cycle fatigue life was established by constant total strain and constant stress testing using smooth specimens and a closed-loop test machine.

Source record↗

Yield stress of cemented tungsten carbide

Cemented tungsten carbide yields plastically at room temperature in the presence of a large hydrostatic pressure component. By approximate analysis of the state of stress in supported opposed anvils and by measurement of the pressure at which the anvil tips exhibit a permanent deviation from planarity, we have obtained the yield stress of such materials. Our value for the yield stress of a 3% cobalt cemented tungsten carbide is 86 kbar.

Ruoff, A. L.↗