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At least 451 records · Page 25

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NASA NTRS2017

Crack Opening Displacement Behavior in Ceramic Matrix Composites

Ceramic Matrix Composites (CMC) modeling and life prediction strongly depend on oxidation, and therefore require a thorough understanding of when matrix cracks occur, the extent of cracking for given conditions (time-temperature-environment-stress), and the interactions of matrix cracks with fibers and interfaces. In this work, the evolution of matrix cracks in a melt-infiltrated Silicon Carbide/Silicon Carbide (SiC/SiC) CMC under uniaxial tension was examined using scanning electron microscopy (SEM) combined with digital image correlation (DIC) and manual crack opening displacement (COD) measurements. Strain relaxation due to matrix cracking, the relationship between COD's and applied stress, and damage evolution at stresses below the proportional limit were assessed. Direct experimental observation of strain relaxation adjacent to regions of matrix cracking is presented and discussed. Additionally, crack openings were found to increase linearly with increasing applied stress, and no crack was found to pass fully through the gage cross-section. This observation is discussed in the context of the assumption of through-cracks for all loading conditions and fiber architectures in oxidation modeling. Finally, the combination of SEM with DIC is demonstrated throughout to be a powerful means for damage identification and quantification in CMC's at stresses well below the proportional limit.

acoustic emission↗

DOE OSTI2021

Core–Multishell-Structured Digital-Gradient Cathode Materials with Enhanced Mechanical and Electrochemical Durability

Ni-rich cathode materials provide high energy density, but their structural and surface instability limits their cyclability and thermal stability. As one of the approaches to mitigate this problem, cathode materials comprising Ni-rich high-capacity core wrapped in Mn-rich multiple shells are produced successfully. In contrast to the conventional batch-type process for concentration-gradient materials, a digital-gradient cascade coprecipitation process described here achieves the improvements in productivity and quality consistency needed to move toward large-scale manufacturing. The core-multishell cathode materials produced in this manner not only have longer cycle life and improved rate performance compared to homogeneous Ni-rich cathode materials having the same overall composition, but also show remarkably enhanced thermal stability and low impedance growth characteristics. In a novel attempt to determine the correlation between the mechanical properties of the core-multishell cathode particles and their electrochemical cyclabilities, their breaking force and elasticity were successfully measured using a statistical approach, which indicates that a cathode particle with stable surface composition as well as high breaking force has improved capacity retention and durability. These results guide the realization of long life and high thermal stability in Ni-rich cathode materials through heterogeneous particle engineering.

25 ENERGY STORAGE↗

DOE OSTI2022

Characterizing the Thermal-Induced Distortion of Large-Scale Polymer Composite Printed Structures

The Big Area Additive Manufacturing (BAAM) system has been used to print large-scale parts, such as automotive structures and molds for tooling, with fiber-reinforced polymer composites. Incorporating reinforcing fibers in printed parts is commonly used to increase stiffness and strength, but it also introduces significant anisotropy in the thermomechanical performance, which can lead to distortion and warping during thermal cycling. Characterizing and understanding how a printed tool distorts is crucial to maintaining tolerances and avoiding part failure. This study uses digital image correlation (DIC) to measure the coefficient of thermal expansion (CTE) of a printed part from room temperature and to a known steady state temperature. The samples were printed with carbon fiber reinforced acrylonitrile butadiene styrene (CF-ABS). Various nozzle geometries were evaluated in this study with the intent of minimizing the thermal- induced distortion experienced by printed parts.

Corum, Tyler↗

NASA NTRSDate not supplied

High-Cycle Fatigue Behavior of SiC-based Ceramic Matrix Composites (CMCs) at High Temperatures

High-cycle fatigue (HCF) behavior of a melt-infiltrated, pre-preg SiC/SiC ceramic matrix composite (CMC) was investigated using dogbone tensile specimens without and with simulated cooling holes at 1500 and 2400 °F. The CMC material used for this study was fabricated by GE Aviation and had a ply configuration of [0/90/0]3. HCF tests were conducted with an R-ratio of 0.6 and a cyclic frequency of 30 Hz. Runout in HCF was defined as 30 million cycles. Monotonic tensile tests were conducted at room temperature (RT) on as-received CMC specimens and on runout HCF specimens to determine residual tensile strengths. Digital image correlation (DIC) and acoustic emission (AE) techniques were used to monitor the initiation and progression of damage in RT tensile tests on specimens with and without holes. Microscopy was performed on the polished edge of specimens without cooling holes and on the polished face of specimens with cooling holes that were tested in HCF and achieved runout. Comparisons were made with baseline specimens. Fractography was performed to examine the fracture surfaces of samples that failed under different loading conditions.

Ceramic Matrix Composites↗

NASA NTRS1981

Calculation of the thermodynamic properties of a mixture of gases as a function of temperature and pressure

The evaluation of the thermodynamic properties of a gas mixture can be performed using a generalized correlation which makes use of the second virial coefficient. This coefficient is based on statistical mechanics and is a function of temperature and composition, but not of pressure. The method provides results accurate to within 3 percent for gases which are nonpolar or only slightly polar. When applied to highly polar gases, errors of 5 to 10 percent may result. For gases which associate, even larger errors are possible. The sequences of calculations can be routinely programmed for a digital computer. The thermodynamic properties of a mixture of neon, argon and ethane were calculated by such a program. The result will be used for the design of the gas replenishment system for the Energetic Gamma Ray Experiment Telescope.

Colon, G.↗

NASA NTRS2010

Wide-Band Heterodyne Submillimetre Wave Spectrometer for Planetary Atmospheres

We present calculations and measurements on a passive submillimetre wave spectroscopic sounder to gather data on the thermal structure, dynamics and composition of the upper atmosphere of a planet, e.g. the stratosphere of Jupiter, or the entire thickness of the atmosphere of Mars. The instrument will be capable of measuring wind speeds, temperature, pressure, and key constituent concentrations in the stratosphere of the target planet. This instrument consists of a Schottky diode based front end and a digital back-end spectrometer. It differs from previous space-based spectrometers in its combination of wide tunability (520-590 GHz), and rapid frequency switching between widely spaced lines within that range. This will enable near simultaneous observation of multiple lines, which is critical to the reconstruction of atmospheric pressure and density versus altitude profiles. At the same time frequency accuracy must be high to enable wind speeds to be determined directly by measurement of the line's Doppler shift.

Submillimeter↗

DOE OSTI2024

System and method for high power diode based additive manufacturing

The present disclosure relates to a system for performing an Additive Manufacturing (AM) fabrication process on a powdered material, deposited as a powder bed and forming a substrate. The system makes use of a laser for generating a laser beam, and an optical subsystem. The optical subsystem is configured to receive the laser beam and to generate an optical signal comprised of electromagnetic radiation sufficient to melt or sinter the powdered material. The optical subsystem uses a digitally controlled mask configured to pattern the optical signal as needed to melt select portions of a layer of the powdered material to form a layer of a 3D part. A power supply and at least one processor are also included for generating a plurality of different power density levels selectable based on a specific material composition, absorptivity and diameter of the powder particles, and a known thickness of the powder bed. The powdered material is used to form the 3D part in a sequential layer-by-layer process.

El-Dasher, Bassem S.↗

DOE OSTI2021

3D Tracking of a Single Electron in IOTA

High-resolution observations of single-particle dynamics have potential as a powerful tool in the diagnostics, tuning and design of storage rings. We are presenting the results of experiments with single electrons that were conducted at Fermilab’s IOTA ring to explore the feasibility of this approach. A set of sensitive, high-resolution digital cameras was used to detect the synchrotron radiation emitted by an electron, and the resulting images were used to reconstruct the time evolution of oscillation amplitudes in all three degrees of freedom. From the evolution of the oscillation amplitudes, we deduce transverse emittances, momentum spread, damping times, beam energy and estimated residual-gas density and composition. To our knowledge, this is the first time that the dynamics of a single particle in a storage ring has been tracked in all three dimensions. We discuss farther development of a single particle diagnostics that may allow reconstruction of its turn-by-turn coordinates over macroscopic periods of time facilitating ultra-precise lattice diagnostics and direct benchmarking of tracking codes.

43 PARTICLE ACCELERATORS↗

DOE OSTI2024

Synthesis of Correct Digital Controller Models from Specifications by Model Transformation (21-0320)

The design of high consequence controllers (in weapons systems, autonomy, etc.) that do what they are supposed to do is a significant challenge. Testing simply does not come close to meeting the requirements for assurance. Today circuit designers at Sandia (and elsewhere) typically capture the core behavior of their components using state models in tools such as STATEFLOW. They then check that their models meet certain requirements (e.g. “The system bus must not deadlock” or “both traffic lights at an intersection must not be green at the same time”) using tools called model checkers. If the model checker returns “yes” then the property is guaranteed to be satisfied by the model. However, there are several drawbacks to this industry practice: (1) there is a lot of detail to get right, this is particularly challenging when there are multiple components requiring complex coordination (2) any errors returned by the model checker have to be traced back through the design and fixed, necessitating rework, (3) there are severe scalability problems with this approach, particularly when dealing with concurrency. All this places high demands on the designers who now face not only an accelerated schedule but also controllers of increasing complexity. This report describes a new and fundamentally different approach to the construction of safety-critical digital controllers. Instead of directly constructing a complete model and then trying to verify it, the designer can start with an initial abstract (think “sketch”) model plus the requirements, from which a correct concrete model is automatically synthesized. There is no need for post-hoc verification of required functional properties. Having tool to carry this out will significantly impact the nation’s ability to ensure the safety of high-consequence digital systems. The approach has been implemented in a prototype tool, along with a suite of examples, including ones that reflect actual problems faced by designers. Our approach operates on a variant of Statecharts developed at Sandia called Qspecs. Statecharts are a widely used formalism for developing concurrent reactive systems, supporting scalability through allowing state models containing composite states, which are the serial or parallel composition of substates which can themselves contain statecharts. Statecharts enable an incremental style of development, in which states are progressively refined to incorporate greater detail in an incremental model of software development. Our approach formulates a set of constraints from the structure of the models and the requirements and propagates these constraints to a fixpoint. The solution to the constraints is an inductive invariant along with guards on the transitions. We also show how our approach extends to implementation refinement, decomposition, composition, and elaboration. We currently handle safety requirements written in LTL (Linear Temporal Logic)

42 ENGINEERING↗

NASA NTRS1984

Geobotanical discrimination of ultramafic parent materials An evaluation of remote sensing techniques

Color and color infrared aerial photography and imagery acquired from a Daedalus DEI-1260 multispectral airborne scanner were employed in an investigation to discriminate ultramafic rock types in a test site in southwest Oregon. An analysis of the relationships between vegetation characteristics and parent materials was performed using a vegetation classification and map developed for the project, lithologic information derived from published geologic maps of the region, and terrain information gathered in the field. Several analytical methods, including visual image analysis, band ratioing, principal components analysis, and contrast enhancement and subsequent color composite generation were used in the investigation. There was a close correspondence between vegetation types and major rock types. These were readily discriminated by the remote sensing techniques. It was found that ultramafic rock types were separable from non-ultramafic rock types and serpentine was distinguishable from non-serpentinized peridotite. Further investigations involving spectroradiometric and digital classification techniques are being performed to further identify rock types and to discriminate chromium and nickel-bearing rock types.

Mouat, D. A.↗

NASA NTRS1986

Analytical Ultrasonics in Materials Research and Testing

Research results in analytical ultrasonics for characterizing structural materials from metals and ceramics to composites are presented. General topics covered by the conference included: status and advances in analytical ultrasonics for characterizing material microstructures and mechanical properties; status and prospects for ultrasonic measurements of microdamage, degradation, and underlying morphological factors; status and problems in precision measurements of frequency-dependent velocity and attenuation for materials analysis; procedures and requirements for automated, digital signal acquisition, processing, analysis, and interpretation; incentives for analytical ultrasonics in materials research and materials processing, testing, and inspection; and examples of progress in ultrasonics for interrelating microstructure, mechanical properites, and dynamic response.

Vary, A.↗

NASA NTRS1987

Materials analysis by ultrasonics: Metals, ceramics, composites

Vary, Alex↗

NASA NTRS1993

Identification of an interstellar oxide grain from the Murchison meteorite by ion imaging

We report here the first use of a new ion-imaging system to locate a rare interstellar aluminum oxide grain in a Murchison acid residue. While several types of carbon-rich interstellar grains, including graphite, diamond, SiC, and TiC, have previously been found, isotopically anomalous interstellar oxide grains have proven more elusive. We have developed an ion imaging system which allows us to map the isotopic composition of large numbers of grains relatively quickly and is, thus, ideally suited to search for isotopically exotic subsets of grains. The system consists of a PHOTOMETRICS CCD camera coupled to the microchannel plate/fluorescent screen of the WU modified CAMECA IMS-3F ion microprobe. Isotopic images of the sample surface are focused on the CCD and digitized. Subsequent image processing identifies individual grains in the images and determines isotopic ratios for each. For the present work, we have imaged in O-16 and O-18; negligible contributions of (17)OH(-) and (16)OH2(-) signals to the O-18 signal allow the use of low mass resolution, simplifying the measurements. Repeated imaging runs on terrestrial corundum particles showed that the system measures isotopic ratios reproducibly to about +/- 40%. Each imaging run took about six minutes to complete, and for this study there were on average 5-15 grains in each image. We have conducted imaging searches in 2-4 micron size separates of both Orgueil and Murchison.

Nittler, L. R.↗

NASA NTRSDate not supplied

Simulating High Energy Dynamic Impact of IM7/PEKK Continuous Fiber Laminated Thermoplastic Composite using Open Hole Coupon Experiments

The use of advanced thermoplastic composites (TPC) for structural applications in the aerospace and automotive industries has grown increasingly popular due to their high performance, high manufactured part output, and sustainability. Enhancing verification simulations of the progressive failure in TPCs at the coupon scale is needed to better validate advanced composite material models at larger length scales, such as element level panels. MAT_213, a tabulated composite material model, has been applied to simulate high velocity dynamic impact (HEDI) and is integrated in the LS-DYNA explicit finite element (FE) software. Previous efforts using MAT_213 have calibrated HEDI simulated failures with experimental data. Traditionally simulations have relied on a structured mesh to represent quasi-isotropic panels. For this study, a continuous fiber unidirectional tape, IM7/PEKK, was analyzed through a series of verification studies of notched laminate coupons, then validation analyses of quasi-isotropic panels under HEDI were compared with experimental data. Experiments using unidirectional TPC were performed to obtain tabulated stress vs strain curves using Digital Image Correlation (DIC) for input into MAT_213. Next, notched coupon experiments were used as an intermediate step to calibrate the damage and failure behavior in MAT_213. Lastly, investigations into differences between HEDI simulations using a fiber aligned mesh were compared with experimental failure patterns and damage sizes. The use of experimentally generated material behavior along with selective mesh layout improved HEDI predictions with minimal material parameter calibration.

Polymer matrix composites↗

NASA NTRS1975

Application of a dedicated micro-processor for automatic data acquisition of load strain and acoustic-emission data

This paper describes an automatic system for acquisition, logging and analysis of stress, strain and acoustic emission data. The complete system is a combination of several standard items of equipment and a newly developed intelligent data logger which has the capability to send data directly to a large scale computer for reduction and plotting. The data logging and all interfacing with peripheral equipment are accomplished using digital electronics. The heart of the system is a four-bit microprocessor and digital cassette tape unit. The system, which is controlled by instructions from a cathode ray tube terminal, has the capability to transmit data from the cassette unit to a large computer via a time sharing option. Typical results are presented for acoustic emission count rate and total count curves superimposed on stress-strain diagrams for boron/epoxy advanced composites.

Wilson, G. H.↗

NASA NTRS1976

Flight simulation testing equipment for composite material systems

A test program is discussed which aims at establishing the time-temperature-stress characteristics of several classes of high-temperature composite materials in order to determine their suitability for applications in supersonic cruise aircraft. Five advanced composite materials (a boron epoxy, a boron polyimide, a graphite epoxy, a graphite polyimide, and diffusion-bonded boron aluminum) are being evaluated using a flight-test simulator capable of long-term automatic testing based on random loading and realistic flight temperature profiles. The design, construction, and checkout of this simulator are described along with the digital load programmer, load magnitude controllers, the hydraulic pumping system, the heating and cooling systems, the control console, and the data recording system. Typical results for short-term tests performed at constant temperatures and accelerated load rates are presented in terms of a random-load spectrum and a wearout model.

Haskins, J. F.↗

NASA NTRS2022

Integrated Topographic Corrections Improve Forest Mapping Using Landsat Imagery

In mountainous environments, topography strongly affects the reflectance due to illumination effects and cast shadows, which introduce errors in land cover classifications. However, topographic correction is not routinely implemented in standard data pre-processing chains (e.g., Landsat Analysis Ready Data), and there is a lack of consensus whether topographic correction is necessary, and if so, how to conduct it. Furthermore, methods that correct simultaneously for atmospheric and topographic effects are becoming available, but they have not been compared directly. Our objects were to investigate (1) the effectiveness of two topographic correction approaches that integrate atmospheric and topographic correction, (2) improvements in classification accuracy when analyzing topographically corrected single-date imagery (14 July 2016 and 2 October 2016), versus a full Landsat time series from 2014 to 2016, and 3) improvements in classification accuracy when including additional terrain information (i.e., topographic slope, elevation, and aspect). We developed a physical based model and compared it with an enhanced C-correction, both of which integrate atmospheric and topographic correction. We compared classification accuracies with and without topographic correction using combinations of single-date imagery, image composites and spectral-temporal metrics generated from the full Landsat time series, and additional terrain information in the Caucasus Mountains. We found that both the enhanced C-correction and the physical model performed very well and largely eliminated the correlation (Pearson’s correlation coefficient r ranges from 0.06 to 0.24) between surface reflectance and illumination condition, but the physical model performed best (r ranges from 0.05 to 0.11). Both image composites, and spectral-temporal metrics generated from corrected imagery, resulted in significantly (p ≤ 0.05) higher classification accuracies and better forest classifications, especially for the mixed forests. Adding terrain information reduced classification error significantly, but not as much as topographic correction. In summary, topographic correction remains necessary, even when analyzing a full Landsat time series and including a digital elevation model in the classification. We recommend that topographic correction should be applied when analyzing Landsat satellite imagery in mountainous region for forest cover classification.

Atmospheric correction↗

NASA NTRS1991

An interferometric spectral mapper for the Cassini mission to Saturn and Titan

The research reported resulted in a detailed proposal for the Cassini Mission that addressed fundamental atmospheric structure and composition questions for both Saturn and Titan. Due to the brief time available between the initiation of the research and the proposal date, it was necessary to develop the science goals in close synchronicity with the instrument design. A major goal of the program was to acquire, implement, and test SWIR and MWIR arrays suitable for use with the DIGITAL ARRAY SCANNED INTERFEROMETERS, (DASI's), for the extended goal of developing DASI's for a range of spectral mapping research in solar system exploration. These goals were all reached or exceeded in the course of this work.

Smith, William Hayden↗