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At least 451 records · Page 25

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DOE OSTI2025

High Strength and Fracture Resistance of Reduced-Activity W-Ta-Ti-V-Zr High-Entropy Alloy for Fusion Energy Applications

Refractory high-entropy alloys (HEAs) are promising candidates for next-generation nuclear applications, particularly fusion reactors, due to their excellent high-temperature mechanical properties and irradiation resistance. Here, the microstructure and mechanical behavior were investigated for an equimolar WTaTiVZr HEA, designed from a palette of low-activation elements. The as-cast alloy exhibited a dendritic microstructure composed of W-Ta rich dendrites and Zr-Ti-V rich inter-dendritic regions, both possessing a body-centered cubic (BCC) crystal structure. Room temperature bulk compression tests showed ultra-high strength of around 1.6 GPa and plastic strain ~6%, with fracture surfaces showing cleavage facets. The alloy also demonstrated excellent high-temperature strength of ~650 MPa at 500 °C. Scratch-based fracture toughness was ~38 MPa√m for the as-cast WTaTiVZr HEA compared to ~25 MPa√m for commercially used pure tungsten. This higher value of fracture toughness indicates superior damage tolerance relative to commercially used pure tungsten. These results highlight the alloy’s potential as a low-activation structural material for high-temperature plasma-facing components (PFCs) in fusion reactors.

Physics↗

DOE OSTI2024

Regulation of Solar Wind Electron Temperature Anisotropy by Collisions and Instabilities

Abstract Typical solar wind electrons are modeled as being composed of a dense but less energetic thermal “core” population plus a tenuous but energetic “halo” population with varying degrees of temperature anisotropies for both species. In this paper, we seek a fundamental explanation of how these solar wind core and halo electron temperature anisotropies are regulated by combined effects of collisions and instability excitations. The observed solar wind core/halo electron data in ( β ∥ , T ⊥ / T ∥ ) phase space show that their respective occurrence distributions are confined within an area enclosed by outer boundaries. Here, T ⊥ / T ∥ is the ratio of perpendicular and parallel temperatures and β ∥ is the ratio of parallel thermal energy to background magnetic field energy. While it is known that the boundary on the high- β ∥ side is constrained by the temperature anisotropy-driven plasma instability threshold conditions, the low- β ∥ boundary remains largely unexplained. The present paper provides a baseline explanation for the low- β ∥ boundary based upon the collisional relaxation process. By combining the instability and collisional dynamics it is shown that the observed distribution of the solar wind electrons in the ( β ∥ , T ⊥ / T ∥ ) phase space is adequately explained, both for the “core” and “halo” components.

Yoon, Peter H. (ORCID:0000000181343790)↗

NASA NTRS1968

Space related technical investigations Progress report, 1 Mar. - 1 Oct. 1968

Space related studies in low temperature physics, semiconductor properties, astrophysics, atomic physics, and plasma physics

Hildebrandt, A. F.↗

NASA NTRSDate not supplied

Magnetic Measurements of Arc Instabilities in Segmented Arc Heater Column

The Aerodynamic Heating Facility (AHF) at NASA Ames Research Center (ARC) generates high enthalpy, supersonic flow environments for ground testing of NASAheat shield materials. This arc jet heater operates by passing a DC arc (<3200A,<2500V) through a gas column (~10cm diameter, 2m length) and ejecting the heatedgas through a supersonic nozzle into a test chamber. The arc plasma is a partially ionized air mixture at low temperature (< 2eV) but needs to be stable for long test times (up to 30min) at high power (< 20MW). Currently, the operational envelope of the facility is limited by arc instabilities including the kink instability. Consequently, it is of interest to characterize these instabilities to better understand facility limits and inform methods to extend stable operational ranges. Due to the high enthalpy and long timescales (i.e., minutes) diagnostics must be non-invasive. This work will cover the development of two sets of magnetic sensors: differential B-dot sensors and tri-axial magnetic hall sensors and will describe initial measurements of arc motion usingthese sensors.

Kink instability↗

NASA NTRSDate not supplied

Magnetic Measurements of Arc Instabilities in Segmented Arc Heater Column

The Aerodynamic Heating Facility (AHF) at NASA Ames Research Center (ARC) generates high enthalpy, supersonic flow environments for ground testing of NASAheat shield materials. This arc jet heater operates by passing a DC arc (<3200 A,<2500 V) through a gas column (~6 cm diameter, 2 m length) and ejecting the heated gas through a supersonic nozzle into a test chamber. The arc plasma is a partially ionized air mixture at low temperature (< 2 eV) but needs to be stable for long test times (up to 30 min) at high power (< 20 MW). Currently, the operational envelope of the facility is limited by arc instabilities including the kink instability. Consequently, it is of interest to characterize these instabilities to better understand facility limits and inform methods to extend stable operational ranges. Due to the high enthalpy and long timescales (i.e., minutes) diagnostics must be non-invasive. This work will cover the development of two sets of magnetic sensors: differential B-dot sensors and tri-axial magnetic hall sensors and will describe initial measurements of arc motion using these sensors.

Kink instability↗

NASA NTRS2005

PAHs and the Diffuse Interstellar Bands. What have we Learned from the New Generation of Laboratory and Observational Studies?

Polycyclic Aromatic Hydrocarbons (PAHs) are an important and ubiquitous component of carbon-bearing materials in space. PAHs are the best-known candidates to account for the IR emission bands (UIR bands) and PAH spectral features are now being used as new probes of the ISM. PAHs are also thought to be among the carriers of the diffuse interstellar absorption bands (DIBs). In the model dealing with the interstellar spectral features, PAHs are present as a mixture of radicals, ions and neutral species. PAH ionization states reflect the ionization balance of the medium while PAH size, composition, and structure reflect the energetic and chemical history of the medium. A major challenge for laboratory astrophysics is to reproduce (in a realistic way) the physical conditions that exist in the emission and/or absorption interstellar zones, An extensive laboratory program has been developed at NASA Ames to characterize the physical and chemical properties of PAHs in astrophysical environments and to describe how they influence the radiation and energy balance in space and the interstellar chemistry. In particular, laboratory experiments provide measurements of the spectral characteristics of interstellar PAH analogs from the ultraviolet and visible range to the infrared range for comparison with astronomical data. This paper will focus on the recent progress made in the laboratory to measure the direct absorption spectra of neutral and ionized PAHs in the gas phase in the near-W and visible range in astrophysically relevant environments. These measurements provide data on PAHs and nanometer-sized particles that can now be directly compared to astronomical observations. The harsh physical conditions of the IS medium - characterized by a low temperature, an absence of collisions and strong V W radiation fields - are simulated in the laboratory by associating a molecular beam with an ionizing discharge to generate a cold plasma expansion. PAH ions are formed from the neutral precursors in an isolated environment at low temperature (of the order of 100 K). The spectra of neutral and ionized PAHs are measured using the high sensitivity methods of cavity ring down spectroscopy (CRDS). These experiments provide unique information on the spectra of free, cold large carbon molecules and ions in the gas phase. Intrinsic band profiles and band positions of cold gas-phase PAHs can now be measured with high- sensitivity spectroscopy and directly compared to the astronomical data. The electronic bands measured for ionized PAH are found to be intrinsically broad (about 20/cm) while the bands associated with the neutral precursors are narrower (of the order of 2 - 10/cm).

Salama, Farid↗

DOE OSTI2023

Thermal photon production in Gubser inviscid relativistic fluid dynamics

The Gubser solution to inviscid relativistic fluid dynamics is used to examine the role of transverse expansion on the energy spectrum of photons radiated by quark-gluon plasma. Transverse flow is shown to be a modest effect on the energy spectrum of photons as a whole, despite its large effect on rare high-energy photons produced at low temperatures. An exact expression is derived for the volume of the plasma as a function of its temperature. Furthermore, a simple formula is obtained for the energy spectrum of high-energy thermal photons, which is used to relate the inverse slope T eff of the photon spectrum at energy E to the maximum temperature of the plasma T 0 , finding T eff ≈ T 0 / (1 + $\frac{5}{2}$ T 0 /E).

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

NASA NTRS2020

Determination of the Complex Refractive Indices of Aerosol Analogs Formed at Low Temperatures with the NASA Ames Optical Constants Facility (OCF)

The NASA Ames COsmic SImulation Chamber (COSmIC) [1] is a unique experimental facility that allows: 1) cooling a gas mixture to low temperature (150 K) in a jet expansion before inducing chemistry by plasma; and 2) controlling the extent of the chemical reactions by employing a pulsed plasma discharge. This enables the study of the early stages of aerosol production, as well as specific chemical pathways in planetary environments (e.g. Titan’s and Pluto’s atmospheres). Both the gas and solid products can be studied. For a decade COSmIC has been used to simulate Titan’s atmospheric chemistry at low, Titan-like temperature [2]. New developments on the COSmIC facility are investigating formation of aerosols in tenuous, or transitory, atmospheres of other icy bodies [3-5], as well as cool exoplanets atmospheres having a hydrocarbon component, that results in formation of hazes and/or surface deposits of refractory materials. The new Ames Optical Constants Facility enables determination of the aerosol analogs' complex refractive indices, n and k, from 0.59 to 200 μm [2]. Here we report efforts of determining n and k from ex-situ transmission measurements of solid samples produced from binary N-CH and Ar-CH, and tertiary N-CH-CH and Ar-CH-CHgas mixtures in COSmIC, and deposited onto various substrates. A computational technique [6] that addresses interference fringes observed in the laboratory transmission data, particularly at wavelengths < 3 μm, has been implemented and applied to determine n and k for the samples. At visible and near-infrared wavelengths(0.4-1.6 μm) the deposit thickness, and its variation, as well as n and k were determined by a commercial entity. These data provide the ability to compare results, from independent methods, in the region of overlap between the two approaches.

Ella M Sciamma-O'Brien↗

NASA NTRS2001

Thermal Electron Contributions to Current-Driven Instabilities: SCIFER Observations in the 1400-km Cleft Ion Fountain and Their Implications to Thermal Ion Energization

SCIFER TECHS observations of the variations in the thermal electron distribution in the 1400-km altitude cleft are associated with periods of intense ion heating and field-aligned currents. Energization of the thermal ion plasma in the mid-altitude cleft occurs within density cavities accompanied by enhanced thermal electron temperatures, large field-aligned thermal electron plasma flows and broadband low-frequency electric fields. Variations in the thermal electron contribution to field-aligned current densities indicate small scale (approximately 100's m) filamentary structure embedded within the ion energization periods. TECHS observations of the field-aligned drift velocities and temperatures of the thermal electron distribution are presented to evaluate the critical velocity thresholds necessary for the generation of electrostatic ion cyclotron and ion acoustic instabilities. This analysis suggests that, during periods of thermal ion energization, sufficient drift exists in the thermal electron distribution to excite the electrostatic ion cyclotron instability. In addition, brief periods exist within the same interval where the drift of the thermal electron distribution is sufficient to marginally excite the ion acoustic instability. In addition, the presence an enhancement in Langmuir emission at the plasma frequency at the center of the ion energization region, accompanied by the emission's second-harmonic, and collocated with observations of high-frequency electric field solitary structures suggest the presence of electron beam driven decay of Langmuir waves to ion acoustic modes as an additional free energy source for ion energization.

Adrian, Mark L.↗

NASA NTRS1993

Thermal spray forming of refractory sample ampoule cartridges for single crystal growth space furnaces

A thermal spray process is being used to build up refractory metals and ceramics into a containment cartridge for high temperature, single crystal semiconductor growth experiments. This process uses high energy plasma inside a low pressure (100-200 torr) inert environment to apply layers of material onto a removable mandrel. A variety of materials are being characterized and evaluated against a demanding set of requirements, including high service temperature (1700 C), oxidation resistance, and resistance to liquid metal attack. Techniques to spray form refractory metals (tungsten, molybdenum, niobium, tantalum) and ceramics (alumina, boron nitride) are being developed in the Plasma Spray Cell at Marshall Space Flight Center. These plasma spray formed materials have been evaluated for mechanical properties, density, microstructure, and resistance to liquid metal attack. Forming techniques and the resultant mechanical and metallurgical properties will be presented.

Zimmerman, Frank↗

NASA NTRS1993

Thermal spray forming of refractory sample ampoule cartridges for single crystal growth space furnaces

Zimmerman, Frank↗

DOE OSTI2023

A stable atmospheric-pressure plasma for extreme-temperature synthesis

Plasmas can generate ultra-high-temperature reactive environments that can be used for the synthesis and processing of a wide range of materials. However, the limited volume, instability and non-uniformity of plasmas have made it challenging to scalably manufacture bulk, high-temperature materials. Here we present a plasma set-up consisting of a pair of carbon-fibre-tip-enhanced electrodes that enable the generation of a uniform, ultra-high temperature and stable plasma (up to 8,000 K) at atmospheric pressure using a combination of vertically oriented long and short carbon fibres. The long carbon fibres initiate the plasma by micro-spark discharge at a low breakdown voltage, whereas the short carbon fibres coalesce the discharge into a volumetric and stable ultra-high-temperature plasma. As a proof of concept, we used this process to synthesize various extreme materials in seconds, including ultra-high-temperature ceramics (for example, hafnium carbonitride) and refractory metal alloys. Moreover, the carbon-fibre electrodes are highly flexible and can be shaped for various syntheses. In conclusion, this simple and practical plasma technology may help overcome the challenges in high-temperature synthesis and enable large-scale electrified plasma manufacturing powered by renewable electricity.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2022

In Situ Tracking of Nonthermal Plasma Etching of ZIF-8 Films

Surface characterization is critical for understanding the processes used for preparing catalysts, sorbents, and membranes. Nonthermal plasma (NTP) is a process that achieves high reactivity at low temperatures and is used to tailor the surface properties of materials. In this work, we combine the capabilities of infrared reflection absorption spectroscopy (IRRAS) with NTP for the in situ interrogation of zeolitic imidazolate framework-8 (ZIF-8) thin films to probe modifications in the material induced by oxygen and nitrogen plasmas. The IRRAS measurements in oxygen plasma reveal etching of organic ligands with sequential removal of the methyl group and imidazole ring and with the formation of carbonyl moieties (C═O). In contrast, nitrogen plasma induces mild etching and grafting of nitrile groups (−C≡N). Scanning electron microscopy imaging shows that oxygen plasma, at prolonged times, significantly degrades the ZIF-8 film at the grain boundaries. Treatment of ZIF-8 membranes using mild plasma conditions yields a fivefold enhancement for H 2 /N 2 and CO 2 /CH 4 ideal selectivities and an eightfold enhancement for CO 2 /N 2 ideal selectivity. Additionally, the new tools described here can be used for spectroscopic in situ tracking of plasma-induced chemistry on thin films in general.

IRRAS↗

DOE OSTI2021

Stimulated excitation of thermal diffusion waves in a magnetized plasma pressure filament

Results are presented from basic heat transport experiments using a magnetized electron temperature filament that behaves as a thermal resonator. Using a small cathode source, low energy electrons are injected along the magnetic field into the afterglow of a pre-existing plasma forming a hot electron filament embedded in a colder plasma. A series of low amplitude, sinusoidal perturbations are added to the cathode discharge bias that creates an oscillating heat source capable of driving large amplitude electron temperature oscillations. Langmuir probes are used to measure the amplitude and phase of the thermal wave field over a wide range of driver frequencies. The results are used to verify the excitation of thermal waves, confirm the presence of thermal resonances, and demonstrate the diagnostic potential of thermal waves through measurement of the parallel thermal diffusivity.

Karbashewski, S. (ORCID:000000034988492X)↗

NASA NTRS1984

Measurements of transition probabilities for spin-changing lines of atomic ions used in diagnostics of astrophysical plasmas

The intensities of ultraviolet, spin-changing, 'intersystem' lines of low-Z atomic ions are frequently used in determinations of electron densities and temperatures in astrophysical plasmas as well as in measurements of element abundances in the interstellar gas. The transition probabilities (A-values) of these lines, which are about five orders of magnitude weaker than allowed lines, have not been measured heretofore and various calculations produce A-values for these lines that differ by as much as 50 percent A radio-frequency ion trap has been used for the first measurements of transition probabilities for intersystem lines seen in astronomical spectra. The measurement procedure is discussed and results for Si III, O III, N II, and C III are reviewed and compared to calculated values. Discrepancies exist; these indicate that some of the calculated A-values may be less reliable than has been beleived and that revisions to the electron densities determined for some astrophysical plasmas may be required.

Smith, P. L.↗

NASA NTRS1979

Observations of warm plasma in the dayside plasma trough at geosynchronous orbit

Positive ions in the energy range E = 3-50 eV have been measured on the dayside at geosynchronous orbit with the University of California at San Diego auroral particles experiment on ATS 6. It is found that the near-equatorial plasma trough contains a warm plasma component with a relatively stable temperature 11 eV and a low 'isotropic component' of density typically in the range 0.1-0.4 ion/cc. The pitch angle distributions of these warm ions are typically field-aligned, indicating an ionospheric origin, and have pitch angle half widths in the range 20-40 deg. Pancake and conical distributions are also observed. Abrupt enhancements of the plasma density to 1-10 ions/cc, or more, are seen in the late afternoon and last from several minutes to a few hours.

Horwitz, J. L.↗

NASA NTRSDate not supplied

Indirect Magnetic Measurements on the Aerodynamic Heating Facility (AHF)

The arc jet complex at NASA Ames Research Center (ARC) investigates various thermal protection systems (TPS) and their performance in high enthalpy flow environments to improve heat shields used in atmospheric entry. The arc jet operates by inducing an arc between two electrodes and passing the heated gas through a supersonic nozzle. The arc plasma is typically a partially ionized air mixture at low temperature (< 2 eV) but operates for long periods of time (up to 30 min) at high power (< 60 MW). However, simulations using the in-house ARC Heater Simulator (ARCHeS) code predict that the arc is still unstable to MHD instabilities, primarily the kink instability, which limit the operational envelope of the facility [1]. Consequently, it is important to better characterize these instabilities to improve facility stability and extend operational ranges. Due to the high enthalpy and long timescales (i.e., minutes) arc diagnostics must be non-invasive (i.e., optical or magnetic). This work will cover the development of tri-axial magnetic hall sensors for arc jet instabilities and subsequent 3D characterization of arc motion. The latest results describing the kink instability amplitude, frequency and wavelength will be presented and represent the first measurements of this instability in a NASA arc jet facility. References: [1] Meurisse, J. (2018). 3D Unsteady Model of Arc Heater Plasma Flow Using the ARC Heater Simulator (ARCHeS), APS Gaseous Electronics Conference, 2018: APS.

Sebastian Vicente Colom↗

DOE OSTI2024

NSTX-U liquid metal core-edge facility (LMCE)

NSTX-U/LMCE will provide a unique and world-leading research facility to address the primary challenge to delivering economic and timely magnetic fusion energy, namely the need to develop a power and particle exhaust and first-wall system that can withstand very high edge heat fluxes, maximize energy confinement, and avoid the production of large masses of solid eroded first-wall material. The NSTX-U/LMCE facility will assess the ability of liquid metals (LMs) – especially liquid lithium – to provide a new boundary condition for magnetic fusion systems, to extend the lifetime of the plasma facing components (PFCs) and improve core plasma confinement. Such capability is needed to establish the basis for next-step fusion facilities including fusion pilot plants, and to maintain U.S. world leadership in core-edge integration research. NSTX-U/LMCE will leverage the ability to generate very high divertor perpendicular heat flux q⊥ ~ 100MW/m 2 , extensive diagnostics, and liquid-metal-applicable infrastructure of NSTX-U. NSTX-U/LMCE will provide access to a high-confinement plasma core with majority self-driven plasma current, the flexibility to test a range of liquid metal divertor concepts, access to a range of separatrix collisionalities (from high to very low), and the ability to controllably vary the first-wall temperature to vary the plasma- wall interaction physics on liquid lithium components. Further, NSTX-U/LMCE will utilize more reactor-relevant high-Z refractory-metal PFC substrates. With these capabilities the NSTX-U/LMCE facility will explore the full continuum of core-edge solutions ranging from high core radiated power, to conditions with radiative losses concentrated in the scrape-off layer (SOL), and ultimately low recycling conditions. The low collisionality SOL that may be accessible in the low recycling regime is relatively unexplored and will require a kinetic treatment of the edge, which can be addressed theoretically, and with experiments in LTX-β. Additional smaller-scale preparatory R&D facilities will be required to reduce the risk of premature technical/engineering failure of liquid metal systems implemented in NSTX-U. The NSTX-U/LMCE facility aligns very well with recommendations in the FESAC Long-Range Plan and NASEM Pilot Plant reports and the Bold Decadal Vision, will be unique in the world program throughout the next decade, and is garnering private company interest in utilizing NSTX-U/LMCE for development of LM PFCs.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗