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At least 451 records · Page 25

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DOE OSTI2025

Mixed Element Microparticle Characterization by Electron Probe Microanalysis

Abstract Microparticle compositional characterization for nuclear forensics has traditionally been achieved by “gold-standard” destructive analytical techniques such as large geometry-secondary ion mass spectrometry and fission track-thermal ionization mass spectrometry, but long processing times and total sample consumption eliminate the option of subsequent analysis by other methods. Electron probe microanalysis has long been widely employed for rapid, nondestructive, micrometer-scale compositional measurements and imaging in fields such as material science and geology and may therefore need to be reevaluated as an alternative tool for microparticle analysis for the nuclear forensics community. This study presents the use of electron probe microanalysis for imaging and quantitative characterization of homogeneous microparticles utilizing a calibration curve based on high-precision quadrupole-inductively coupled plasma-mass spectrometry analyses. Samples of opportunity synthesized at Savannah River National Laboratory, nickel-doped cerium oxide microparticles, were selected as analogs for plutonium-doped uranium oxide microparticles. Positive detection and accurate quantification of variable amounts of nickel dopant down to trace levels (10s of parts per million) suggest applicability of this technique to other mixed element systems (e.g., actinides). Quantitative single-particle characterization via electron probe microanalyzer may thus provide a high fidelity, nondestructive complement to techniques currently in use.

Riche, Alexis T. (ORCID:0009000121978126)↗

DOE OSTI2025

Strategies for preparing and analyzing thin passive films with atom probe tomography

Atom probe tomography provides a unique, three-dimensional map of elemental and isotopic distributions over a wide range of materials with near-atomic scale resolution and is particularly strong at analyzing buried interfaces within materials. However, it is much more difficult to apply atom probe to the analysis of nanoscale surface films, such as those formed during alloy passivation, where unique challenges persist for sample preparation and data collection. Here, we present sample preparation strategies involving the deposition of a < 100 nm capping layer that enables reliable characterization of thin passive films approximately 2–5 nm thick formed on binary and multi-principal element alloys via atom probe tomography. Several capping layer materials (Pt, Ti, Ni/Cr bi-layer) and deposition methods are contrasted. Our results indicate a sputtered Ni/Cr bi-layer enables the characterization of the entire passive film and concentration profiles that can easily be interpreted to clearly distinguish base alloy/passive film/capping layer interfaces. Lastly, we highlight ongoing challenges and opportunities for this experimental approach.

Kautz, Elizabeth J. [University of Florida]↗

DOE OSTI2025

Cosmic-ray cooling in active galactic nuclei as a new probe of inelastic dark matter

We present a novel way to probe inelastic dark matter using cosmic-ray (CR) cooling in active galactic nuclei (AGNs). Dark matter (DM) in the vicinity of supermassive black holes may scatter off CRs, resulting in the rapid cooling of CRs for sufficiently large cross sections. This in turn can alter the high-energy neutrino and gamma-ray fluxes detected from these sources. We show that AGN cooling bounds obtained through the multimessenger data of NGC 1068 and TXS 0506 + 056 allows us to reach unprecedently large mass splittings for inelastic DM (≳ TeV), orders of magnitude larger than those probed by direct detection experiments and DM capture in neutron stars. Furthermore, we demonstrate that cooling bounds from AGNs can probe thermal light DM with small mass splittings. This provides novel and complementary constraints in parts of a parameter space accessible solely by colliders and beam-dump experiments.

astronomical black holes↗

DOE OSTI2026

Jet charge with global event shapes: Probing quark flavor dynamics

We propose measuring the jet electric charge of jet regions, defined within the framework of global event shapes, as a probe of quark flavor dynamics within the nucleon and the hadronization process. In particular, we consider a measurement of the jet region charge while simultaneously keeping track of the energy flow throughout the event, as characterized by the global event shape. As a concrete example, we focus on the measurement of the (Q), the jet charge of the jet region (𝐽) defined within the framework of the 1-Jettiness global event shape (𝜏 1 ) for the Deep Inelastic Scattering (DIS) process, 𝑒 − +𝑝→𝑒 − +𝐽+𝑋, with unpolarized or longitudinally polarized protons. The 1-Jettiness distribution, binned according to jet charge, allows for enhanced quark flavor separation of the initial state unpolarized or polarized PDFs. On the other hand, the jet charge distribution binned by 1-Jettiness can serve as a probe of quark flavor dynamics in the final state hadronization process. We derive a factorization theorem for simultaneous measurements of 𝜏 1 and Q in the resummation region, 𝜏 1 ≪𝑃 𝐽 𝑇 , where 𝑃 𝐽 𝑇 denotes the transverse momentum of the jet region. The correlation between the jet region charge and the charge of the struck quark is expected to be the strongest in the resummation region. The factorization theorem contains a new universal , generalizing the standard jet function to include a jet charge measurement. Therefore these universal functions can be extracted from a global analysis of N-jettiness and thrust at 𝑒 + ⁢𝑒 − colliders. We provide simulation studies to demonstrate the sensitivity of the 1-Jettiness jet charge observable to quark flavor dynamics in nucleon structure and explore the possibility of probing the final state hadronization process. This observable is well-suited for applications with existing HERA data and the future Electron-Ion Collider (EIC).

Mantry, Sonny [University of North Georgia, Dahlon↗

DOE OSTI2025

Pump with Broadband Probe Experiments for Single-Shot Measurements of Plasma Conditions and Crossed-Beam Energy Transfer

Here, a novel technique for measuring plasma conditions using monochromatic pump-broadband-probe laser interactions has been experimentally demonstrated. Originally proposed in Ludwig et al. [Phys. Plasmas 26, 113108 (2019)], this method utilizes crossed-beam energy transfer between the broadband probe and the pump, mediated by plasma ion acoustic waves. The complete energy transfer spectrum can be captured in a single shot, enabling the inference of plasma parameters such as density, electron and ion temperatures, and flow velocity. Compared to Thomson scattering, this technique offers signal enhancements typically larger than 9 orders of magnitude, significantly reducing the required probe laser intensity and facilitating interactions that are linear and measurements that are nonperturbative of the plasma. Furthermore, it provides a powerful tool for advancing studies of crossed-beam energy transfer under conditions relevant to inertial confinement fusion experiments.

Physics - Plasma physics↗

DOE OSTI2026

Nanoscale Defects as Probes of Time-Reversal Symmetry Breaking

Nanoscale defects such as nitrogen-vacancy (NV) centers can serve as sensitive and noninvasive probes of electromagnetic fields and fluctuations from materials, which in turn can be used to characterize these systems. Here we specifically discuss how NV centers can probe time-reversal symmetry breaking (TRSB) phenomena in low-dimensional electronic systems. We argue that the difference in relaxation rates Γ$_{±\hat{z}}$ of NV centers starting from 𝑚 = ±1 spin states to the ground state with 𝑚 = 0 directly probes TRSB. The effect arises from the difference in the fluctuation spectrum of left- and right-polarized electromagnetic fields emanating from such materials. In the quantum Hall setting, the NV center experiences (nearly zero) large additional contribution to its relaxation due to the presence of the material when its magnetic dipole (anti)aligns with the external field. More generally, the difference in the relaxation rates is sensitive to the imaginary part of the wave-vector-dependent Hall conductivity. We argue that this can be used to determine the Hall viscosity, which can potentially distinguish candidate fractional quantum Hall states and be used to infer the pairing angular momentum in TRSB superconductors. We compute the average relaxation rate [Γ$_{+\hat{z}}$ + Γ$_{-\hat{z}}$] near thin film superconductors and find that it exhibits a Hebel-Slichter-like enhancement below 𝑇 𝑐 . The difference Γ$_{+\hat{z}}$ −Γ$_{-\hat{z}}$ also inherits this peak but is only nonzero for 𝑇 < 𝑇 𝑐 and only if the superconductivity is chiral. We provide concrete estimates for observing this effect in stacked twisted bismuth strontium calcium copper oxide flakes.

NV centers↗

DOE OSTI2024

Probing Majorana Wave Functions in Kitaev Honeycomb Spin Liquids with Second-Order Two-Dimensional Spectroscopy

Two-dimensional coherent terahertz spectroscopy (2DCS) emerges as a valuable tool to probe the nature, couplings, and lifetimes of excitations in quantum materials. It thus promises to identify unique signatures of spin liquid states in quantum magnets by directly probing properties of their exotic fractionalized excitations. Here, in this study, we calculate the second-order 2DCS of the Kitaev honeycomb model and demonstrate that distinct spin liquid fingerprints appear already in this lowest-order nonlinear response $\chi^{(2)}_{yzx}$⁡($ω_1$, $ω_2$) when using crossed light polarizations. We further relate the off-diagonal 2DCS peaks to the localized nature of the matter Majorana excitations trapped by $\mathbb{Z}_2$ flux excitations and show that 2DCS thus directly probes the inverse participation ratio of Majorana wave functions. By providing experimentally observable features of spin liquid states in the 2D spectrum, our Letter can guide future 2DCS experiments on Kitaev magnets.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2025

Probing Curved Spacetime with a Distributed Atomic Processor Clock

Quantum dynamics on curved spacetime has never been directly probed beyond the Newtonian limit. Although we can describe such dynamics theoretically, experiments would provide empirical evidence that quantum theory holds even in this extreme limit. The practical challenge is the minute spacetime curvature difference over the length scale of the typical extent of quantum effects. Here, we propose a quantum network of alkaline earth (like) atomic processors for constructing a distributed quantum state that is sensitive to the differential proper time between its constituent atomic processor nodes, implementing a quantum observable that is affected by post-Newtonian curved spacetime. Conceptually, we propose to delocalize one clock between three locations by encoding the presence or absence of a clock into the state of the local atoms. By separating three atomic nodes over approximately kilometer-scale elevation differences and distributing one clock between them via a 𝑊 state, we demonstrate that the curvature of spacetime is manifest in the interference of the three different proper times that give rise to three distinct beat notes in our nonlocal observable. We further demonstrate that 𝑁-atom entanglement within each node enhances the interrogation bandwidth by a factor of 𝑁. We discuss how our proposed system can probe new facets of fundamental physics, such as the linearity, unitarity, and probabilistic nature of quantum theory on curved spacetime. Our protocol combines several recent advances with neutral atom and trapped ions to realize a novel quantum probe of gravity uniquely enabled by quantum networks.

Covey, Jacob P. [Univ. of Illinois at Urbana-Champ↗

DOE OSTI2025

Probing Gluon Fluctuations in Nuclei with the First Energy-Dependent Measurement of Incoherent 𝐽/𝜓 Photoproduction in Ultraperipheral PbPb Collisions

Incoherent 𝐽/𝜓 photoproduction in heavy ion ultraperipheral collisions (UPCs) provides a sensitive probe of localized, fluctuating gluonic structures within heavy nuclei. This Letter reports the first measurement of the photon-nucleon center-of-mass energy (𝑊 𝛾⁢N ) dependence of this process in PbPb UPCs at a nucleon-nucleon center-of-mass energy of 5.02 TeV, using 1.52 nb −1 of data recorded by the CMS experiment. The measurement covers a wide 𝑊 𝛾⁢N range of ≈40–400 GeV, probing gluons carrying a fraction 𝑥 of nucleon momentum down to an unexplored regime of 6.5 ×10 −5 . Compared to baseline predictions neglecting nuclear effects, the measured cross sections exhibit significantly greater suppression at lower 𝑥. Additionally, the ratio of incoherent to coherent photoproduction is found to be constant across the probed 𝑊 𝛾⁢N and 𝑥 range, disfavoring the establishment of the black disk limit. This Letter provides critical insights into the 𝑥-dependent evolution of fluctuating gluonic structures within nuclei and calls for further advancements in theoretical models incorporating nuclear shadowing and gluon saturation.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2026

Dark-matter-enhanced probe of relic neutrino clustering

We propose heavy decaying dark matter (DM) as a new probe of the cosmic neutrino background (C⁢𝜈⁢B). Heavy DM, with mass ≳ 10 9 GeV, decaying into neutrinos can be a new source of ultrahigh-energy (UHE) neutrinos. Including this contribution along with the measured astrophysical and predicted cosmogenic neutrino fluxes, we study the scattering of UHE neutrinos with the C⁢𝜈⁢B via standard weak interactions mediated by the 𝑍 boson. We solve the complete neutrino transport equation, taking into account both absorption and reinjection effects, to calculate the expected spectrum of UHE neutrino flux at future neutrino telescopes, such as the IceCube-Gen2 radio. We argue that such observations can be used to probe the C⁢𝜈⁢B properties and, in particular, local C⁢𝜈⁢B clustering. We find that, depending on the absolute neutrino mass and the DM mass and lifetime, a local C⁢𝜈⁢B overdensity ≳ 10 6 can be probed at the IceCube-Gen2 radio within ten years of data taking.

Dark matter↗

DOE OSTI2025

Integral Field Probe for Mapping of Curved Magnets

The Single Stretched Wire (SSW) method allows highly precise integral field measurements by recording voltage across a tensioned wire mounted to 2-axis linear stages at either end of the magnet aperture. However, traditional SSW probes are not well suited for curved accelerator magnets, which are essential for steering charged particles along arced trajectories in storage rings or beamlines. The tension required to eliminate sag demands a purely straight path, making them incompatible with non-linear magnet geometries. To address this limitation for curved magnets, a modified approach was developed using a segmented, 3D-printed support structure that incorporates a pre-shaped anti-sag curve. Under its own weight and that of the wire bundle, the structure deforms to lie flat while conforming to the curvature of the magnet in the horizontal plane. The optimal geometry of the probe was derived using an iterative process combining FEA simulations in Ansys Mechanical with testing of various carbon fiber-reinforced filaments. The printed and assembled probe was successfully used to measure the SDD-059 magnet at Fermilab, yielding promising results.

Jakopin, Alexander [Northern Illinois U.]↗

DOE OSTI2025

Insights into the hydro-mechanical behavior of a decimeter-scale fracture using the mini-SIMFIP probe

ABSTRACT: Understanding hydro-mechanical couplings in fractured rocks is essential for predicting the rock mass response during high-pressure fluid injection, including the stimulation of enhanced geothermal systems. However, fluid-driven fracture dislocations are challenging to measure due to the need for local displacement data at high fluid pressures. In this study, fluid-driven displacement across a decimeter-scale laboratory fracture was investigated using the mini-SIMFIP (step rate injection method for fracture in-situ properties) probe, which is a smaller version of the SIMFIP tool (Guglielmi et al., 2014). The mini-SIMFIP probe is able to resolve the full 3D displacement vector of a fracture. The probe was installed in one of two boreholes across a decimeter-scale saw-cut granite fracture. Two pressure step injection tests were conducted under the same isotropic stress conditions. By varying injection between the boreholes, we estimated the aperture profile across the fracture. The results show a consistent pressure-dependent opening as long as steady-state flow was maintained. At a certain pressure step, steady-state conditions were no longer achievable and the fracture opened rapidly. The pressure-opening relationship diverged between the two tests and indicated a homogenization of the aperture profile and an increase in the non-linearity of the flow regime.

Osten, J↗

NASA NTRS1967

Movable RF probe eliminates need for calibration in plasma accelerators

Movable RF antenna probe in plasma accelerators continuously maps the RF field both within and beyond the accelerator. It eliminates the need for installing probes in the accelerator walls. The moving RF probe can be used to map the RF electrical field under various accelerator conditions.

Miller, D. B.↗

NASA NTRS1968

Vacuum probe sampler removes micron-sized particles from surfaces

Vacuum probe sampler removes micron-sized particles from sensitive surfaces, without damage to the surface. The probe has a critical orifice to ensure an optimum airflow rate that disturbs the boundary layer of air and raises bacteria from the surface into the probe with the moving air stream.

Whitfield, W. J.↗

NASA NTRS1969

Concept for a multifunctional oscilloscope probe

Multifunctional oscilloscope probe incorporates required electronic components so that any one of three desired functions /direct, demodulation, or low capitance/ can be switched into the oscilloscope. The probe obviates the need for the three seperate oscilloscope probes previously used in checking electronic equipment.

Stringer, E. J.↗

NASA NTRS1971

Dynamics of short pressure probes

Report presents practical information for incorporating particle impact protection features and average total pressure measurement into probe design while optimizing probe transient response. Computer program calculates probe response, based on Bergh-Tijdeman equation.

Englund, D. R.↗

NASA NTRS1971

Apollo 14 mission: Failure to achieve docking probe capture latch engagement

Six docking attempts were required in order to successfully achieve capture latch engagement during the transposition and docking phase following translunar injection. After docking, the probe and drogue were examined by the crew. Probe operation appeared normal and radial marks were noted on the drogue. During all subsequent operations, the probe operated properly.

Source record↗

NASA NTRS1972

Systems-level study of a nonsurvivable Jupiter turbopause probe. Volume 1: Summary

The design of a space probe to explore the atmosphere of the planet Jupiter is discussed. Five major areas were considered: (1) definition of science requirements, (2) mission evaluation, (3) definition of probe system, (4) definition of spacecraft support requirements, and (5) nonequilibrium flow field analysis for communications blackout evaluation. The overall mission and system design are emphasized. The integration of the various technologies into complete systems designs is described. Results showed that a nonsurvivable turbopause probe mission to Jupiter with adequate data return to meet the science objectives is feasible and practical.

Wiltshire, R. S.↗