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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 469 records · Page 26

Analyzing the effect of misalignment on single-filament carbon fiber tensile testing via stereoscopic computer vision imaging

An understanding of the constitutive properties of carbon fibers (CF) is critical to the accuracy of high-resolution composite simulations and to the development of CF derived from low-cost alternative precursor materials. Single-fiber tensile testing is a capable tool to measure CF properties and is well suited to research efforts where only a small number of fibers may be available. However, single-fiber tensile tests are challenging to conduct due to the difficulty in handling small diameter fibers (5-15 μm), the brittleness of single fibers, and the required nanoscale/microscale resolution of testing equipment. The accuracy of the measured properties depends on several factors, but a critical factor is fiber misalignment, especially at short gauge lengths. Current standards do not address the effect of tensile specimen misalignment on measured properties. Furthermore, this work presents a robust method of fiber alignment using stereoscopic computer vision that enables users to align fibers vertically for tensile testing to improve the accuracy of resulting mechanical properties. Additionally, an analytical relationship between fiber misalignment angle and measured properties is developed and validated against the experimental results. As a result, new best practices for single-fiber tensile testing of CF are recommended.

47 OTHER INSTRUMENTATION↗

An Assessment of the Usability of Machine Learning Based Tools for the Security Operations Center

Gartner, a large research and advisory company, anticipates that by 2024 80% of security operation centers (SOCs) will use machine learning (ML) based solutions to enhance their operations. 1 1 https://www.ciodive.com/news/how-data-science-tools-can-lighten-the-load-for-cybersecurity-teams/572209/ In light of such widespread adoption, it is vital for the research community to identify and address usability concerns. This work presents the results of the first in situ usability assessment of ML-based tools. With the support of the US Navy, we leveraged the national cyber range-a large, air-gapped cyber testbed equipped with state-of-the-art network and user emulation capabilities-to study six US Naval SOC analysts' usage of two tools. Our analysis identified several serious usability issues, including multiple violations of established usability heuristics for user interface design. We also discovered that analysts lacked a clear mental model of how these tools generate scores, resulting in mistrust a and/or misuse of the tools themselves. Surprisingly, we found no correlation between analysts' level of education or years of experience and their performance with either tool, suggesting that other factors such as prior background knowledge or personality play a significant role in ML-based tool usage. Our findings demonstrate that ML-based security tool vendors must put a renewed focus on working with analysts, both experienced and inexperienced, to ensure that their systems are usable and useful in real-world security operations settings.

Oesch, T↗

Energy gain scale calibration of the XRISM Resolve microcalorimeter spectrometer: ground calibration results and on-orbit comparison

The Resolve instrument aboard the X-ray Imaging and Spectroscopy Mission (XRISM) is a 36-pixel microcalorimeter spectrometer that provides nondispersive spectroscopy with ∼ 5 eV spectral resolution in the soft X-ray waveband. Resolve has a requirement to provide an absolute energy-scale calibration of ± 2 eV from 0.3 to 12 keV. We describe our ground calibration strategy and results of a subset of the ground calibration campaigns, including a discussion of improvements in the energy scale ground calibration compared with Hitomi’s. These improvements include calibration of the low-energy band below 4 keV with the instrument in the flight dewar and the dewar aperture door open, which was not performed for Hitomi, and thorough measurements over an extended high-energy waveband to 22 keV. We also developed an improved technique for gain calibration of “mid-res” secondary events, which have suppressed gain due to proximity to a preceding X-ray event (18 to 70 ms) on the same pixel. We provide a discussion of the on-orbit energy scale monitoring campaigns and an assessment of the Resolve energy scale uncertainties, a key parameter for astrophysics analysis. Energy-scale calibration approaches for future space-based instruments, including the X-ray Integral Field Unit on Athena and microcalorimeter spectrometers proposed or under discussion for future X-ray observatory concepts, have heritage in the calibration of XRISM. We briefly comment on lessons learned from Resolve calibration that are relevant for these future instruments.

Aluminum↗

Evaluation of coupled wind-wave model simulations of offshore winds in the Mid-Atlantic Bight using lidar-equipped buoys.

From 2014 to 2017, two Department of Energy buoys equipped with Doppler lidar were deployed off the U.S. East Coast to provide long term measurements of hub-height wind speed in the marine environment. In this study, we performed simulations of selected cases from the deployment using a 5-km configuration of the Weather Research and Forecasting (WRF) model, to see if simulated hub height speeds could produce closer agreement with the observations than existing reanalysis products. For each case we performed two additional simulations: one in which marine surface roughness height was one-way coupled to forecast wave parameters from a standalone WaveWatch III (WW3) simulation, and another in which WRF and WW3 were two-way coupled using the Coupled-Ocean-Atmosphere-Wave-Sediment-Transport (COAWST) framework. It was found that all the 5-km WRF simulations improved 90-m wind speed statistics for the tropical cyclone case of 08 May 2015 and the cold frontal case of 25 Mar 2016, but not the nor-easter of 18 Jan 2016. The impact of wave coupling on buoy-level (4 m) wind speed was modest and case dependent, but when present, the impact was typically seen at 90 m as well, being as large as 10% in stable conditions. One-way wave coupling consistently reduced wind speeds, improving biases for 25 Mar 2016 but worsening them for 08 May 2015. Two-way wave coupling mitigated these negative biases, improved wave field representation and statistics, and mostly improved 4-m wind field correlation coefficients, at least at the VA buoy, largely due to greater self-consistency between wind and wave fields.

54 ENVIRONMENTAL SCIENCES↗

Experimental Investigation on Heating Performance of a Cold Climate Thermoelectric-Assisted Heat Pump

To accelerate the electrification of air source heat pumps (ASHPs) in cold climates across the United States, various initiatives have been launched to enhance the effectiveness of ASHPs. One avenue of research involves incorporating thermoelectric (TE) technology into vapor compression refrigeration cycles. This study aims to assess the heating performance of a cold climate ASHP by employing TE modules as a liquid line subcooler. The tested system is a nominal 4.5-ton split heat pump utilizing R410A, equipped with a scroll compressor and an accumulator. An electronic expansion valve was employed for both cooling and heating modes. Two configurations of TE sub-coolers, one utilizing 2 TE bundles and the other 4 TE bundles, were integrated into the liquid line of the tested system. The heating performance of these configurations was evaluated. The results revealed that activating the TE subcooler led to a notable increase in total heat capacity, reaching 1318 W at -15.0 °C and 1164 W at -19.0 °C. The corresponding TE coefficients of performance (COPs) were 1.76 and 1.63, respectively. The activation of the TE sub-cooler resulted in a slight reduction in the overall system COP, with a decrease ranging from -2.6% to -4.2% for these two temperatures. The system COPs were measured at 2.10 and 1.86 for -15.0 °C and -19.0 °C, respectively. This prototype demonstrated a significant augmentation in heating capacity with a minimal sacrifice in COP.

Hu, Yifeng↗

Modeled Results of Four Residential Energy Efficiency Measure Packages for Deriving Advanced Building Construction Research Targets

The Advanced Building Construction (ABC) Initiative from the U.S. Department of Energy Building Technologies Office is working to accelerate industrialized construction innovations for decarbonizing buildings. To inform performance and cost targets for research under the ABC Initiative, this analysis used the ResStock™ tool to evaluate the energy savings, utility bill impacts, and carbon emissions impacts of four simulated upgrade packages with specific target performance levels on a large sample of residential dwelling units (approximately 550,000) representative of the U.S. housing stock.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

Enzymatic Laser-Induced Graphene Biosensor for Electrochemical Sensing of the Herbicide Glyphosate

Glyphosate is a globally applied herbicide yet it has been relatively undetectable in-field samples outside of gold-standard techniques. Its presumed nontoxicity toward humans has been contested by the International Agency for Research on Cancer, while it has been detected in farmers’ urine, surface waters and crop residues. Rapid, on-site detection of glyphosate is hindered by lack of field-deployable and easy-to-use sensors that circumvent sample transportation to limited laboratories that possess the equipment needed for detection. Herein, the flavoenzyme, glycine oxidase, immobilized on platinum-decorated laser-induced graphene (LIG) is used for selective detection of glyphosate as it is a substrate for GlyOx. The LIG platform provides a scaffold for enzyme attachment while maintaining the electronic and surface properties of graphene. The sensor exhibits a linear range of 10–260 µm, detection limit of 3.03 µm, and sensitivity of 0.991 nA µm -1 . The sensor shows minimal interference from the commonly used herbicides and insecticides: atrazine, 2,4-dichlorophenoxyacetic acid, dicamba, parathion-methyl, paraoxon-methyl, malathion, chlorpyrifos, thiamethoxam, clothianidin, and imidacloprid. Sensor function is further tested in complex river water and crop residue fluids, which validate this platform as a scalable, direct-write, and selective method of glyphosate detection for herbicide mapping and food analysis.

47 OTHER INSTRUMENTATION↗

Implementation and validation of optimal start control strategy for air conditioners and heat pumps

Commercial buildings are responsible for approximately 20 % of the total energy consumption and greenhouse gas emissions in the United States. Over 85 % of these buildings lack building automation systems, and many are small (<50,000 square feet), underserved, and use rooftop units (RTUs) for heating, ventilation, and air-conditioning needs. Because these buildings lack proper energy management systems, several operational deficiencies lead to excess energy consumption. Studies have shown that managing the RTUs’ heating and cooling set points, schedules, setbacks, and optimal start can result in a 20 % to 25 % reduction in electricity consumption in small commercial buildings. These buildings typically use fixed schedules to start the RTUs 60 to 120 min before occupancy begins, which results in excess energy consumption. This paper presents research that demonstrates and evaluates the performance of four optimal start methods, which utilize data-based modeling as a key element in facilitating adaptive control in response to time-varying inputs while requiring minimal sensor inputs. The evaluation found energy savings in two commercial buildings equipped with RTUs by periodically alternating four different optimal start models during the cooling and heating season. The resulting energy savings are positive for all models and range from 2 to 5 kWh/day/unit. The units on the east side of the building showed higher savings, while interior units showed greater variability in savings due to the differences in capacities and room sizes. Savings were considerably greater during the heating season compared to the cooling season. The performance of all four models on Mondays was poor; models suggested a shorter optimal start time, which resulted in relatively larger errors. Finally, the future work will look at using a different model for the days after weekends and holidays.

42 ENGINEERING↗

Expanding the application of a UV-visible reporter for transient gene expression and stable transformation in plants

Abstract Green fluorescent protein (GFP) has been widely used for monitoring gene expression and protein localization in diverse organisms. However, highly sensitive imaging equipment, like fluorescence microscope, is usually required for the visualization of GFP, limitings its application to fixed locations in samples. A reporter that can be visualized in real-time regardless the shape, size and location of the target samples will increase the flexibility and efficiency of research work. Here, we report the application of a GFP-like protein, called eYGFPuv, in both transient expression and stable transformation, in two herbaceous plant species ( Arabidopsis and tobacco) and two woody plant species (poplar and citrus). We observed bright fluorescence under UV light in all of the four plant species without any effects on plant growth or development. eYGFPuv was shown to be effective for imaging transient expression in leaf and root tissues. With a focus on in vitro transformation, we demonstrated that the transgenic events expressing 1x eYGFPuv could be easily identified visually during the callus stage and the shoot stage, enabling early and efficient selection of transformants. Furthermore, whole-plant level visualization of eYGFPuv revealed its ubiquitous stability in transgenic plants. In addition, our transformation experiments showed that eYGFPuv can also be used to select transgenic plants without antibiotics. This work demonstrates the feasibility of utilizing 1x eYGFPuv in studies of gene expression and plant transformation in diverse plants.

59 BASIC BIOLOGICAL SCIENCES↗

First Experiments: New Science Opportunities at the Spallation Neutron Source Second Target Station (abridged)

This brochure is an abridged version of a more comprehensive companion report. DOE proposes to build a Second Target Station (STS) at SNS to produce beams of cold neutrons with world-leading peak brightness at a repetition rate of 15 Hz, providing broad energy/wavelength ranges that can be used simultaneously. Construction of the STS will provide transformative capabilities that allow thousands of users from national laboratories, universities, and industry to address grand scientific challenges [Hemminger 2015], advance energy research, and accelerate industrial innovations through the combination of cold (long-wavelength) neutrons of unprecedented peak brightness and short neutron pulses with broad ranges of usable wavelengths or energy. The STS Project, now in progress at ORNL, will design, construct, install, and commission the facilities and equipment needed to create a world-leading source of cold neutrons of unprecedented peak brightness at SNS. Key aspects of the STS design, including preliminary descriptions of an illustrative suite of eight instruments, are presented in the section “The STS at SNS.” The capabilities offered by the STS instruments (22 when fully built out) will complement those of the FTS and HFIR, providing the United States with unparalleled resources for neutron scattering at the world’s leading high–peak brightness cold neutron source.

43 PARTICLE ACCELERATORS↗

Construction Methodology Transformation for the Benefit of Workforce Development

Construction is a key economic engine driving both national and global economies. While manual, onsite construction methods dominate the U.S. construction industry, a major shift towards offsite methods has been underway due to its efficiency, speed, and potential cost savings. The workforce necessary for offsite construction growth does not exist in its current form because of the focus on onsite methodologies and the lack of exposure to offsite building methods at all levels of a student’s learning journey. The growth of the U.S. construction industry and competitiveness in an increasingly global construction market over the coming decades can only be supported by a dramatic increase in the use of offsite methods, which requires ramping up workforce training for certain skillsets. The goal of Construction Methodology Transformation for the Benefit of Workforce Development was to understand the opportunities and barriers in both education and industry and to identify best practices for offering curriculum and training to educators, industry, and students that would support skills needed for careers in offsite construction. Our team proposed combining three offsite construction workforce development needs: content development, exposure and training, and job placement - under a single Platform model that would increase experience and career opportunities for students and help match them with potential industry members. Through our proposed solution we expected to see: developed offsite curriculum being utilized by educators and students; an increase in the identification of construction technology and offsite construction methods; an average increase in knowledge gain of at least 25% after participation in pilots; better equipped candidates who are prepared for jobs in offsite construction; and a beta workforce development platform that helps build more pathways for students looking for careers in offsite construction. The two pilots included almost 250 students and resulted in an average knowledge gain of 37 percent. Our research has identified areas of opportunity, for both education and industry to make collaborative training programs more efficient and successful. The chosen techniques for this program are extremely effective when both the school and factory have solid processes and cultures in place to accept students into training programs. This project serves as an important stepping stone to industrywide collaboration to move workforce development for offsite construction forward across the country. With continued collaboration programs like this can provide much needed early exposure and training in offsite construction and we can begin to fill important positions for the future of construction.

99 GENERAL AND MISCELLANEOUS↗

Recent advances in nano-scale spatial resolution x-ray microscopy instrumentation at NSLS-II

X-ray microscopy is an invaluable and powerful characterization tool applied in many scientific fields, such as materials science, biology, environmental science, and energy research. In recent years it has been driven by rapid developments of novel technologies and systems resulting in imaging experiments elucidating structural inhomogeneities and chemical reactions at the nanometer scale. To obtain high spatial resolution comprehensive chemical and structural information, an X-ray microscope must be equipped with adequate capabilities and allow for simultaneous acquisition of multiple datasets. In recent years, a number of X-ray microscopes have been designed, constructed, and commissioned at NSLS-II. Here we provide an overview of the microscopy instrumentation development program at NSLS-II and specifically focus on the multilayer Laue lens-based hard X-ray nanoprobe optimized for ~10 nm spatial resolution imaging, its current status, and future upgrades along with recently constructed Kirkpatrick-Baez based scanning microscope designed for ~100 nm spatial resolution experiments.

36 MATERIALS SCIENCE↗

Use of Sensors and Machine Learning for Signal Discovery in a Solvent Extraction Process – 23280

Reprocessing is an important step in the nuclear fuel cycle where usable nuclear materials are extracted from spent fuel for recycling. The extraction of materials for reuse simultaneously reduces not only the volume of nuclear waste, but its decay time to radioactivity levels similar to that of the originating uranium ore. As part of an initiative to steward research, development, and innovation into the nuclear fuel cycle, Idaho National Laboratory is designing and constructing a solvent extraction testbed named Beartooth. Beartooth will allow researchers to refine extraction processes, test innovative extraction processes, and give early career scientists opportunities to gain skills in performing separations chemistry that uses centrifugal contactors. In addition, the Beartooth testbed is being uniquely designed to enable novel technologies including machine learning capabilities for the characterization of chemical process operations in near real-time. To aid in the design of Beartooth, a team of researchers are installing a variety of atypical sensors into a system of contactors for signal discovery. The team will implement machine learning methods on sensor data to determine signal features with the goal of providing a process operator with a deeper understanding of the chemical process and equipment usage. This work will summarize sensors utilized and preliminary results from an infrared camera.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Real-Time Coupling of Geographically Distributed Research Infrastructures: Taxonomy, Overview, and Real-World Smart Grid Applications

Novel concepts enabling a resilient future power system and their subsequent experimental evaluation are experiencing a steadily growing challenge: large scale complexity and questionable scalability. The requirements on a research infrastructure (RI) to cope with the trends of such a dynamic system therefore grow in size, diversity and costs, making the feasibility of rigorous advancements questionable by a single RI. Analysis of large scale system complexity has been made possible by the real-time coupling of geographically separated RIs undertaking geographically distributed simulations (GDS), the concept of which brings the equipment, models and expertise of independent RIs, in combination, to optimally address the challenge. This article presents the outputs of IEEE PES Task Force on Interfacing Techniques for Simulation Tools towards standardization of GDS as a concept. First, the taxonomy for setups utilized for GDS is established followed by a comprehensive overview of the advancements in real-time couplings reported in literature. The overview encompasses fundamental technological design considerations for GDS. The article further presents four application oriented case studies (real-world implementations) where GDS setups have been utilized, demonstrating their practicality and potential in enabling the analysis of future complex power systems.

distributed laboratories↗

A frugal CRISPR kit for equitable and accessible education in gene editing and synthetic biology

Equitable and accessible education in life sciences, bioengineering, and synthetic biology is crucial for training the next generation of scientists, fostering transparency in public decision-making, and ensuring biotechnology can benefit a wide-ranging population. As a groundbreaking technology for genome engineering, CRISPR has transformed research and therapeutics. However, hands-on exposure to this technology in educational settings remains limited due to the extensive resources required for CRISPR experiments. Here, we develop CRISPRkit, an affordable kit designed for gene editing and regulation in high school education. CRISPRkit eliminates the need for specialized equipment, prioritizes biosafety, and utilizes cost-effective reagents. By integrating CRISPRi gene regulation, colorful chromoproteins, cell-free transcription-translation systems, smartphone-based quantification, and an in-house automated algorithm (CRISPectra), our kit offers an inexpensive (~$2) and user-friendly approach to performing and analyzing CRISPR experiments, without the need for a traditional laboratory setup. Experiments conducted by high school students in classroom settings highlight the kit’s utility for reliable CRISPRkit experiments. Furthermore, CRISPRkit provides a modular and expandable platform for genome engineering, and we demonstrate its applications for controlling fluorescent proteins and metabolic pathways such as melanin production. We envision CRISPRkit will facilitate biotechnology education for communities of diverse socioeconomic and geographic backgrounds.

59 BASIC BIOLOGICAL SCIENCES↗

CAN-D: A Modular Four-Step Pipeline for Comprehensively Decoding Controller Area Network Data

Controller area networks (CANs) are a broadcast protocol for real-time communication of critical vehicle subsystems. Original equipment manufacturers of passenger vehicles hold secret their mappings of CAN data to vehicle signals, and these definitions vary according to make, model, and year. Without these mappings, the wealth of real-time vehicle information hidden in the CAN packets is uninterpretable, severely impeding vehicle-related research, including CAN cybersecurity and privacy studies, aftermarket tuning, efficiency and performance monitoring, and fault diagnosis to name a few. Guided by the four-part CAN signal definition, we present CAN-D (CAN-Decoder), a modular, four-step pipeline for identifying each signal's boundaries (start bit and length), endianness (byte ordering), signedness (bit-to-integer encoding), and by leveraging diagnostic standards, augmenting a subset of the extracted signals with meaningful, physical interpretation. En route to CAN-D, we provide a comprehensive review of the CAN signal reverse engineering research. All previous methods ignore endianness and signedness, rendering them incapable of decoding many standard CAN signal definitions. Incorporating endianness grows the search space from 128 to 4.72E21 signal tokenizations and introduces a web of changing dependencies. In response, we formulate, formally analyze, and provide an efficient solution to an optimization problem, allowing identification of the optimal set of signal boundaries and byte orderings. In addition, we provide two novel, state-of-the-art signal boundary classifiers—both of which are superior to previous approaches in precision and recall in three different test scenarios—and the first signedness classification algorithm, which exhibits a $>$ 97% F-score. Altogether, CAN-D is the only solution with the potential to extract any CAN signal that is also the state of the art. In evaluation on 10 vehicles of different makes, CAN-D's average $\ell ^1$ error is five times better (81% less) than all previous methods and exhibits lower average error, even when considering only signals that meet prior methods’ assumptions. Finally, CAN-D is implemented in lightweight hardware, allowing for an on-board diagnostic (OBD-II) plugin for real-time in-vehicle CAN decoding.

42 ENGINEERING↗

Carbon dioxide, water vapor and methane soil efflux (soil respiration) in a Pinus palustris restoration site in Georgetown, SC

This dataset contains processed data from a combination of survey flux chambers and long-term automated flux chambers. Biweekly soil flux measurements were conducted from June 2023 through December 2025 at a longleaf pine restoration site in Georgetown, SC. Processed, QAQC’d data can be found in the file: 1_DATA_ESS_DOE_HR_RS_HB3_QAQC_Survey_Data_20260223.csv. Raw and working data files (.json, & .81x format) from LI-COR equipment are included for reference and can be accessed using SoilFluxPro software. CSV metadata files describe the raw data and modifications made using SoilFluxPro v5 and Matlab R2024b, as well as formatting and units for processed CSVs. Matlab code is included for reading in the processed CSVs. This research was performed as part of the project: “Improving models of stand and watershed carbon and water fluxes with more accurate representations of soil-plant-water dynamics in southern pine ecosystems”, which examines in part the effects hydraulic redistribution on soil efflux of carbon dioxide, water vapor and methane, as well as soil moisture and temperature in a southern pine ecosystem with sandy soils and high water table.

CARBON DIOXIDE FLUX↗

Enabling Data Exchange and Data Integration with the Common Information Model: An Introduction for Power Systems Engineers and Application Developers

The Common Information Model (CIM) is an open-source information model that is used to model an electrical network and the various equipment used on the network. CIM is widely used for data exchange of bulk transmission power systems and is finding increasing use for distribution systems. Use of a non-proprietary information model (such as CIM) that has been agreed upon and adopted by numerous utilities, vendors, and researchers allows significant reduction in the effort and cost of data integration. Likewise, adoption of open data platforms built around the CIM increases available functionalities for managing and optimizing the smart grid of the future. This report is intended as an introduction to CIM for utility engineers, power systems researchers, and application developers, providing a broad view of the CIM and how particular profiles can be adapted for various use cases. Unlike most other CIM introduction documents and the International Electrotechnical Commission (IEC) standards (which are mostly targeted to an audience of data scientists, enterprise database managers, and platform developers), this report is intended for users of traditional power systems analysis software and other readers without any prior experience with canonical information models, data profiles, or UML modeling.

24 POWER TRANSMISSION AND DISTRIBUTION↗