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DOE OSTI2021

Correlating Nanoscale Secondary Ion Mass Spectrometry and Atom Probe Tomography Analysis of Uranium Enrichment in Metallic Nuclear Fuel

Distribution and enrichment of 235U within nuclear fuels are essential to material performance and reactor safety. With the development of metallic U fuels, understanding 235U homogeneity has become increasingly important, however, it is difficult to map with high spatial, and mass resolution to analyze both matrix and secondary phase precipitates. Here, we analyze 235U enrichment in matrix and carbide phases in LEU-Mo via two chemical imaging modalities: nanoscale secondary ion mass spectrometry (nanoSIMS) and atom probe tomography (APT). NanoSIMS and APT provided consistent results, with no statistically significant difference between measured and nominal enrichment (19.75 % 235U).

U-10Mo, atom probe tomography, nanoscale secondary↗

NASA NTRS1974

Planetary mission summaries. Volume 1: Introduction and overview

Tabular synopses of twelve missions are presented along with the Mariner Jupiter/Saturn 1977 mission for comparison. Mission definitions considered include: Mars Polar Orbiter; Mars Surface Sample Return; Mars Rover; Marine Jupiter/Uranus 1979 with Uranus Entry Probe; Mariner Jupiter Orbiter; Mariner Mercury Orbiter 1978; Early Mariner Comet Flyby Solar Electric Encke Slow Flyby; Mariner Encke Ballistic Flyby; Solar Electric Encke Rendezvous 1981; Venus Orbital Imaging Radar; Solar Electric Out-of-the-Eliptic Probe 1979. Technical conclusions of mission studies are given in order that these results may interact with the broader questions of scope, pace, and priorities in the planetary exploration program.

Source record↗

DOE OSTI2024

Flexible Soft X-Ray Image Sensors based on Metal Halide Perovskites With High Quantum Efficiency

Soft X-ray imaging is a powerful tool to explore the structure of cells, probe material with nanometer resolution, and investigate the energetic phenomena in the universe. Conventional soft X-ray image sensors are by and large Si-based charge coupled devices that suffer from low frame rates, complex fabrication processes, mechanical inflexibility, and required cooling below -60 °C. Here, a soft X-ray photodiode is reported based on low-cost metal halide perovskite with comparable performance to commercial Si-based device. Nanothrough network electrode minimized the optical loss due to the shadowing of insensitive layers, while a multidimensional perovskite heterojunction is generated to reduce the photo-generated carrier loss. Further, this strategy promoted a record quantum efficiency of 8 × 10 3 % without cooling, several orders of magnitude greater than the previously achieved. Flexible and curved soft X-ray imaging arrays are fabricated based on this high-performance device structure, demonstrating stable soft X-ray response and sharp imaging capabilities. This work highlights the low-cost and efficient perovskite photodiode as a strong candidate for the next-generation soft X-ray image sensors.

36 MATERIALS SCIENCE↗

DOE OSTI2026

Imaging from Macro to Nanoscale: Multimodal Advances in Chemical and Biomedical Imaging

Imaging increasingly serves as a multiscale framework for linking molecular mechanisms to cellular behavior, tissue architecture, and organ phenotypes in biology and unraveling fundamental processes in chemistry, physics and materials science. This Perspective highlights recent advances in chemical and biomedical imaging across macro-, micro-, and nanoscales, using representative examples published in Chemical and Biomedical Imaging (CBMI). At the macroscale, we discuss chemically selective MRI, including endogenous and exogenous CEST strategies, together with photoacoustic imaging as a hybrid modality with functional and chemical contrast. At the microscale, we consider fluorescence, label-free optical and vibrational imaging, and selected X-ray approaches that expand sensitivity, specificity, and temporal resolution in biological and materials systems. At the nanoscale, we highlight super-resolution fluorescence microscopy, single-molecule methods, tip-enhanced Raman spectroscopy, and correlative imaging strategies that resolve local heterogeneity and molecular organization. Across scales, a common theme emerges that advances in probes, contrast mechanisms, instrumentation, and sample handling are enabling chemically informed imaging that connects molecular specificity with biological context.

multiscale imaging↗

DOE OSTI2021

py4DSTEM: A Software Package for Four-Dimensional Scanning Transmission Electron Microscopy Data Analysis

Scanning transmission electron microscopy (STEM) allows for imaging, diffraction, and spectroscopy of materials on length scales ranging from microns to atoms. By using a high-speed, direct electron detector, it is now possible to record a full two-dimensional (2D) image of the diffracted electron beam at each probe position, typically a 2D grid of probe positions. These 4D-STEM datasets are rich in information, including signatures of the local structure, orientation, deformation, electromagnetic fields, and other sample-dependent properties. However, extracting this information requires complex analysis pipelines that include data wrangling, calibration, analysis, and visualization, all while maintaining robustness against imaging distortions and artifacts. In this paper, we present py4DSTEM, an analysis toolkit for measuring material properties from 4D-STEM datasets, written in the Python language and released with an open-source license. We describe the algorithmic steps for dataset calibration and various 4D-STEM property measurements in detail and present results from several experimental datasets. We also implement a simple and universal file format appropriate for electron microscopy data in py4DSTEM, which uses the open-source HDF5 standard. We hope this tool will benefit the research community and help improve the standards for data and computational methods in electron microscopy, and we invite the community to contribute to this ongoing project.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2022

DEVELOPMENT OF A QUANTUM ELECTRON BEAM DIAGNOSTIC APPARATUS

Spatial properties of electron beams are the essential parameters needed in particle physics and accelerator research. Beam characterization using optical detection methods through the interaction between photons and electrons such as Compton scattering, or electro-optic sampling of the electric field of electrons have been extensively explored and successfully implemented as non-invasive diagnostics at various accelerator facilities. However, such methods often suffer from inherently low sensitivity. Here we present the study of a new type of electron beam diagnostic device for direct optical imaging of electron beams at various energy levels. The concept is based on the extremely high sensitivity of atoms, prepared in a specific "dark superposition" quantum state, to the external electric or magnetic perturbations induced by the passing charged particle, which allows atoms to change polarization of the probe light or absorb probe light and to fluoresce, enabling direct 3D imaging of the charged particles with high resolution. We report our recent experiment results and the design effort on a compact apparatus intended to be tested with the relativistic electron beams at Jefferson Laboratory.

Zhang, S.↗

DOE OSTI2023

LensWatch. I. Resolved HST Observations and Constraints on the Strongly Lensed Type Ia Supernova 2022qmx (“SN Zwicky”)

Supernovae (SNe) that have been multiply imaged by gravitational lensing are rare and powerful probes for cosmology. Each detection is an opportunity to develop the critical tools and methodologies needed as the sample of lensed SNe increases by orders of magnitude with the upcoming Vera C. Rubin Observatory and Nancy Grace Roman Space Telescope. The latest such discovery is of the quadruply imaged Type Ia SN 2022qmx (aka, "SN Zwicky") at z = 0.3544. SN Zwicky was discovered by the Zwicky Transient Facility in spatially unresolved data. Here we present follow-up Hubble Space Telescope observations of SN Zwicky, the first from the multicycle "LensWatch (www.lenswatch.org)" program. We measure photometry for each of the four images of SN Zwicky, which are resolved in three WFC3/UVIS filters (F475W, F625W, and F814W) but unresolved with WFC3/IR F160W, and present an analysis of the lensing system using a variety of independent lens modeling methods. We find consistency between lens-model-predicted time delays (≲1 day), and delays estimated with the single epoch of Hubble Space Telescope colors (≲3.5 days), including the uncertainty from chromatic microlensing (~1–1.5 days). Our lens models converge to an Einstein radius of ${\theta }_{{\rm{E}}}=({0.168}_{-0.005}^{+0.009})^{\prime\prime} $, the smallest yet seen in a lensed SN system. The "standard candle" nature of SN Zwicky provides magnification estimates independent of the lens modeling that are brighter than predicted by $\sim {1.7}_{-0.6}^{+0.8}$ mag and $\sim {0.9}_{-0.6}^{+0.8}$ mag for two of the four images, suggesting significant microlensing and/or additional substructure beyond the flexibility of our image-position mass models.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2024

High redshift LBGs from deep broadband imaging for future spectroscopic surveys

Lyman break galaxies (LBGs) are promising probes for clustering measurements at high redshift, z > 2, a region only covered so far by Lyman-α forest measurements. Here, in this paper, we investigate the feasibility of selecting LBGs by exploiting the existence of a strong deficit of flux shortward of the Lyman limit, due to various absorption processes along the line of sight. The target selection relies on deep imaging data from the HSC and CLAUDS surveys in the g, r, z and u bands, respectively, with median depths reaching 27 AB in all bands. The selections were validated by several dedicated spectroscopic observation campaigns with DESI. Visual inspection of spectra has enabled us to develop an automated spectroscopic typing and redshift estimation algorithm specific to LBGs. Based on these data and tools, we assess the efficiency and purity of target selections optimised for different purposes. Selections providing a wide redshift coverage retain 57% of the observed targets after spectroscopic confirmation with DESI, and provide an efficiency for LBGs of 83 ± 3%, for a purity of the selected LBG sample of 90 ± 2%. This would deliver a confirmed LBG density of ~ 620 deg$^{-2}$ in the range 2.3 < z < 3.5 for a r-band limiting magnitude r < 24.2. Selections optimised for high redshift efficiency retain 73% of the observed targets after spectroscopic confirmation, with 89 ± 4% efficiency for 97 ± 2% purity. This would provide a confirmed LBG density of ~ 470 deg$^{-2}$ in the range 2.8 < z < 3.5 for a r-band limiting magnitude r < 24.5.A preliminary study of the LBG sample 3d-clustering properties is also presented and used to estimate the LBG linear bias. A value of b$_{LBG}$ = 3.3 ± 0.2 (stat.) is obtained for a mean redshift of 2.9 and a limiting magnitude in r of 24.2, in agreement with results reported in the literature.

79 ASTRONOMY AND ASTROPHYSICS↗

NASA NTRS2017

Chasing Shadows: Rotation of the Azimuthal Asymmetry in the TW Hya Disk

We have obtained new images of the protoplanetary disk orbiting TW Hya in visible, total intensity light with the Space Telescope Imaging Spectrograph (STIS) on the Hubble Space Telescope (HST), using the newly commissioned BAR5 occulter. These HSTSTIS observations achieved an inner working angle of approximately 0 "2, or11.7 au, probing the system at angular radii coincident with recent images of the disk obtained by ALMA and in polarized intensity near-infrared light. By comparing our new STIS images to those taken with STIS in 2000 and with NICMOS in 1998, 2004, and 2005, we demonstrate that TW Hyas azimuthal surface brightness asymmetry moves coherently in position angle. Between 50 au and 141 au we measure a constant angular velocity in the azimuthal brightness asymmetry of 22.deg7 yr(exp -1) in a counterclockwise direction, equivalent to a period of 15.9yrassuming circular motion. Both the (short) inferred period and lack of radial dependence of the moving shadow pattern are inconsistent with Keplerian rotation at these disk radii. We hypothesize that the asymmetry arises from the fact that the disk interior to 1 au is inclined and precessing owing to a planetary companion, thus partially shadowing the outer disk. Further monitoring of this and other shadows on protoplanetary disks potentially opens anew avenue for indirectly observing the sites of planet formation.

protoplanetary disk orbiting TW Hya↗

NASA NTRSDate not supplied

Wind Tunnel PSD and MVD Characterization Using New 1D2D Optical Array Probes

This work explores characterization of the liquid clouds using a combination of a forward scattering probe and two Optical Array Probes. Current OAP probes provide particle shape, size, and number concentration from two-dimensional shadow images. However, past studies have shown that such images are subject to distortion when outside of the focal plane. This affects the retrieval of particle size distributions, particularly in the Supercooled Large Droplet size range. In this article, the use of a Droplet Measurement Technologies Cloud Droplet Probe and two new OAPs produced by Science Engineering Associates, is examined using wind tunnel data, to assess suitability for use in a wind tunnel calibration in SLD conditions. The new OAP probes exploit a flexible and simple grey scale imaging method to eliminate some present shortcomings of commonly used OAPs, and to reduce correction factors. Spinning disk measurements were used to specify probe depth of field, and average size errors. Composite spectra covering the nominal 2-3200 µm size range were formed by crossing over from the CDP to 1D2D-X at 48 µm, and then to the 1D2D-Y at about 400 µm. A good overlap was found at the crossover points without any artificial scaling. Composite spectra adequately closed the liquid water content distribution, and provided integrated LWCs within about 35% of the hot-wire LWCs used for tunnel calibration. This discrepancy was at least partially attributed to LWC underestimation by the hot-wire at high MVD. A model of probe performance was used to show an example of expected accuracy of ideal probes subject to the same OAP distortions and using the same mitigating procedures and corrections, predicting PSD Median Volume Diameter and integrated LWC errors of less than 10%.

Aircraft Icing↗

DOE OSTI2020

Does Selectivity of Molecular Catalysts Change with Time? Polymerization Imaged by Single‐Molecule Spectroscopy

Abstract The chemoselectivity of molecular catalysts underpins much of modern synthetic organic chemistry. However, little is known about the selectivity of individual catalysts because this single‐catalyst‐level behavior is hidden by the bulk catalytic behavior. Here, for the first time, the selectivity of individual molecular catalysts for two different reactions is imaged in real time at the single‐catalyst level. This imaging is achieved through fluorescence microscopy paired with spectral probes that produce a snapshot of the instantaneous chemoselectivity of a single catalyst for either a single‐chain‐elongation or a single‐chain‐termination event during ruthenium‐catalyzed polymerization. Superresolution imaging of multiple selectivity events, each at a different single‐molecular ruthenium catalyst, indicates that catalyst selectivity may be unexpectedly spatially and time‐variable.

Garcia, IV, Antonio↗

DOE OSTI2020

Device-Level Multidimensional Thermal Dynamics With Implications for Current and Future Wide Bandgap Electronics

Researchers have been extensively studying wide-bandgap (WBG) semiconductor materials such as gallium nitride (GaN) with an aim to accomplish an improvement in size, weight, and power of power electronics beyond current devices based on silicon (Si). However, the increased operating power densities and reduced areal footprints of WBG device technologies result in significant levels of self-heating that can ultimately restrict device operation through performance degradation, reliability issues, and failure. Typically, self-heating in WBG devices is studied using a single measurement technique while operating the device under steady-state direct current measurement conditions. However, for switching applications, this steady-state thermal characterization may lose significance since the high power dissipation occurs during fast transient switching events. Therefore, it can be useful to probe the WBG devices under transient measurement conditions in order to better understand the thermal dynamics of these systems in practical applications. In this work, the transient thermal dynamics of an AlGaN/GaN high electron mobility transistor (HEMT) were studied using thermoreflectance thermal imaging and Raman thermometry. Also, the proper use of iterative pulsed measurement schemes such as thermoreflectance thermal imaging to determine the steady-state operating temperature of devices is discussed. These studies are followed with subsequent transient thermal characterization to accurately probe the self-heating from steady-state down to submicrosecond pulse conditions using both thermoreflectance thermal imaging and Raman thermometry with temporal resolutions down to 15 ns.

42 ENGINEERING↗

NASA NTRS2001

X-Ray Probes of Cosmic Star Formation History

We discuss the imprints left by a cosmological evolution of the star formation rate (SFR) on the evolution of X-ray luminosities Lx of normal galaxies, using the scheme earlier proposed by us, wherein the evolution of LX of a galaxy is driven by the evolution of its X-ray binary population. As indicated in our earlier work, the profile of Lx with redshift can both serve as a diagnostic probe of the SFR profile and constrain evolutionary models for X-ray binaries. We report here the first calculation of the expected evolution of X-ray luminosities of galaxies, updating our work by using a suite of more recently developed SFR profiles that span the currently plausible range. The first Chandra deep imaging results on Lx evolution are beginning to probe the SFR profile of bright spiral galaxies; the early results are consistent with predictions based on current SFR models. Using these new SFR profiles, the resolution of the "birthrate problem" of low-mass X-ray binaries and recycled, millisecond pulsars in terms of an evolving global SFR is more complete. We discuss the possible impact of the variations in the SFR profile of individual galaxies and galaxy types.

Ghosh, Pranab↗

NASA NTRS2005

Building the Case for SNAP: Creation of Multi-Band, Simulated Images With Shapelets

Dark energy has simultaneously been the most elusive and most important phenomenon in the shaping of the universe. A case for a proposed space-telescope called SNAP (SuperNova Acceleration Probe) is being built, a crucial component of which is image simulations. One method for this is "Shapelets," developed at Caltech. Shapelets form an orthonormal basis and are uniquely able to represent realistic space images and create new images based on real ones. Previously, simulations were created using the Hubble Deep Field (HDF) as a basis Set in one band. In this project, image simulations are created.using the 4 bands of the Hubble Ultra Deep Field (UDF) as a basis set. This provides a better basis for simulations because (1) the survey is deeper, (2) they have a higher resolution, and (3) this is a step closer to simulating the 9 bands of SNAP. Image simulations are achieved by detecting sources in the UDF, decomposing them into shapelets, tweaking their parameters in realistic ways, and recomposing them into new images. Morphological tests were also run to verify the realism of the simulations. They have a wide variety of uses, including the ability to create weak gravitational lensing simulations.

Ferry, Matthew A.↗

DOE OSTI2021

An imaging refractometer for density fluctuation measurements in high energy density plasmas

In this work, we report on a recently developed laser-probing diagnostic which allows direct measurements of ray-deflection angles in one axis, whilst retaining imaging capabilities in the other axis. This allows us to measure the spectrum of angular deflections from a laser beam which passes though a turbulent high-energy-density plasma. This spectrum contains information about the density fluctuations within the plasma, which deflect the probing laser over a range of angles. We create synthetic diagnostics using ray-tracing to compare this new diagnostic with standard shadowgraphy and schlieren imaging approaches, which demonstrates the enhanced sensitivity of this new diagnostic over standard techniques. We present experimental data from turbulence behind a reverse shock in a plasma and demonstrate that this technique can measure angular deflections between 0.06 and 34 mrad, corresponding to a dynamic range of over 500.

47 OTHER INSTRUMENTATION↗

DOE OSTI2023

Vacuum-Healing of Grain Boundaries in Sodium-Doped CuInSe 2 Solar Cell Absorbers

Alkali metal doping and grain boundaries (GB) have been at the center of attention within the Cu(In,Ga)(S,Se) 2 photovoltaics community for years. This study provides the first experimental evidence that the GB of sodium-doped CuInSe 2 thin films may undertake reversible oxidation even at room temperature, whereas undoped films may not. The findings are corroborated by cathodoluminescence imaging, secondary ion mass spectrometry, and Kelvin probe force microscopy on air-exposed films subsequently subject to vacuum. A thermochemical assessment identifies the likely solid-gas equilibria involved. These reactions open new research questions with respect to the beneficial role played by alkali metal dopants in chalcopyrite solar cells and may steer the community toward new breakthroughs.

14 SOLAR ENERGY↗

DOE OSTI2023

Expanded Coverage of Phytocompounds by Mass Spectrometry Imaging Using On-Tissue Chemical Derivatization by 4-APEBA

Probing the entirety of any species metabolome is an analytical grand challenge, especially at a cellular scale. Where spatial metabolomics, completed primarily by matrix-assisted laser desorption/ionization (MALDI), has limited molecular coverage for several reasons. To expand the scope of spatial metabolomics, we developed an on-tissue chemical derivatization (OTCD) workflow using 4-APEBA for confident identification of several dozen elusive phytocompounds, including several phytohormones, which have various roles within stress responses and cellular communication. Superiority of 4-APEBA is established in comparison to other derivatization agents with (1) broad specificity towards carbonyls, (2) low background, and (3) introduction of bromine isotopes, where the latter two facilitate confident bioinformatics. In conclusion, the outlined workflow trailblazes a path towards spatial hormonomics within plant samples, enhancing detection of carboxylates, aldehydes, ketones, and plausibly phenols.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2021

Spatial Mapping of Electrostatic Fields in 2D Heterostructures

In situ electron microscopy is an effective tool for understanding the mechanisms driving novel phenomena in 2D structures. However, due to practical challenges, it is difficult to address these technologically relevant 2D heterostructures with electron microscopy. Here, we use the differential phase contrast (DPC) imaging technique to build a methodology for probing local electrostatic fields during electrical operation with nanoscale spatial resolution in such materials. We find that, by combining a traditional DPC setup with a high-pass filter, we can largely eliminate electric fluctuations emanating from short-range atomic potentials. Using a method based on this filtering algorithm, a priori electric field expectations can be directly compared with experimentally derived values to readily identify inhomogeneities and potentially problematic regions. Furthermore, we use this platform to analyze the electric field and charge density distribution across layers of hBN and MoS 2 .

79 ASTRONOMY AND ASTROPHYSICS↗