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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 487 records · Page 27
All sourcesNASA NTRSDOE OSTI
NASA NTRS1972

Microscopic observations of X-ray and gamma-ray induced decomposition of ammonium perchlorate crystals

The X-ray and gamma-ray induced decomposition of ammonium perchlorate was studied by optical, transmission, and scanning electron microscopy. This material is a commonly used oxidizer in solid propellents which could be employed in deep-space probes, and where they will be subjected to a variety of radiations for as long as ten years. In some respects the radiation-induced damage closely resembles the effects produced by thermal decomposition, but in other respects the results differ markedly. Similar radiation and thermal effects include the following: (1) irregular or ill-defined circular etch pits are formed in both cases; (2) approximately the same size pits are produced; (3) the pit density is similar; (4) the c face is considerably more reactive than the m face; and (5) most importantly, many of the etch pits are aligned in crystallographic directions which are the same for thermal or radiolytic decomposition. Thus, dislocations play an important role in the radiolytic decomposition process.

Herley, P. J.↗
NASA NTRS1971

High-resolution electron microscope observation of voids in amorphous Ge.

Electron micrographs have been obtained which clearly show the existence of a void network in amorphous Ge films formed at substrate temperatures of 25 and 150 C, and the absence of a void network in films formed at higher substrate temperatures of 200 and 250 C. These results correlate quite well with density measurements and predictions of void densities by indirect methods.

Donovan, T. M.↗
NASA NTRS1973

Scanning electron microscope study of polytetrafluoroethylene sliding on aluminum single crystals

Friction experiments were conducted in air with polytetrafluoroethylene (PTFE) sliding on aluminum single crystals. Mechanical scoring of the crystals with (110) and (100) orientations was observed with a single pass of the PTFE slider. No scoring was observed on the (111). The degree of scoring of the crystals is related to the hardness, with the hardest surface (111) showing no damage and the softest surface (110) showing the most severe scoring. Scoring is caused by work-hardened pieces of aluminum which, as a consequence of the adhesion between PTFE and aluminum, were pulled out of the bulk and became embedded in the PTFE polymer.

Brainard, W. A.↗
NASA NTRS1973

Scanning electron microscope study of Apollo 15 green glass

Apollo 15 green glass droplets and related forms show a variety of low velocity impact features which occurred at the time of formation of the droplets. Composite forms, which consist of a crystallized core on which mounds of glass adhere, indicate a sequence of core formation and crystallization, followed by impact of molten droplets. The complicated and time dependent texture and morphology of the green glass forms are best explained by formation in a volcanic lava fountain rather than by meteorite impact.

Mckay, D. S.↗
NASA NTRS1973

Evidence for a ubiquitous, sub-microscopic 'magnetite-like' constituent in the lunar soils

Electron spin resonance (ESR) has been employed in a study of the ferromagnetic constituents of a wide variety of soils from six sampled regions of the moon as well as glasses made to simulate lunar compositions. A significant result has been that magnetite-like phases (magnetic iron spinel) precipitated in and on simulated lunar glasses as a result of sub-solidus oxidation yield room-temperature ESR spectra virtually identical with the line shape predicted for spherical, single domain particles of metallic Fe. It is shown that such magnetite-like phases can nevertheless be distinguished from metallic iron on the basis of the temperature dependence of the ESR intensity.

Griscom, D. L.↗
NASA NTRS1974

External field effects on solidification - Macroscopic and microscopic models

Comparison of theoretical effects of magnetic and gravitational fields on melts of metals and semiconductors provides two kinds of insight into space processing materials problems. First, the task of comparing effects of the two fields yields mathematical models which may be used to estimate material properties and responses to processing under various field conditions. Then, by using these models, microgravity effects can be inferred from magnetic field data already obtained in laboratories on earth. Magnetohydrodynamics (static and oscillating fields) and the Free Volume Model are used to study macroscopic effects, and Sekerka's interface stability theory is used to show how external fields can affect microsegregation. It is demonstrated that the mathematical formalism is essentially the same for describing macroscopic effects of both microgravity and magnetic fields.

Miller, R. I.↗
NASA NTRS1974

A scanning electron microscope study of olivine crystal surfaces

SEM photographs were taken of euhedral olivine grains from the Murchison C2 chondrite and several terrestrial and lunar occurrences. In general, the crystal faces of the meteorite grains are rough and uneven, with irregular growth patterns. They are very similar to crystal faces on terrestrial olivine grains that formed by sublimation from a vapor phase. They are very different from the relatively smooth and featureless surfaces of magmatic olivine crystals that precipitated from igneous melts. Qualitatively, the surface morphology of the crystal supports the contention that many euhedral crystals of olivine in C2 meteorites condensed from a gas phase.

Olsen, E. J.↗
NASA NTRS1975

Scanning electron microscope investigation of the structural growth in thick sputtered coatings

Sputtered S-Monel, silver, and 304 stainless steel coatings and molybdenum disulfide coatings were deposited on mica and metal substrates with various surface finishes to investigate the structural growth of the coating by scanning electron microscopy. The geometry and the surface morphology of the nodules are characterized. Compositional changes within the coating were analyzed by energy dispersive X-ray analysis. Defects in the surface finish act as preferential nucleation sites and form isolated overlapping and complex nodules and various unusual surface overgrowths on the coating. The nodule boundaries are very vulnerable to chemical etching and these nodules do not disappear after full annealing. Further, they have undesirable effects on mechanical properties; cracks are initiated at the nodules when the coating is stressed by mechanical forces.

Spalvins, T.↗