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At least 487 records · Page 27

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DOE OSTI2026

Synthesis of boron-carbide aerogels

We present the synthesis of boron carbide aerogels utilizing nano-boron powder and resorcinol–formaldehyde (RF) organic aerogels as precursors. Monolithic aerogels were fabricated from suspensions of boron nanoparticles and RF via an organic sol-gel process, enabling effective distribution of boron in the gel network. The resulting gels underwent supercritical drying, thermal reduction, and subsequent heat treatment to yield boron carbide aerogels with densities ranging from 37 to 55 mg/cm³. By tuning the boron-to-carbon ratio, heat treatment temperature, and dwell time, surface areas up to 53 m²/g were obtained. X-ray diffraction analysis confirmed the formation of the boron carbide phase and detected the presence of residual carbon within the structure.

Materials science↗

DOE OSTI2025

Convection-Permitting Ensembles of an Isolated Mountain Thunderstorm during RELAMPAGO/CACTI

Abstract The north–south-oriented Sierras de Córdoba (SDC) ridge in central Argentina is noted for initiating thunderstorms that may grow into intense mesoscale convective systems (MCSs). It also initiates more isolated, shorter-lived cells under weaker synoptic forcing. These cells are less impactful than MCSs but may be difficult to predict in convective-scale numerical weather prediction (NWP) due to their strong sensitivities to subgrid and partially resolved processes. To study the mechanisms and predictability of such cells, convection-permitting ensemble simulations were conducted of an isolated, diurnally forced SDC thunderstorm during Cloud, Aerosol, and Complex Terrain Interactions (CACTI)/Remote Sensing of Electrification, Lightning, and Mesoscale/Microscale Processes with Adaptive Ground Observations (RELAMPAGO). The rich observational data facilitated detailed ensemble verification, where dry biases in the surface energy balance and soil moisture were identified. These biases promoted rapid removal of convective inhibition and an early onset of precipitating cells over the SDC that were shallower and weaker than the observed cell. Correction, and then overcorrection, of the soil moisture bias in two successive ensembles was required to rectify the surface energy balance and improve the representation of the SDC cell. Nevertheless, substantial ensemble variability in convective precipitation was found, with some members producing more widespread convection than observed and others producing no deep convection at all. This variability was largely explained by a combination of thermodynamic and dynamic mechanisms, dominated by a positive sensitivity of convective precipitation to preconvective moist instability over the ridge. Secondary sensitivities were found to low-level upward mass flux and midlevel cross-barrier winds, the latter of which caused gravity waves with elevated downdrafts that tended to suppress incipient clouds.

Lopez, Andres [Department of Atmospheric and Ocean↗

NASA NTRS1984

A possible source for the Martian circumpolar dune material

The properties of freeze dried dilute dispersions of dust in water are of considerable interest in studies of sedimentary processes in the polar regions of Mars. The formation of a rind residue due to the sublimation of water ice containing various amounts of clay may be an important step in these processes. Such phenomena may occur as the result of seasonal or long term (climatic) sublimation of dirty ice caps on Mars. The development and disruption of dust residues on the surface of ice dust mixtures as a result of preferential ice sublimation were simulated in the laboratory. The characteristics of the resulting particles are described and a scenario for the formation of a Martian circumpolar dune field is suggested.

Saunders, R. S.↗

NASA NTRS1985

Equipment for Hot-to-serve Foods

Patented surface heating devices with a much faster air-to-solid heat transfer rate than previous air ovens were developed. The accelerated surface heating can brown, sear or crisp much more rapidly than in conventional ovens so that partially prepared food can be finished quickly and tastefully immediately before serving. The crisp, freshly browned surfaces result from the faster heat transfer which does not dry out the food. The devices are then compared to convection ovens and microwave heating processes.

Smith, D. P.↗

NASA NTRS1993

Protein crystal growth

Proteins account for 50% or more of the dry weight of most living systems and play a crucial role in virtually all biological processes. Since the specific functions of essentially all biological molecules are determined by their three-dimensional structures, it is obvious that a detailed understanding of the structural makeup of a protein is essential to any systematic research pertaining to it. At the present time, protein crystallography has no substitute, it is the only technique available for elucidating the atomic arrangements within complicated biological molecules. Most macromolecules are extremely difficult to crystallize, and many otherwise exciting and promising projects have terminated at the crystal growth stage. There is a pressing need to better understand protein crystal growth, and to develop new techniques that can be used to enhance the size and quality of protein crystals. There are several aspects of microgravity that might be exploited to enhance protein crystal growth. The major factor that might be expected to alter crystal growth processes in space is the elimination of density-driven convective flow. Another factor that can be readily controlled in the absence of gravity is the sedimentation of growing crystal in a gravitational field. Another potential advantage of microgravity for protein crystal growth is the option of doing containerless crystal growth. One can readily understand why the microgravity environment established by Earth-orbiting vehicles is perceived to offer unique opportunities for the protein crystallographer. The near term objectives of the Protein Crystal Growth in a Microgravity Environment (PCG/ME) project is to continue to improve the techniques, procedures, and hardware systems used to grow protein crystals in Earth orbit.

Bugg, Charles E.↗

NASA NTRS1994

Climatic implications of the seasonal variation of upper troposphere water vapor

Satellite observations indicate that the humidity of the upper troposphere is higher in summer than in winter. We use general circulation model (GCM) simulations to explore the processes that maintain upper troposphere water vapor and determine its seasonal cycle. In the subtropics, drying by Hadley cell subsidence and stratiform condensation is offset primarily by moistening by eddies, with moist convection playing a minor role. Elsewhere, both mean meridional circulation and eddies moisten the upper troposphere and are balanced primarily by stratiform condensation drying. The effect of the seasonal shift of the Hadley cell is limited to latitudes equatorward of 30 deg. At higher latitudes where the largest observed summer moistening occurs, eddy moisture fluxes are primarily responsible despite the eddies being weaker in summer than winter. The same mechanism causes upper level humidity to increase in GCM climate warming simulations. The observed seasonal variation may thus be a good proxy for decadal climate change. This suggests that upper troposphere water vapor feedback is positive at all latitudes, consistent with GCM predictions.

Del Genio, Anthony D.↗

NASA NTRS2005

Space Environmentally Durable Polyimides and Copolyimides

Polyimides displaying low color in thin films, atomic oxygen resistance, vacuum ultraviolet radiation resistance, solubility in organic solvents in the imide form, high glass transition (T(sub g)) temperatures, and high thermal stability are provided. The poly(amide acid)s, copoly(amide acid)s, polyimides and copolyimides are prepared by the reaction of stoichiometric ratios of an aromatic dianhydride with diamines which contain phenylphosphine oxide groups in polar aprotic solvents. Controlled molecular weight oligomeric (amide acid)s and imides can be prepared by offsetting the stoichiometry according to the Carothers equation using excess diamine and endcapping with aromatic anhydrides The polyimide materials can be processed into various material forms such as thin films, fibers, foams, threads, adhesive film, coatings, dry powders, and fiber coated prepreg, and uses include thin film membranes on antennas, second-surface mirrors, thermal optical coatings, and multilayer thermal insulation (MLI) blanket materials.

John W Connell↗

NASA NTRS1957

The Effect of Solid Admixtures on the Velocity of Motion of a Free Dusty Air Jet

In dusty air flows occurring in industrial practice in transport by air pressure of friable materials, in the drying, annealing, and so forth, of a pulverized solid mass in suspension, and in other processes, the concentration of solid particles usually has a magnitude of the order of 1 kg per 1 kg of air. At such a concentration, the ratio of the volume of the particles to the volume of the air is small (less than one-thousandth part). However, regardless of this, the presence of a solid admixture manifests itself in the rules for the velocity distribution of the air in a dusty air flow. As a result, the rules of velocity change are different for clean and for dusty air flows. The estimation of the influence of the admixture on the velocity of the motion of the flow presents a definitive interest. One of the attempts to estimate that influence on the axial velocity of a free axially symmetrical jet with admixtures was made by Abramovich. Abramovich assumed beforehand that the fine particles of the admixture in the jet are subject to the motion of the air (that is, that the velocity of the admixture is approximately equal to the local velocity of the air); he then took as the basis of his considerations, in solving the problem, the condition that the amount of motion of the two-phase jet must be constant.

Chernov, A. P.↗

NASA NTRS2003

Pulsed Plasma Thruster (PPT) Technology: Earth Observing-1 PPT Operational and Advanced Components Being Developed

In 2002 the pulsed plasma thruster (PPT) mounted on the Earth Observing-1 spacecraft was operated successfully in orbit. The two-axis thruster system is fully incorporated in the attitude determination and control system and is being used to automatically counteract disturbances in the pitch axis of the spacecraft. The first tests conducted in space demonstrated the full range of PPT operation, followed by calibration of control torques from the PPT in the attitude control system. Then the spacecraft was placed in PPT control mode. To date, it has operated for about 30 hr. The PPT successfully controlled pitch momentum during wheel de-spin, solar array acceleration and deceleration during array rewind, and environmental torques in nominal operating conditions. Images collected with the Advanced Landsat Imager during PPT operation have demonstrated that there was no degradation in comparison to full momentum wheel control. In addition, other experiments have been performed to interrogate the effects of PPT operation on communication packages and light reflection from spacecraft surfaces. Future experiments will investigate the possibility of orbit-raising maneuvers, spacecraft roll, and concurrent operation with the Hyperion imager. Future applications envisioned for pulsed plasma thrusters include longer life, higher precision, multiaxis thruster configurations for three-axis attitude control systems or high-precision, formationflying systems. Advanced components, such as a "dry" mica-foil capacitor, a wear-resistant spark plug, and a multichannel power processing unit have been developed under contract with Unison Industries, General Dynamics, and C.U. Aerospace. Over the last year, evaluation tests have been conducted to determine power processing unit efficiency, atmospheric functionality, vacuum functionality, thruster performance evaluation, thermal performance, and component life.

Pencil, Eric J.↗

NASA NTRS2002

Processes Controlling Water Vapor in the Winter Arctic Tropopause Region

This work describes transport and thermodynamic processes that control water vapor near the tropopause during the SAGE III-Ozone Loss and Validation Experiment (SOLVE), held during the Arctic 1999/2000 winter season. Aircraft-based water vapor, carbon monoxide, and ozone measurements were analyzed so as to establish how deeply tropospheric air mixes into the Arctic lowermost stratosphere and what the implications are for cloud formation and water vapor removal in this region of the atmosphere. There are three major findings. First, troposphere-to-stratosphere exchange extends into the Arctic stratosphere to about 13 km. Penetration is to similar levels throughout the winter, however, because ozone increases with altitude most rapidly in the early spring, tropospheric air mixes with the highest values of ozone in that season. The effect of this upward mixing is to elevate water vapor mixing ratios significantly above their prevailing stratospheric values of above 5ppmv. Second, the potential for cloud formation in the stratosphere is highest during early spring, with about 20% of the parcels which have ozone values of 300-350 ppbv experiencing ice saturation in a given 10 day period. Third, during early spring, temperatures at the troposphere are cold enough so that 5-10% of parcels experience relative humidities above 100%, even if the water content is as low as 5 ppmv. The implication is that during this period, dynamical processes near the Arctic tropopause can dehydrate air and keep the Arctic tropopause region very dry during early spring.

Pfister, Leonhard↗

NASA NTRS2006

Space Environmentally Durable Polyimides and Copolyimides

Polyimides displaying low color in thin films, atomic oxygen resistance, vacuum ultraviolet radiation resistance, solubility in organic solvents in the imide form, high glass transition (T(sub g)) temperatures, and high thermal stability are provided. The poly(amide acid)s, copoly(amide acid)s, polyimides and copolyimides are prepared by the reaction of stoichiometric ratios of an aromatic &anhydride with diamines which contain phenylphosphine oxide groups in polar aprotic solvents. Controlled molecular weight oligomeric (amide acid)s and imides can be prepared by offsetting the stoichiometry according to the Carothers equation using excess diamine and endcapping with aromatic anhydrides. The polyimide materials can be processed into various material forms such as thin films, fibers, foams, threads, adhesive film, coatings, dry powders, and fiber coated prepreg, and uses include thin film membranes on antennas, second-surface mirrors, thermal optical coatings, and multilayer thermal insulation (MLI) blanket materials.

Connell, John W.↗

NASA NTRS2013

Notched Strength Allowables and Inplane Shear Strength of AS4/VRM-34 Textile Laminates

Notched and unnotched strength allowables were developed for a textile composite to provide input data to analytical structural models based on the Pultruded Rod Stiffened Efficient Unitized Structure (PRSEUS) concept. Filled-hole tensile strength, filled-hole compressive strength, and inplane shear strength along stitch lines have been measured. The material system evaluated in this study is based on warp-knitted preforms of AS4 carbon fibers and VRM-34 epoxy resin, which have been processed via resin infusion and oven curing. All specimens were tested in as-fabricated (dry) condition. Filled-hole strengths were evaluated with and without through-thickness stitching. The effects of scaling on filled-hole tensile strength were evaluated by testing specimens in two widths, but with identical width / hole-diameter ratios. Inplane shear specimens were stitched in two configurations, and two specimen thicknesses were tested for each stitch configuration.

Grenoble, Ray W.↗

NASA NTRS2016

Terrestrial Testing of the CapiBRIC, a Microgravity Optimized Brine Processor

Utilizing geometry based static phase separation exhibited in the radial vaned capillary drying tray, a system was conceived to recover water from brine. This technology has been named the Capillary BRIC; abbreviated CapiBRIC. The CapiBRIC utilizes a capillary drying tray within a drying chamber. Water is recovered from clean water vapor evaporating from the free surface leaving waste brine solids behind. A novel approach of optimizing the containment geometry to support passive capillary flow and static phase separation provides the opportunity for a low power system that is not as susceptible to fouling as membranes or other technologies employing physical barriers across the free brine surface to achieve phase separation in microgravity. Having been optimized for operation in microgravity, full-scale testing of the CapiBRIC as designed cannot be performed on the ground as the force of gravity would dominate over the capillary forces. However, subscale units relevant to full-scale design were used to characterize fill rates, containment stability, and interaction with a variable volume reservoir in the PSU Dryden Drop Tower (DDT) facility. PSU also using tested units scaled such that capillary forces dominated in a 1-g environment to characterize evaporation from a free-surface in 1-g upward, sideways and downward orientations. In order to augment the subscale testing performed by PSU, a full scale 1-g analogue of the CapiBRIC drying unit was initiated to help validate performance predictions regarding expected water recovery ratio, estimated processing time, and interface definitions for inlets, outlets, and internal processes, including vent gas composition. This paper describes the design, development and test of the terrestrial CapiBRIC prototypes.

Sargusingh, Miriam J.↗

NASA NTRS2018

Modification of Radiator Pigments by Atomic Layer Deposition (ALD)

The optical and physical properties of spacecraft radiator coatings are dictated by orbital environmental conditions. For example, coatings must adequately dissipate charge buildup when orbital conditions, such as polar, geostationary or gravity neutral, result in surface charging. Current dissipation techniques include depositing a layer of ITO (indium tin oxide) on the radiator surface in a high temperature process. Other examples include the application of variable emittance coatings such as the use of VO2 to optimize radiator size, allowing for a decrease in heater power budget. The application of these enhanced coatings must be such that the properties in question are tailored to mission-specific requirements. Modification of these coatings can be accomplished during coating application preprocessing by using a deposition technique prevalent in the semiconductor micro processing industry called Atomic Layer Deposition (ALD). The preprocessing is rendered directly on the coating dry pigment before binding. ALD is a cost effective nano-manufacturing technique that allows for the conformal coating of substrates with atomic-level thickness control in a benign temperature and pressure environment. Through the introduction of paired precursor gases, thin films can be deposited on a myriad of substrates ranging from glass, polymers, aerogels, metals, powders, and other high aspect-ratio micro- and nano-structures. By providing atomic-level control, where single layers of atoms can be deposited, the fabrication of metal transparent films, precise nano-laminates, and coatings of nano-channels and pores is achievable. We have demonstrated a method for the ALD of In2O3 and ITO films on a variety of substrates from Si(100) wafers, glass slides, and on Z93P pigments (patent pending). The results indicate excellent growth of 4-22 nm thick films demonstrating an order of magnitude decrease in resistivity on the pigments.

ITO↗

DOE OSTI2025

Shear Assisted Processing and Extrusion of Magnesium Alloy Machining Chips

The Pacific Northwest National Laboratory (PNNL) utilized Shear Assisted Processing and Extrusion (ShAPE) to convert magnesium alloy machining chips directly into wrought material. PNNL fabricated 0.25” and 0.50” round rod from cold compacted briquettes pressed from dry-machined chips by Loukus Technologies. The alloy composition is proprietary and protected by a Materials Transfer Agreement (MTA) between PNNL and Loukus. Extrusions were fabricated using the ShAPE 2.0 machine, tooling, and process. PNNL is evaluating tensile properties per ASTM E8 and microstructure for grain size, texture, and porosity using Scanning Electron Microscopy (SEM) and Electron Backscatter Diffraction (EBSD). Tensile properties and microstructure results were not available at the time of writing this document. Extruded rods have also been sent to Loukus for evaluation.

36 MATERIALS SCIENCE↗

NASA NTRS2022

Remote Sensing of Aerosol Water Fraction, Dry Size Distribution and Soluble Fraction Using Multi-Angle, Multi-Spectral Polarimetry

A framework to infer volume water fraction, soluble fraction and dry size distributions of fine-mode aerosol from multi-angle, multi-spectral polarimetry retrievals of column-averaged ambient aerosol properties is presented. The method is applied to observations of the Research Scanning Polarimeter (RSP) obtained during two NASA aircraft campaigns, namely the Aerosol Cloud meTeorology Interactions oVer the western ATlantic Experiment (ACTIVATE) and the Cloud, Aerosol, and Monsoon Processes Philippines Experiment (CAMP2Ex). All aerosol retrievals are statistically evaluated using in situ data. Volume water fraction is inferred from the retrieved ambient real part of the refractive index, assuming a dry refractive index of 1.54 and by applying a volume mixing rule to obtain the effective ambient refractive index. The uncertainties in inferred volume water fraction resulting from this simplified model are discussed and estimated to be lower than 0.2 and decreasing with increasing volume water fraction. The daily mean retrieved volume water fractions correlate well with the in situ values with a mean absolute difference of 0.09. Polarimeter-retrieved ambient effective radius for daily data is shown to increase as a function of volume water fraction as expected. Furthermore, the effective variance of the size distributions also increases with increasing effective radius, which we show is consistent with an external mixture of soluble and insoluble aerosol. The relative variations of effective radius and variance over an observation period are then used to estimate the soluble fraction of the aerosol. Daily results of soluble fraction correlate well with in situ-observed sulfate mass fraction with a correlation coefficient of 0.79. Subsequently, inferred water and soluble fractions are used to derive dry fine-mode size distributions from their ambient counterparts. While dry effective radii obtained in situ and from RSP show similar ranges, in situ values are generally substantially smaller during the ACTIVATE deployments, which may be due to biases in RSP retrievals or in the in situ observations, or both. Both RSP and in situ observations indicate the dominance of aerosol with low hygroscopicity during the ACTIVATE and CAMP2Ex campaigns. Furthermore, RSP indicates a high degree of external mixing of particles with low and high hygroscopicity. These retrievals of fine-mode water volume fraction and soluble fraction may be used for the evaluation of water uptake in atmospheric models. Furthermore, the framework allows us to estimate the variation in the concentration of fine-mode aerosol larger than a specific dry radius limit, which can be used as a proxy for the variation in cloud condensation nucleus concentrations. This framework may be applied to multi-angle, multi-spectral satellite data expected to be available in the near future.

Amount of water in particulate matter↗

NASA NTRS2008

The NASA Orbiting Carbon Observatory (OCO) Mission: Objectives, Approach, and Status

The Orbiting Carbon Observatory (OCO) is a NASA Earth System Science Pathfinder (ESSP) mission that is currently under development at the Jet Propulsion Laboratory (JPL). OCO will make global, space-based measurements of atmospheric carbon dioxide (CO2) with the precision, resolution, and coverage needed to characterize regional-scale sources and sinks of this important greenhouse gas. The observatory consists of a dedicated spacecraft bus that carries a single instrument. The bus employs single-string version of Orbital Sciences Corporation (OSC) LEOStar-2 architecture. This 3-axis stabilized bus includes a propulsion system for orbit insertion and maintenance, provides power, points the instrument, receives and processes commands from the ground, and records, stores, and downlinks science and engineering data. The OCO instrument incorporates 3 oboresighted, high resolution grating spectrometers that will make coincident measurements of reflected sunlight in near-infrared CO2 and molecular oxygen (O2) bands. The instrument was designed and manufactured by Hamilton Sundstrand (Pomona, CA), and then integrated, flight qualified, and calibrated by JPL. It is scheduled for delivery to OSC (Dulles, VA) for integration with the spacecraft bus in the spring of 2008. OCO will be launched from the Vandenberg Air Force Base on a dedicated OSC Taurus XL launch vehicle in December 2008. It will fly in formation with the Earth Observing System Afternoon Constellation, a group of satellites that files in a 98.8 minute, 705 km altitude, sun-synchronous orbit. This orbit provides coverage of the sunlit hemisphere with a 16-day ground track repeat cycle. OCO will fly approx.4 minutes ahead of the EOS Aqua platform, with an ascending nodal crossing time of approx.1:26 PM. The OCO science data will be transmitted to the NASA Ground Network Stations in Alaska and Virginia, and then transferred to the OCO Ground Data System at JPL. There, the CO2 and O2 spectra will be analyzed by the OCO Science Team to provide spatially resolved estimates of the column-averaged CO2 dry air mole fraction, XCO2. These measurements are expected to improve our understanding of the nature and processes that regulate atmospheric CO2 enabling more reliable forecasts of CO2 buildup and its impact on climate change.

global measurements↗

NASA NTRS2006

Optimal Composite Material for Low Cost Fabrication of Large Composite Aerospace Structures using NASA Resins or POSS Nanoparticle Modifications

Thermoplastic laminates in situ consolidated via tape or tow placement require full mechanical properties. Realizing full properties requires resin crystallinity to be controlled - partial crystallinity leads to unacceptably low laminate compression properties. There are two approaches: utilize an amorphous matrix resin; or place material made from a semi-crystalline resin featuring kinetics faster than the process. In this paper, a matrix resin evaluation and trade study was completed with commercial and NASA amorphous polyimides on the one hand, and with PEKK mixed with POSS nanoparticles for accelerated crystallinity growth on the other. A new thermoplastic impregnated material, 6 mm wide (0.25-in) AS-4 carbon/LaRC(TradeMark)8515 dry polyimide tow, was fabricated. Since LaRC(TradeMark)8515 is fully amorphous, it attains full properties following in situ consolidation, with no post processing required to build crystallinity. The tow in situ processing was demonstrated via in situ thermoplastic filament winding it into rings.

Lamontia, Mark A.↗