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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 487 records · Page 27

Residual water bactericide monitor development program

A silver-ion bactericidal monitor is considered for the Space Shuttle Potable Water System. Potentiometric measurement using an ion-selective electrode is concluded to be the most feasible of available techniques. Four commercially available electrodes and a specially designed, solid-state, silver-sulfide electrode were evaluated for their response characteristics and suitability for space use. The configuration of the solid-state electrode with its Nernstian response of 10 to 10,000 ppb silver shows promise for use in space. A pressurized double-junction reference electrode with a quartz-fiber junction and a replaceable bellows electrolyte reservoir was designed verification-tested, and paired with a solid-state silver-sulfide electrode in a test fixture.

Source record↗

Ku-band miniature modulators

Ku-band microminiature modulators were designed to convert a 10 mW signal at 400 MHz to a 10 mW signal at 15 GHz. The designs incorporate gallium arsenide Schottky barrier varactors used in upper-sideband up-converters. The use of Ku-band microstrip circulators and hairpin resonator bandpass filters at 2.1 GHz and 2.5 GHz is included. The design and fabrication of a single up-conversion unit with a double up-conversion unit are compared. Various filter configurations are studies, and the use of both alumina and quartz substrates are considered. The various impedance matching networks are evaluated using computer aided design techniques.

Ernst, R. L.↗

Pulsed electromagnetic acceleration

Direct measurements of the power deposited in the anode of a multimegawatt MPD accelerator using thermocouples attached to a thin shell anode reveal a dramatic decrease in the fractional anode power from 50% at 200 KW input power to less than 10% at 20 MW power. The corresponding local power flux peak at a value of 10,000 W/sq cm at the lip of the anode exhaust orifice, a distribution traced to a corresponding peak in the local current density at the anode. A comparison of voltage-current characteristics and spectral photographs of the MPD discharge using quartz, boron nitride and plexiglas insulators with various mass injection configurations led to the identification of different voltage modes and regions of ablation free operation. The technique of piezoelectric impact pressure measurement in the MPD exhaust flow was refined to account for the effects due to probe yaw angle.

Jahn, R. G.↗

ATS-F radiant cooler contamination test in a hydrazine thruster exhaust

A test was conducted under simulated space conditions to determine the potential thermal degradation of the ATS-F radiant cooler from any contaminants generated by a 0.44-N(0.1-lbf) hydrazine thruster. The radiant cooler, a 0.44-N(0.1-lbf)hydrazine engine, and an aluminum plate simulating the satellite interface were assembled to simulate their flight configuration. The cooler was provided with platinum sensors for measuring temperature, and its surfaces were instrumented with six quartz crystal microbalance units (QCM) to measure contaminant mass deposits. The complete assembly was tested in the molecular sink vacuum facility (Molsink) at the Jet Propulsion Laboratory. This was the first time that a radiant cooler and a hydrazine engine were tested together in a very-high-vacuum space simulator, and this test was the first successful measurement of detectable deposits from hydrazine rocket engine plumes in a high vacuum. The engine was subjected to an accelerated duty cycle of 1 pulse/min, and after 2-hr of operation, the QCMs began to shift in frequency. The tests continued for several days and, although there was considerable activity in the QCMs, the cooler never experienced thermal degradation.

Chirivella, J. E.↗

Molecular flux measurements in the back flow region of a nozzle plume

A series of tests were conducted to measure the mass flux in the far field of a nozzle plume in a high vacuum with emphasis on the back flow region. The measurements presented provided fairly accurate data for off-axis angles as large as 140 deg (i.e., in the back flow region). This region, since it is well behind the exit plane, is of paticular interest to those concerned with instrument contamination. Usually sensitive spacecraft surfaces are located in the region affected by the back flow. Parameters such as expansion ratio, throat diameter, nozzle lip shape, and plenum (chamber) pressure were varied, carbon dioxide and nitrogen gases were flowed and mass flux measurements were taken using quartz crystal microbalances in as many as nine different locations relative to the tests nozzle. Several conclusions with respect to the effect of nozzle and gas parameters on the amount of back flow mass flux are offered, and it was demonstrated that gaseous mass fluxes, which are not predictable by present theories, are encountered in the region behind the nozzle exit plane. This knowledge is significant if materials incompatible with the gaseous exhaust products are used in this region.

Chirivella, J. E.↗

The effect of surface conditions on the work function of insulators and semiconductors

Ionization energies of organic semiconductors were determined using single crystals of the material. The theory of the method is essentially that of Millikan's oil drop experiment. The technique employed in the experiment is based on the electrostatic method of balancing a charged particle in an electric field against the force of gravity for different excitation energies above the threshold value, and from an estimate of the balancing voltages, read off the ionization energy from the intercept of the energy axis in a plot wavelength corresponding to the balancing potential for the incident radiation of wavelength. In the modified technique which is adopted in the present experimental investigation, a small single crystal is suspended by a fine quartz fiber between two vertical capacitor plates to which a suitable high voltage is applied.

George, A.↗

Star tracking reticles

A method for the production of reticles, particularly those for use in outer space, where the product is a quartz base coated with highly adherent layers of chromium, chromium-silver, and silver vacuum deposited through a mask, and then coated with an electrodeposit of copper from a copper sulfate solution followed by an electrodeposit of black chromium is described. The masks are produced by coating a beryllium-copper alloy substrate with a positive working photoresist, developing the photoresist, according to a pattern to leave a positive mask, plating uncoated areas with gold, removing the photoresist, coating the substrate with a negative working photoresist, developing the negative working photoresist to expose the base metal of the pattern, and chemically etching the unplated side of the pattern to produce the mask.

Smith, W. O.↗

Two-pass-internal second-harmonic generation using a prism coupler.

A dispersive quartz prism is used to couple the total second harmonic generated in both directions by an internal cavity frequency doubler. The study shows that the dispersion of air and mirror reflection phase shifts can be compensated for by a slight nonphase match condition in the doubler.

Gonzalez, D. G.↗

Removal of hydrocarbon contaminant film from spacecraft optical surfaces using a radiofrequency-excited oxygen plasma.

Results of a study on the feasibility of removing contaminant films from optical surfaces in vacuum, using an oxygen plasma, are discussed. Contaminant films were deposited onto optical surfaces from butadiene and methane gases at a pressure of about 4 torr in the presence of ultraviolet radiation. Optical surfaces evaluated included ultraviolet-reflecting mirrors, gratings, quartz disks, and spacecraft thermal control surfaces. In general, it was found that contaminants could be removed successfully from surfaces using an oxygen plasma. Exceptions were the white-paint thermal control surfaces, which, when contaminated, degraded further during exposure to the oxygen plasma.

Beverly, W. D.↗

Indium sealing techniques.

Gold films are used as an alloying flux to form 5-micron-thick indium film seals at temperatures below 300 C. Pyrex was sealed to quartz, ULE, CER-VIT, Irtran 2, Ge, GaAs, Invar, Kovar, Al, and Cu. The seals can also be used as current feedthroughs and graded seals.

Hochuli, U.↗

Organic inclusions within hydrothermal minerals from S.W. Africa and elsewhere.

It was observed that quartz crystals from veins within a diabase dike of precambrian age from S.W. Africa contain organic particles which closely resemble, in detailed morphology, coacervates, proteinoid microspheres or fossil and recent microorganisms. The microphotospectrographs in visible and near-ultraviolet light of these minute particles revealed a strong absorption peak at the vicinity of 4000 A, which is indicative of lipids. Hydrothermal mineral from veins from a number of other localities proved to contain the biomorphic organic particles. The theoretical significance of these organic particles is discussed with reference to problems of origin of life.

Mueller, G.↗

Sampling nitric oxide from combustion gases.

Experimental study of several sampling tube and probe material compositions and designs aimed at preventing nitric oxide reduction when sampling nitric oxide from combustion gases. A 250,000 Btu/h furnace fired with technical grade methane was used for testing the sampling probes over a wide range of air-fuel mixtures. The results obtained include the finding that the use of stainless steel in probes creates inaccuracies in near-stoichiometric and fuel-rich sampling in hydrocarbon flames. For very fuel-rich flames, water cooling is needed even in quartz probes to prevent significant reduction of nitric oxide.-

England, C.↗

Thermal shielding by subliming volume reflectors in convective and intense radiative environments.

The behavior of dielectric materials having densely packed internal scattering centers subject to extreme convective and radiative environments is analyzed. Experiments have shown that these materials act as volume reflectors of incident radiation even when the exposed surface is being eroded by thermochemical ablation. The analysis was applied to interpret experiments of subliming Teflon models exposed to combined radiative and convective fluxes up to 1.7 kW/sq cm for several seconds. Results show that, although the exposed surface receded at an apparently steady rate, the internal temperature climbed continually, due to internal absorption of radiation and would have caused failure internally if the test duration were extended a few seconds. Thus, performance is time-limited by the internal absorption coefficient. Results were obtained for larger configurations and other materials. Typically, Teflon shells may withstand radiant fluxes up to 20 kW/sq cm for about 5 sec and fritted quartz up to 50 kW/sq cm for about 8 sec (corresponding to the Jupiter entry).

Howe, J. T.↗

Impact gages for detecting meteoroid and other orbital debris impacts on space vehicles.

Impacts on space vehicles have been simulated using the McDonnell Douglas Aerophysics Laboratory (MDAL) Light-Gas Guns to launch particles at hypervelocity speeds into scaled space structures. Using impact gages and a triangulation technique, these impacts have been detected and accurately located. This paper describes in detail the various types of impact gages (piezoelectric PZT-5A, quartz, electret, and off-the-shelf plastics) used. This description includes gage design and experimental results for gages installed on single-walled scaled payload carriers, multiple-walled satellites and space stations, and single-walled full-scale Delta tank structures. A brief description of the triangulation technique, the impact simulation, and the data acquisition system are also included.

Mastandrea, J. R.↗

Evaporation rate and vapor pressure of selected polymeric lubricating oils.

A recently developed ultrahigh-vacuum quartz spring mass sorption microbalance has been utilized to measure the evaporation rates of several low-volatility polymeric lubricating oils at various temperatures. The evaporation rates are used to calculate the vapor pressures by the Langmuir equation. A method is presented to accurately estimate extended temperature range evaporation rate and vapor pressure data for polymeric oils, incorporating appropriate corrections for the increases in molecular weight and the change in volatility of the progressively evaporating polymer fractions. The logarithms of the calculated data appear to follow linear relationships within the test temperature ranges, when plotted versus 1000/T. These functions and the observed effusion characteristics of the fluids on progressive volatilization are useful in estimating evaporation rate and vapor pressure changes on evaporative depletion.

Gardos, M. N.↗

Mass flux measurements and correlations in the back flow region of a nozzle plume.

A series of tests were conducted to measure the mass flux in the far field of a nozzle plume in a high vacuum with emphasis on the back flow region. The measurements presented in this report provide fairly accurate data for off-axis angles as large as 140 deg (i.e., the back flow region). The tests utilized five different nozzles. Parameters such as expansion ratio, throat diameter, nozzle lip shape, and plenum (chamber) pressure were varied. Carbon dioxide and nitrogen gases were passed through, and mass flux measurements were taken using quartz crystal microbalances in as many as nine different locations relative to the test nozzle. The tests resulted in a large matrix of data that were correlated and compared to existing prediction theories. Several conclusions with respect to the effect of nozzle and gas parameters on the amount of back flow mass flux are offered, and it was demonstrated that gaseous mass fluxes, which are not predictable by present theories, are encountered in the region behind the nozzle exit plane.

Chirivella, J. E.↗

An ERTS multispectral scanner experiment for mapping iron compounds.

An experiment is described which is designed to produce visible-reflective infrared ratio images from ERTS satellite data. The ERTS-A multispectral scanner has two channels in the visible-reflective infrared wavelength region which should be capable of duplicating aircraft scanner results. The average reflectances in the four ERTS-A MSS spectral bands for a few minerals and some vegetation are tabulated. The mineral laboratory samples were granular, with a particle diameter range of 250 to 1200 micrometer. If there were no spectral atmospheric or illumination variation effects, the ratio of energies in band 1 to band 4 would permit discrimination of pyroxenes (found in basic and ultrabasic rocks), quartz (found in acidic rocks), limonite and hematite (iron oxides), and green vegetation, on the basis of their respective ratio magnitudes.

Vincent, R. K.↗