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DOE OSTI2024

Advanced Instrumentation for Metal Additive Manufacturing

Laser powder bed fusion (LPBF) is the most widely used process for metal additive manufacturing (AM), particularly where complex geometries provide performance advantages unattainable with traditional manufacturing techniques. However, LPBF is highly sensitive to innate variability in both the powder spreading and fusion steps, often leading to defects such as pores that are difficult to detect yet significantly impair component mechanical properties and fatigue life. This thesis presents a range of novel instruments enabling both precise assessment of powder layer characteristics and in-situ thermal metrology of metal AM to advance the quality control of LPBF. First, leveraging a custom X-ray microscope and a radiation-transport model developed through this work, transmission X-ray imaging is used to study spreading of thin metal powder layers. Effective layer depth is directly mapped at a process-relevant size scale, surpassing optical techniques that can only estimate local deposition from layer surface topography. Layer packing density and quality are shown to be influenced by powder flowability and particle size relative to nominal powder layer thickness. Layer quality is additionally connected to the geometry of the spreading implement and its velocity. This technique and its presented findings enable pairing feedstocks with spreading strategies that create layers with consistent packing density and uniformity. Second, a twofold approach is employed to optically interrogate the laser fusion step of LPBF for observing signatures of defect formation. Aperture division multiplexing is conceptualized, providing for simultaneous laser delivery and high-fidelity infrared (IR) process monitoring through a common optic. In-situ microscopy at 50 μm spatial resolution and at mid-wave IR wavelengths is proven readily achievable with the first purpose-built optic of this type. Next, a bespoke imaging spectrometer, along with a temperature-emissivity separation technique, is used to retrieve accurate process temperatures over a 1000 K range. Data from these instruments are correlated to porosity as fine as 4.3 μm in two LPBF test artifacts, as verified using computed tomography (CT), establishing the viability of robust optically-based component qualification.

Penny, Ryan↗

NASA NTRS1986

Fourier-Transform Infrared Spectrometer

Fourier-transform spectrometer provides approximately hundredfold increase in luminosity at detector plane over that achievable with older instruments of this type. Used to analyze such weak sources as pollutants and other low-concentration substances in atmosphere. Interferometer creates fringe patterns on two distinct arrays of light detectors, which observe different wavelength bands. Objective lens focuses scene on image plane, which contains optical chopper. To make instrument less susceptible to variations in scene under observation, field and detector lenses focus entrance aperture, rather that image, onto detector array.

Schindler, R. A.↗

NASA NTRS1988

A compact imaging spectrometer for studies of space vehicle induced environment emissions

On the basis of spectral measurements made from the Space Shuttle and on models of the possible Space Station external environment, it appears likely that, even at the planned altitudes of Space Station, photon emissions will be induced. These emissions will occur to some degree throughout the UV-visible-IR spectrum. The emissions arise from a combination of processes including gas phase collisions between relatively energetic ambient and surface emitted or re-emitted atoms or molecules, where the surface raises some species to excited energy states. At present it is not possible to model these processes or the anticipated intensity levels with accuracy, as a number of fundamental parameters needed for such calculations are still poorly known or unknown. However, it is possible that certain spectral line and band features will exceed the desired goal that contaminant emissions not exceed the natural zodiacal background. However, in the near infrared and infrared, it appears that this level will be exceeded to a significant degree. Therefore it will be necessary to monitor emission levels in the vicinity of Space Station, both in order to establish the levels and to better model the environment. In this note, we briefly describe a small spectrometer that is suitable for monitoring the spectrum from 1200A to less than or approximately 12,000A. This instrument uses focal plane array detectors to image this full spectral range simultaneously. The spectral resolution is 4 to 12A, depending on the portion of the wavelength range.

Torr, Marsha R.↗

DOE OSTI2026

Spectrometer-free quantitative vapor sensing and classification via spatiotemporal imaging of porous silicon metasurfaces

Metasurfaces offer a compact platform for optical vapor sensing, but their practical deployment has been limited by weak evanescent light–matter interactions and reliance on spectrally resolved instrumentation. Here, we report porous silicon (pSi) metasurfaces for spectrometer-free quantitative detection of volatile organic compounds (VOCs) with strongly enhanced light–matter interaction. The engineered porosity increases sensitivity by >100× relative to non-porous dielectric metasurfaces, enabling limits of detection of 1.65 ppm for methanol and 9.1 ppm for ethanol across a broad dynamic range (<10 ppm to >103 ppm). Imaging-based readout provides a lightweight, spectrometer-free pathway for real-time quantitative sensing. Beyond quantitative detection, the mesoporous architecture introduces adsorption–desorption kinetics as an additional information channel. Analysis of the resulting spatiotemporal signatures enables kinetic fingerprinting without reliance on infrared spectral features or surface functionalization, and a lightweight machine-learning classifier differentiates acetone, methanol, ethanol, and isopropanol with 91.6% accuracy. These results establish porous metasurfaces as spatiotemporal sensing elements that couple quantitative vapor detection with kinetic fingerprinting through real-time dynamical responses, enabling low-cost, high-performance optical sensors.

Dash, Tomoshree [Clemson University]↗

NASA NTRS1986

Trace element-induced stress in freshwater wetland vegetation: Preliminary results

Airborne Imaging Spectrometer (AIS) data were acquired over an area of freshwater wetlands in Central California on September 23, 1985. Plant samples were subsequently collected along the flight line with the goal of relating plant tissue chemistry to spectral reflectance in the near-infrared region. It was determined that a consistent relationship existed between spectral response and plant tissue chemistry. This was especially evident in the 1500 to 1700 nm region.

Wood, B. L.↗

NASA NTRS1993

Automatic definition of spectral units in the equatorial regions of Mars

ISM was the first instrument that acquired spectra of small areas (25x25 sq km) on a planetary surface. The data set consists mainly in images made up of about 3000 such pixels, each one corresponding to a near-infrared spectrum (0.76 to 3.15 microns in 128 spectral channels) with high signal-to-noise ratio. These data were used to define spectral units and to constrain the mineralogy of surface materials in the equatorial regions of the planet. Future spaceborne imaging spectrometers (e.g. OMEGA on board the Mars-94 Russian spacecraft) are expected to provide several hundred times as much data as ISM, so there's a strong need for fast and reliable processing methods. The present work is an attempt to define spectral units in the region of Syrtis Major-Isidis Planitia by means of G-mode analysis. The method allows to cluster the spectra according to their similarities; different levels of classification can be achieved by tuning a threshold of confidence.

Erard, Stephane↗

NASA NTRS2005

X-Ray Spectroscopy of Optically Bright Planets using the Chandra Observatory

Since its launch in July 1999, Chandra's Advanced CCD Imaging Spectrometer (ACIS) has observed several planets (Venus, Mars, Jupiter and Saturn) and 6 comets. At 0.5 arc-second spatial resolution, ACIS detects individual x-ray photons with good quantum efficiency (25% at 0.6 KeV) and energy resolution (20% FWHM at 0.6 KeV). However, the ACIS CCDs are also sensitive to optical and near-infrared light, which is absorbed by optical blocking filters (OBFs) that eliminate optical contamination from all but the brightest extended sources, e.g., planets. .Jupiter at opposition subseconds approx.45 arc-seconds (90 CCD pixels.) Since Chandra is incapable of tracking a moving target, the planet takes 10 - 20 kiloseconds to move across the most sensitive ACIS CCD, after which the observatory must be re-pointed. Meanwhile, the OBF covering that CCD adds an opt,ical signal equivalent to approx.110 eV to each pixel that lies within thc outline of the Jovian disk. This has three consequences: (1) the observatory must be pointed away from Jupiter while CCD bias maps are constructed; (2) most x-rays from within the optical image will be misidentified as charged-particle background and ignored; and (3) those x-rays that are reported will bc assigned anomalously high energies. The same also applies to thc other planets, but is less serious since they are either dimmer at optical wavelengths, or they show less apparent motion across the sky, permitting reduced CCD exposure times: the optical contamination from Saturn acids approx.15 eV per pixel, and from Mars and Venus approx.31 eV. After analyzing a series of short .Jupiter observations in December 2000, ACIS parameters were optimized for the February 2003 opposition. CCD bias maps were constructed while Chandra pointed away from Jupiter, and the subsequent observations employed on-board software to ignore any pixel that contained less charge than that expected from optical leakage. In addition, ACIS was commanded to report 5 x 5 arrays of pixel values surrounding each x-ray event, and the outlying values were employed during ground processing to correct for the optical contamination.

Ford, P. G.↗

NASA NTRS1983

An imaging spectrometer experiment for the Shuttle

An imaging spectrometer experiment concept for earth remote sensing, developed as part of NASA's Multispectral Linear Array program, will map a series of test sites at high spatial and spectral resolution from the vantage point of the Shuttle payload bay. The instrument covers the spectral range from 0.4 to 2.5 micrometers with a sampling interval of 10 nanometers in the visible and near infrared (to 1.0 micrometer) and 20 nanometers in the short wavelength infrared (1.0 to 2.5 micrometers). Resolution corresponding to a ground instantaneous field of view (pixel size) of 30 meters is provided over a swath width of 12 kilometers. On-board data editing is utilized to select a subset of the data stream for transmission to the ground. The instrument utilizes silicon and mercury cadmium telluride area array detectors. Pointing mirrors are included to permit specific test sites to be imaged from the Shuttle orbit.

Wellman, J. B.↗

DOE OSTI2020

Jupiter in the Ultraviolet: Acetylene and Ethane Abundances in the Stratosphere of Jupiter from Cassini Observations between 0.15 and 0.19 μm

At wavelengths between 0.15 and 0.19 μm, the far-ultraviolet spectrum of Jupiter is dominated by the scattered solar spectrum, attenuated by molecular absorptions primarily by acetylene and ethane, and to a lesser extent ammonia and phosphine. We describe the development of our radiative transfer code that enables the retrieval of abundances of these molecular species from ultraviolet reflectance spectra. As a proof-of-concept we present an analysis of Cassini Ultraviolet Imaging Spectrograph (UVIS) observations of the disk of Jupiter during the 2000/2001 flyby. The ultraviolet-retrieved acetylene abundances in the upper stratosphere are lower than those predicted by models based solely on infrared thermal emission from the mid-stratosphere observed by the Composite Infrared Spectrometer (CIRS), requiring an adjustment to the vertical profiles above 1 mbar. We produce a vertical acetylene abundance profile that is compatible with both CIRS and UVIS, with reduced abundances at pressures <1 mbar: the 0.1 mbar abundances are 1.21 ± 0.07 ppm for acetylene and 20.8 ± 5.1 ppm for ethane. Finally, we perform a sensitivity study for the JUICE ultraviolet spectrograph, which has extended wavelength coverage out to 0.21 μm, enabling the retrieval of ammonia and phosphine abundances, in addition to acetylene and ethane.

79 ASTRONOMY AND ASTROPHYSICS↗

NASA NTRS1983

The NASA MLA program

The NASA Multispectral Linear Array (MLA) program is structured to provide for the evolutionary development of advanced sensor concepts, technologies, and scientific basis for future remote sensing missions. Program elements include the development of multispectral visible and shortwave infrared (SWIR) detector arrays, optics and on-board signal processing technologies, sensor design studies, and supporting research. The research consists of advanced airborne sensor development with data acquisitions, field measurements, and supporting science studies. At the present time, two instrument concepts, including an imaging spectrometer, are in development as payloads for a series of Shuttle remote sensing research flights beginning as early as 1987. Progressively more advanced capability instruments suitable for extended duration Shuttle, free flyer, and space platform missions in the 1990's are also being studied.

Ando, K. J.↗

NASA NTRS1993

Galileo/NIMS near-infrared thermal imagery of the surface of Venus

Numerous highland and lowland features on the surface of Venus are observed in multispectral imagery acquired at approximately 50 km spatial resolution by the Near-Infrared Mapping Spectrometer (NIMS) on board the Galileo spacecraft in Feb. 1990. Specifically, such features are observed at 1.18 microns, a wavelength particularly sensitive to thermal emission from the hot, lower atmosphere (less than 10 km) and surface, and show up particularly well when this image is 'de-clouded' using a simultaneously-acquired 2.3-microns image of the upper, cloudy atmosphere. Due to the steep atmospheric temperature gradient (approximately 8 degrees per kilometer), hot lowland areas appear relatively bright, while cooler, highland areas appear dark (due to the steep atmospheric temperature gradient - approximately 8 degrees per kilometer - surface temperatures span approximately 100 K over the 13 kilometer range of surface altitudes observed in this image). Prominent highland features include Maxwell Montes (approximately 12 km altitude), Alpha Regio (2.5 km), Eistla Regio (approximately 2.0 km), Bell Regio (2-3 km), and the western edge of Aphrodite Terra (2-2.5 km). Low-lying regions include Sedna Planitia (-1.0 km), Tinatin Planitia (-0.5 km), and the Bereghinya Planitia (0 km). From correlations with radar altimetry maps, such imagery may place useful constraints on surface emissivity and temperature variations, as well as on the nature of continuum opacity of CO2 in the 1-micron region.

Carlson, R. W.↗

NASA NTRS1996

Design considerations for AIRES, an airborne infrared echelle spectrometer for SOFIA

The airborne infrared echelle spectrometer (AIRES) was proposed as a facility instrument for the stratospheric observatory for infrared astronomy (SOFIA) project. The preliminary AIRES design uses multiple two dimensional detector arrays and a 1.2 m long, 76 deg blaze angle echelle to combine high spectral resolution with diffraction limited imaging in the cross-dispersion direction. A preliminary optical design and the mechanical architecture are presented together with the analysis and prototyping of lightweight aluminum echelles. Instrument efficiencies are calculated and compared for different gratings, and the associated mechanical design tradeoffs are discussed.

Haas, Michael R.↗

NASA NTRS1983

Short wavelength infrared hybrid focal plane arrays

The employment of area focal plane arrays (FPA) has made it possible to obtain second generation infrared imaging systems with high resolution and sensitivity. The Short Wavelength Infrared (SWIR) region (1-2.5 microns) is of importance for imaging objects at high temperature and under conditions of reflected sunlight. The present investigation is concerned with electrooptical characterization results for 32 x 32 SWIR detector arrays and FPAs which are suitable for use in a prototype imaging spectrometer. The employed detector material is Hg(1-x)Cd(x)Te grown by liquid phase epitaxy on a CdTe transparent substrate. Attention is given to details of processing, the design of the detector array, the multiplexer, the fabrication of the hybrid FPA, and aspects of performance.

Vural, K.↗

NASA NTRS1998

Cryogenic Optical Performance of the Cassini Composite InfraRed Spectrometer (CIRS) Flight Telescope

The CIRS half-meter diameter beryllium flight telescope's optical performance was tested at the instrument operating temperature of 170 Kelvin. The telescope components were designed at Goddard Space Flight Center (GSFC) but fabricated out of house and then assembled, aligned and tested upon receipt at GSFC. A 24 inch aperture cryogenic test facility utilizing a 1024 x 1024 CCD array was developed at GSFC specifically for this test. The telescope,s image quality (measured as encircled energy), boresight stability and focus stability were measured. The gold coated beryllium design exceeded the cold image performance requirement of 80% encircled energy within a 460 micron diameter circle.

Losch, Patricia↗

NASA NTRS1998

Cryogenic Optical Performance of the Cassini Composite Infrared Spectrometer (CIRS) Flight Telescope

The CIRS half-meter diameter beryllium flight telescope's optical performance was tested at the instrument operating temperature of 170 Kelvin. The telescope components were designed at Goddard Space Flight Center (GSFC) but fabricated out of house and then assembled, aligned and tested upon receipt at GSFC. A 24 inch aperture cryogenic test facility utilizing a 1024 x 1024 CCD array was developed at GSFC specifically for this test. The telescope's image quality (measured as encircled energy), boresight stability and focus stability were measured. The gold coated beryllium design exceeded the image performance requirement of 80% encircled energy within a 432 microns diameter circle.

Losch, Patricia↗

NASA NTRS2002

A Chandra X-ray Study of Cygnus A: The Nucleus - 2

We report Chandra Advanced CCD Imaging Spectrometer and quasi-simultaneous Rossi X-Ray Timing Explorer (RXTE) observations of the nearby, powerful radio galaxy Cygnus A, with the present paper focusing on the properties of the active nucleus. In the Chandra observation, the hard (less than a few keV) X-ray emission is spatially unresolved with a size is approximately 1" (1.5 kpc, H(sub 0) = 50 km/s/Mpc) and coincides with the radio and near-infrared nuclei. In contrast, the soft (less than 2 keV) emission exhibits a bipolar nebulosity that aligns with the optical bipolar continuum and emission-line structures and approximately with the radio jet. In particular, the soft X-ray emission corresponds very well with the [O III] (lambda)5007 and H(alpha) + [N II] lambda(lambda)6548, 6583 nebulosity imaged with Hubble Space Telescope. At the location of the nucleus, there is only weak soft X-ray emission, an effect that may be intrinsic or result from a dust lane that crosses the nucleus perpendicular to the source axis. The spectra of the various X-ray components have been obtained by simultaneous fits to the six detectors. The compact nucleus is detected to 100 keV and is well described by a heavily absorbed power-law spectrum with Gamma(sub h) = 1.52(sup + 0.12, sub -0.12) (similar to other 0.12 narrow-line radio galaxies) and equivalent hydrogen column N(sub H)(nuc) = 2.0(sup +0.1, sub -0.1) x 10(exp 23)/sq cm. This 0.2 column is compatible with the dust obscuration to the near-infrared source for a normal gas-to-dust ratio. The soft (less than 2 keV) emission from the nucleus may be described by a power-law spectrum with the same index (i.e., Gamma(sub l) = Gamma(sub h), although direct fits suggest a slightly larger value for Gamma(sub l). Narrow emission lines from highly ionized neon and silicon, as well as a "neutral" Fe K(alpha) line, are detected in the nucleus and its vicinity (r approximately less than 2 kpc). The equivalent width (EW) of the Fe K(alpha) line (182(sup +40, sub -54) eV) is in good agreement with theoretical predictions for the EW versus N(sub H)(nuc) relationship in various geometries. An Fe K edge is also seen. The RXTE observations indicate a temperature of kT = 6.9(sup +0., sub -1.0) keV for the cluster gas (discussed in Paper III of this series) and cluster emission lines of Fe K(alpha) and Fe K(beta) and/or Ni K(alpha). We consider the possibility that the extended soft X-ray emission is electron-scattered nuclear radiation. Given that 1% of the unabsorbed 2 - 10 keV nuclear radiation would have to be scattered, the necessary gas column [N(sub H)(Scattering) approx. = 3.5 x 10(exp 22)/sq cm] would absorb the X-rays rather than scatter them if the gas is cold. Thus, the scattering plasma must be highly ionized. If this ionization is achieved through photoionization by the nucleus, the ionization parameter zeta greater than 1 ergs cm/s and the electron density n(sub e) approx. = 6 cc given the observed distance of the soft X-ray emission from the nucleus. The electron column density inferred from the X-ray observations is much too low to account for the extended optical scattered light, strongly suggesting that the polarized optical light is scattered by dust. The presence of highly ionized Ne lines in the soft X-ray spectrum requires 20 ergs cm/s approximately less than zeta approximately less than 300 ergs cm/s these lines may originate closer to the nucleus than the extended soft continuum or in a lower density gas. A collisionally ionized thermal model of the extended soft X-rays cannot be ruled out but is unattractive in view of the low metal abundance required (Z = 0.03 Z(mass)). The hard X-ray to far-infrared ratio for the nucleus of Cygnus A is similar to that seen in Seyfert 1 and unobscured radio galaxies. By means of the correlation between hard X-ray luminosity and nuclear optical absolute magnitude for these classes of object, we estimate M(sub B) = -22.4 for Cygnus A, near the .borderline between Seyfert galaxies and QSOs.

Young, Andrew J.↗

DOE OSTI2024

Multicolor Inks of Black Phosphorus for Midwave‐Infrared Optoelectronics

Abstract Black phosphorus (bP) based ink with a bulk bandgap of 0.33 eV ( λ = 3.7 µm) has recently been shown to be promising for large‐area, high performance mid‐wave infrared (MWIR) optoelectronics. However, the development of multicolor bP inks expanding across the MWIR wavelength range has been challenging. Here a multicolor ink process based on bP with spectral emission tuned from 0.28 eV ( λ = 4.4 µm) to 0.8 eV ( λ = 1.5 µm) is demonstrated. Specifically, through the reduction of bP particle size distribution (i.e., lateral dimension and thickness), the optical bandgap systematically blueshifts, reaching up to 0.8 eV. Conversely, alloying bP with arsenic (bP 1− x As x ) induces a redshift in the bandgap to 0.28 eV. The ink processed films are passivated with an infrared‐transparent epoxy for stable infrared emission in ambient air. Utilizing these multicolor bP‐based inks as an infrared light source, a gas sensing system is demonstrated that selectively detects gases, such as CO 2 and CH 4 whose absorption band varies around 4.3 and 3.3 µm, respectively. The presented ink formulation sets the stage for the advancement of multiplex MWIR optoelectronics, including spectrometers and spectral imaging using a low‐cost material processing platform.

Kim, Jae Ik↗

NASA NTRS2004

Undersampling Correction for Array Detector-Based Satellite Spectrometers

Array detector-based instruments are now fundamental to measurements of ozone and other atmospheric trace gases from space in the ultraviolet, visible, and infrared. The present generation of such instruments suffers, to a greater or lesser degree, from undersampling of the spectra, leading to difficulties in the analysis of atmospheric radiances. We provide extended analysis of the undersampling suffered by modem satellite spectrometers, which include Global Ozone Monitoring Experiment (GOME), Scanning Imaging Absorption Spectrometer for Atmospheric Chartography (SCIAMACHY), Ozone Monitoring Instrument (OMI), and Ozone Mapping and Profiler Suite (OMPS). The analysis includes basic undersampling, the effects of binning into separate detector pixels, and the application of high-resolution Fraunhofer spectral data to correct for undersampling in many useful cases.

Chance, Kelly↗