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At least 523 records · Page 29

Complete resolution across the neodymium/samarium isotopic envelope with a liquid sampling‐atmospheric pressure glow discharge — Orbitrap mass spectrometer

Rationale Nd and Sm isotope ratios play an important role in geological dating and as nuclear forensic signatures; however, the overlap of the respective 144, 148, 150 Nd/Sm isobars requires prior separations to be performed before analysis on typical MS platforms. The work presented here overcomes these isobaric interferences using ultrahigh‐mass resolution to alleviate interference without prior chemical separations. Methods A liquid sampling‐atmospheric pressure glow discharge ion source was coupled to a standard, QExactive Focus Orbitrap mass spectrometer, providing a mass resolution of ~80 k. A Spectroswiss FTMS booster X2 data acquisition package was used to collect extended transients, providing much higher mass resolution; ~230 k and ~600 k are employed here for Nd and Sm isotopes. Results While the standard Orbitrap resolution is far greater than typical “atomic” MS platforms, it was insufficient to alleviate all isobars. The use of a resolution of ~230 k resulted in baseline separation across the entire isotopic envelope for both Nd and Sm. Isotope ratios obtained from Nd:Sm mixtures using high‐resolution were equivalent to those found for individual‐element solutions, while isotope ratios obtained at a resolution of ~80 k (standard for the OEM data system) showed large deviations. Conclusions Use of ultrahigh‐resolution is an attractive alternative to extensive chemical separations to alleviate severe isobaric interferences. Sufficient mass resolution greatly reduces/eliminates the need for sample manipulations (separations) before analysis while reducing costs and total analysis times.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Small Hot Jet Acoustic Rig Validation

The Small Hot Jet Acoustic Rig (SHJAR), located in the Aeroacoustic Propulsion Laboratory (AAPL) at the NASA Glenn Research Center in Cleveland, Ohio, was commissioned in 2001 to test jet noise reduction concepts at low technology readiness levels (TRL 1-3) and develop advanced measurement techniques. The first series of tests on the SHJAR were designed to prove its capabilities and establish the quality of the jet noise data produced. Towards this goal, a methodology was employed dividing all noise sources into three categories: background noise, jet noise, and rig noise. Background noise was directly measured. Jet noise and rig noise were separated by using the distance and velocity scaling properties of jet noise. Effectively, any noise source that did not follow these rules of jet noise was labeled as rig noise. This method led to the identification of a high frequency noise source related to the Reynolds number. Experiments using boundary layer treatment and hot wire probes documented this noise source and its removal, allowing clean testing of low Reynolds number jets. Other tests performed characterized the amplitude and frequency of the valve noise, confirmed the location of the acoustic far field, and documented the background noise levels under several conditions. Finally, a full set of baseline data was acquired. This paper contains the methodology and test results used to verify the quality of the SHJAR rig.

Brown, Cliff↗

Defining Change Thresholds: What Change Is Outside Typical Sources of Variation?

Researchers often have a difficult time defining meaningful thresholds for change. We sometimes identify subtle changes but what amount of change is beyond typical sources of variation? This is especially complicated when trying to understand new disease pathogenesis like the constellation of eye changes leading to Spaceflight-associated Neuro-ocular Syndrome (SANS). To support decision makers in defining minimal meaningful change, we used a Bayesian hierarchical model to estimate innate sources of variability such as natural day to day variation. Healthy subjects were recruited and imaged with MRI, OCT, and US on separate days and measured by several technicians. Models were developed specifying random effects for the sources of variation – between left and right eyes, within-individuals over time, between raters, and finally between individuals. This allowed us to find the posterior distribution for the total typical variation, within an eye, which we use to define a threshold where change beyond typical sources of variation is likely. This threshold is now used as our earliest indicator of systematic increase in Total Retinal Thickness (a precursor to optic disc edema).

Millennia Young↗

Improved position and new optical candidate for A0538-66

An analysis of HEAO 1 modulation collimator data leading to an improved position determination and a new optical counterpart candidate for the transient X-ray source A0538-66 is reported. Data obtained during five outbursts, all of which were separated by 16.7 days or a small multiple thereof, indicates that the outbursts, although of varying duration, intensity, and hardness ratio originated from the same source, at a position of 5 h 35 min 42.7 sec RA and 66 deg 53 arcmin 44 arcsec dec. The improved position determination is found to exclude the previously suggested optical counterpart, and a search of archive plates of the Large Magellanic cloud in the refined error regions has lead to the tentative identification of a B-type star with an observed B variability of 1 mag with the X-ray source.

Johnston, M. D.↗

Three precise gamma-ray burst source locations

The precise source regions of three moderately intense gamma ray bursts are derived. These events were observed with the first interplanetary burst sensor network. The optimum locations of the detectors, widely separated throughout the inner solar system, allowed for high accuracy, over-determined source fields of size 0.7 to 7.0 arc-min(2). All three locations are at fairly high galactic latitude in regions of low source confusion; none can be identified with a steady source object. Archived photographs were searched for optical transients that are able to be associated with these source fields; one such association was made.

Cline, T. L.↗

Three precise gamma-ray burst source locations

The precise source regions of three moderately intense gamma ray bursts are derived. These events were observed with the first interplanetary burst sensor network. The optimum locations of the detectors, widely separated throughout the inner solar system, allowed for high accuracy, over-determined source fields of size 0.7 to 7.0 arc-min(2). All three locations are at fairly high galactic latitude in regions of low source confusion; none can be identified with a steady source object. Archived photographs were searched for optical transients that are able to be associated with these source fields; one such association was made.

Cline, T. L.↗

Shadow mask for X-ray spectrometer

Imaging technique may be used in series with flat or conical Bragg crystals to separate spatial/spectral convolution when spectrometer is scanned across extended source emitting at more than one wavelength. Technique allows line direction and continuum to be detected and provides data for spatial mapping of source.

Woodgate, B. E.↗

Time-dependent radio fine structure of the quasar 3C 345

Results are reported for VLBI observations of 3C 345 at a wavelength of 3.8 cm with left circular polarization. Sixteen sets of correlated flux densities and three sets of closure phases were obtained from observations made over a three-year period with six independent interferometers formed from up to four antennas. The mathematical models employed to represent the radio brightness distribution of the source are described, and the data are analyzed on the basis of a two-component model. The results show that the compact source in 3C 345 consists of two components whose separation increased by about 0.3 milliarcsec over the observational period, that the smaller and weaker component is to the east and south of the larger and stronger one, and that the apparent expansion velocity would be about 2.5c for a redshift of 0.6, a Hubble constant of 60 km/sec per Mpc, and a deceleration parameter of unity. It is concluded that these findings are difficult to reconcile with the 'Christmas tree' model for the apparent change of separation with time over any given series of observations.

Wittels, J. J.↗

Baffle design for earth radiation rejection in the Cryogenic Limb-Scanning Interferometer/Radiometer

The Cryogenic Limb-Scanning Interferometer/Radiometer (CLIR) is being developed to observe infrared emissions of the earth's upper atmosphere from space. The earth's surface is an extended source of intense background radiation with a small angular separation from the desired scene. The CLIR employs an off-axis Gregorian Telescope whose primary mirror and baffles are cooled by an open-cycle cryogen system. A system of specular annular baffles has been developed to minimize both stray light problems and cryogen consumption by retro-mapping the aperture into itself. Each off-axis ray which enters the aperture and strikes the specular baffle surface is reflected so that it passes out of the aperture and is not absorbed on a cryogenic surface. The specular baffle which lies closest to the aperture is an ellipsoid whose foci trace out the circular aperture on revolution about the axis. Its theoretical 'ray trace' efficiency is 100 percent. A subsequent baffle has an elliptical cross section whose near focus traces out the central hole in the ellipsoidal baffle and whose far focus traces out the aperture. Its theoretical efficiency is about 90 percent. These baffles reduce the earth radiation heat load on the cryogenic cooler by an order of magnitude, changing it from the dominant cause of cryogen consumption to a relatively small effect. An aperture shield is also desirable to reduce cryogen consumption, stray light, and contamination.

Bremer, J. C.↗

Workshop on Two-Phase Fluid Behavior in a Space Environment

The Workshop was successful in achieving its main objective of identifying a large number of technical issues relating to the design of two-phase systems for space applications. The principal concern expressed was the need for verified analytical tools that will allow an engineer to confidently design a system to a known degree of accuracy. New and improved materials, for such applications as thermal storage and as heat transfer fluids, were also identified as major needs. In addition to these research efforts, a number of specific hardware needs were identified which will require development. These include heat pumps, low weight radiators, advanced heat pipes, stability enhancement devices, high heat flux evaporators, and liquid/vapor separators. Also identified was the need for a centralized source of reliable, up-to-date information on two-phase flow in a space environment.

Swanson, Theodore D.↗

The relation between FIR and H I emission in galaxies

This project explored the relationship between the global far-infrared and neutral hydrogen (H I) emission from galaxies, based on data from the Infrared Astronomy Satellite (IRAS) and published radio data. 100 and 60 micron IRAS fluxes were used to establish a temperature corrected measure of the cold dust emission, and H I fluxes were drawn from the literature with the greatest possible consistency. The degree of correlation between the FIR and H I fluxes was found to be better than in previous studies, comparable to the correlation previously found between FIR and CO fluxes. The improvement was obtained largely by (1) separating 'stripped' from 'unstripped' galaxies, and (2) using compatible sources of H I data. Stripping occurs in clusters of galaxies and is probably caused by ram-pressure effects as a galaxy travels through the intergalactic medium. Our results suggest that stripped galaxies have had their outer-disk gas removed (approximately 80% of their total H I) while retaining most of their 100-micron-emitting dust. This strongly shifts the ratio of their 100-micron-to-H I fluxes. The second problem, arising from diverse sources of data, arises because differing telescopes and observational techniques give rise to substantial disagreement in the measured H I flux, and this degrades the correlation of the FIR and H I fluxes.

Schneider, Stephen E.↗

The Real-Time Wall Interference Correction System of the NASA Ames 12-Foot Pressure Wind Tunnel

An improved version of the Wall Signature Method was developed to compute wall interference effects in three-dimensional subsonic wind tunnel testing of aircraft models in real-time. The method may be applied to a full-span or a semispan model. A simplified singularity representation of the aircraft model is used. Fuselage, support system, propulsion simulator, and separation wake volume blockage effects are represented by point sources and sinks. Lifting effects are represented by semi-infinite line doublets. The singularity representation of the test article is combined with the measurement of wind tunnel test reference conditions, wall pressure, lift force, thrust force, pitching moment, rolling moment, and pre-computed solutions of the subsonic potential equation to determine first order wall interference corrections. Second order wall interference corrections for pitching and rolling moment coefficient are also determined. A new procedure is presented that estimates a rolling moment coefficient correction for wings with non-symmetric lift distribution. Experimental data obtained during the calibration of the Ames Bipod model support system and during tests of two semispan models mounted on an image plane in the NASA Ames 12 ft. Pressure Wind Tunnel are used to demonstrate the application of the wall interference correction method.

Ulbrich, Norbert↗

Confirmation of NLDN Long Range Strike Locations with LIS Observations

This study compares the lightning locations reported by the National Lightning Detection Network (NLDN) with the lightning locations determined by the Lightning Imaging Sensor (LIS). The NLDN system identifies the rf signature of cloud-to-ground lightning. The LIS data is the top level of a hierarchy of optical data objects. The centroid and timing of each LIS lightning activity center are compared with each flash in a subset of the NLDN long range lightning location data in a portion of the Atlantic Ocean and the Caribbean Sea consisting of those locations more than 625 km from any sensor. This subset is produced by analyzing each reported NLDN location to determine if that location is within the LIS field of view at the time of the reported flash. The Tropical Rainfall Measuring Mission Satellite (TRMM) orbit limits the cross-sensor comparison to tropical and sub-tropical regions. Because the rf-detection system depends on ionospheric propagation conditions, a separate analysis was made for daylight conditions at both source and sensor as well as nighttime at both places. A full year of data is compared to provide an adequate sample of each data set. Confirmation of lightning in the general location of the NLDN report is established when LIS detected one or more centers of lightning activity within a 2 degree radius from the NLDN location.

Boeck, William↗

Radiolytic Model for Chemical Composition of Europa's Atmosphere and Surface

The overall objective of the present effort is to produce models for major and selected minor components of Europa s neutral atmosphere in 1-D versus altitude and in 2-D versus altitude and longitude or latitude. A 3-D model versus all three coordinates (alt, long, lat) will be studied but development on this is at present limited by computing facilities available to the investigation team. In this first year we have focused on 1-D modeling with Co-I Valery Shematovich s Direct Simulation Monte Carlo (DSMC) code for water group species (H2O, O2, O, OH) and on 2-D with Co-I Mau Wong's version of a similar code for O2, O, CO, CO2, and Na. Surface source rates of H2O and O2 from sputtering and radiolysis are used in the 1-D model, while observations for CO2 at the Europa surface and Na detected in a neutral cloud ejected from Europa are used, along with the O2 sputtering rate, to constrain source rates in the 2-D version. With these separate approaches we are investigating a range of processes important to eventual implementation of a comprehensive 3-D atmospheric model which could be used to understand present observations and develop science requirements for future observations, e.g. from Earth and in Europa orbit. Within the second year we expect to merge the full water group calculations into the 2-D version of the DSMC code which can then be extended to 3-D, pending availability of computing resources. Another important goal in the second year would be the inclusion of sulk and its more volatile oxides (SO, SO2).

Cooper, John F.↗

Spectral Separation of the Turbofan Engine Coherent Combustion Noise Component

The core noise components of a dual spool turbofan engine (Honeywell TECH977) were separated by the use of a coherence function. A source location technique based on adjusting the time delay between the combustor pressure sensor signal and the far-field microphone signal to maximize the coherence and remove as much variation of the phase angle with frequency as possible was used. While adjusting the time delay to maximize the coherence and minimize the cross spectrum phase angle variation with frequency, the discovery was made that for the 130 microphone a 90.027 ms time shift worked best for the frequency band from 0 to 200 Hz while a 86.975 ms time shift worked best for the frequency band from 200 to 400 Hz. Since the 0 to 200 Hz band signal took more time to travel the same distance, it is slower than the 200 to 400 Hz band signal. This suggests the 0 to 200 Hz coherent cross spectral density band is partly due to indirect combustion noise attributed to hot spots interacting with the turbine. The signal in the 200 to 400 Hz frequency band is attributed mostly to direct combustion noise.

Miles, Jeffrey Hilton↗

Improving the Near-Earth Micrometeoroid and Orbital Debris Environment Definition with LADC

The Large Area Debris Collector (LADC) is a 10 m(sup 2) aerogel and acoustic sensor system designed to characterize and collect submillimeter micrometeoroids and orbital debris on the International Space Station (ISS). The project is led by the U.S. Naval Research Laboratory (NRL) with major collaboration by the NASA Orbital Debris Program Office at Johnson Space Center. The U.S. Department of Defense Space Test Program (STP) is responsible for the integration, deployment, and retrieval of the system. The deployment is scheduled for August 2007 with an orbital collection period of one to two years. The combined area time product of LADC will provide a much needed orbital debris population update in the size regime that is important to the safety community - 100 mm and larger. Another key element for LADC is the source identification of the collected samples. Impact features such as track length and track volume can be used to estimate the impact speed and direction of any selected residual embedded in aerogel. Acoustic sensors can provide impact timing and impact location information. The combined dynamical signatures make it possible to reconstruct the orbits of some of the collected samples and lead to their source identification. Compositional analysis on the residuals can also separate debris from meteoroids and provide additional population breakdown for orbital debris (e.g., Al, paint, steel, Al2O3). To maximize the science return and minimize potential contamination from other ISS modules, a careful selection of the location and orientation of LADC on the ISS is needed. Key issues and engineering constraints encountered during mission preparation, and the expected science return based on the mission configuration, are summarized in this paper.

Liou, J.-C.↗

Growth and Saturation of Ion Acoustic Waves in Hall Thrusters

In this paper we present for the first time a conjecture that the electron transport in Hall thrusters is controlled by ion acoustic waves in two distinct ion populations. The first, and largest population, is the main beam, an ion fluid generated upstream of the Acceleration Region. These ions experience electrons with largest ExB drift, but because beam ions have been heated during the ionization process, Landau damping limits the growth of ion acoustic waves. The second population is composed of ions generated at low potentials farther downstream that don’t thermalize with the fast moving ion beam. The existence of this separate population has been recognized for decades as the source of the high angle ions in Hall thruster plumes. Because these ions aren’t heated and have velocities much different from main beam ions, the amplitude of ion acoustic waves in this population is not Landau damped and grows to saturation. Scattering from these waves reduces the Hall parameter in the near plume where slow ions make up a significant fraction of the population.

Katz, Ira↗

X-Ray Computed Tomography During Preliminary Examination of Apollo Drive Tube 73001

Introduction: Starting in 2019, the Apollo Next Generation Sample Analysis (ANGSA) Program has enabled consortium studies of specially curated Apollo samples that were previously unstudied (or under studied). This began with unsealed core tube 73002 [1,2] that is the upper part of a station 3 double drive tube. More recently the pro-gram extended to the study of a variety of frozen Apollo 17 samples [3], as well as the gas extraction [4] and dis-section [5] of 73001, the lower half of the station 3 double drive tube, that was sealed under vacuum on the Moon. In this abstract we will examine the role of X-ray Computed Tomography (XCT) during the preliminary examination process for sealed core 73001, including: (1) engineering scans to aid in understanding the gas extraction process, whole-core scanning prior to opening to inform extrusion and dissection work, and (3) individual particle scanning to characterize rock fragment lithologies for follow on studies. Methodology: Sample 73001 is a 33 cm long, 4 cm diameter regolith sample collected inside a drive tube (~1 mm aluminum walls). That drive tube was sealed inside a 0.5 mm thick stainless steel (SS) Core Sample Vacuum Container (CSVC). XCT scans for engineering purposes were done on the Nikon XTH 320 system at Johnson Space Center using the 225 kV multi-metal reflection source at 215 kV, 179 A, and a 38.49 m voxel size. Individual >4 mm particles separated from the core during processing (then triply sealed in Teflon bags) were also scanned at JSC using the 180 kV source at 90 kV, 33 A, and a 2.98 – 10.65 m voxel size. Whole-core scans were done at the University of Texas High-Resolution X-ray Computed Tomography Facility (UTCT) on the 225 kV reflection source on the North Star Imaging cabinet XCT system. These scans included: (1) a series of 9 overlapping super-resolution scans each covering a ~4 cm length of the tube at 190 kV, 180 µA, and a 12.9 µm voxel size and (2) a lower resolution continuous helical scan of the entire core at 190 kV, 180 µA, and a 51.8 µm voxel size. Progress and Results: Before piercing and extracting the gas from sample 73001, an XCT scan of the bottom portion of the CSVC was used to confirm the location of the Teflon cap on the inner drive tube, to ensure it was not accidentally pierced during gas extraction. Similarly, after piercing, the bottom and top portions of the CSVC were scanned in order to capture engineering knowledge about the results of the piercing process, as well as the metal knife edge vacuum seal (SS into In-Ag alloy). Both scans will provide constraints on future work of this type, particularly for samples collected during the Artemis mission. Another finding from these "engineering" scans was that the device in the drive tube that immobilizes the regolith (the keeper) was not seated in the tube properly. This meant that (1) the drive tube could not be removed from the CSVC for the trip to UTCT, and (2) the procedure for opening and extruding the drive tube had to be modified. Had either of these things not been known prior to opening the CSVC, it could have led to an inability to XCT scan the whole core at high resolution and/or potential disruption of the core stratigraphy during extrusion. At UTCT, the entire length of the core was scanned at high resolution (12.9 microns per voxel). This scan serves multiple purposes: (1) A lower resolution (and uncorrected) version of these scans stitched together was used to help inform the processors of potential pitfalls during extrusion and dissection; and (2) the full resolution corrected data will serve as the permanent in situ record of the stratigraphy of the sample and will enable future researchers to perform a variety of analyses. So far, 92 of the 121 >4 mm particles separated during dissection pass 1 of sample 73001 have been individually scanned. These scans clearly show the lithology of each particle while keeping the particles in pristine condition. Because of the dust adhering to particle exteriors it would otherwise be impossible to determine lithologies in a non-contaminating way. Thus far the types of lithologies seen in sample 73001 (e.g., regolith breccias, impact-melt breccias, agglutinates, and basalts) are similar to those previously identified in sample 73002 [2]. By the time of the meeting, all particles from all 3 dissection passes will have been scanned and statistics on the different lithologies in 73001 compiled. References: [1] Shearer et al. (2020) 51st LPSC, abstract 1181. [2] Zeigler et al. (2020) 51st LPSC, abstract 3023. [3] Kent et al. (2022) This Volume. [4] McDonald et al. (2022) European Lunar Symposium. [5] Gross et al (2022) This volume.

Moon↗