Basic studies on dispersion hardening
Transmission electron microscopy and X-ray diffraction observations of substructure and elastic strains in cold worked and annealed dispersion strengthened alloys
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Transmission electron microscopy and X-ray diffraction observations of substructure and elastic strains in cold worked and annealed dispersion strengthened alloys
Nonuniform stock removal, quenching rate, cold working, hardness, and aging factors affect on chemical milling characteristics of aluminum alloys
The inelastic deformation of engineering alloys was recently shown to be rate (time)-dependent at room temperature. Experiments reported herein demonstrate that inelastic strain path length is a suitable measure for the modeling of work hardening for these materials, whereas inelastic work is not appropriate. The measured deformation induced temperature change is well predicted by a previously proposed theory of thermomechanical coupling. It has been derived by neglecting the stored energy of cold work and by assuming tha the internal energy expression for thermoelasticity is valid even when the mechanical deformation is inelastic.
This UNT Senior design team was tasked by NASA to develop a variable conductance thermal radiator prototype for CO2 deposition for deep space transit. NASA selects university teams every year to partake in the X-HAB Academic Innovation Challenge, with this year’s number of teams being six. Air Revitalization is a crucial system for any space travel, be it for Low Earth Orbit, such as the International Space Station, or for deep space transit. Current systems, such as the Carbon Dioxide Removal Apparatus aboard the ISS, require upkeep and maintenance, which cannot be done on long distance space missions. For the past several years, NASA has done research on Cryogenic systems for Carbon Dioxide removal. These systems operate on the fact that Carbon Dioxide freezes at a higher temperature than Oxygen and Nitrogen, so Carbon Dioxide can be frozen out of the cabin atmosphere without the use of filters, which degrade over time. To cool the cabin air down to a temperature where Carbon Dioxide freezes, Stirling cryocoolers have been used, which have shown promise in the hope of Carbon Dioxide deposition for Cabin Air Revitalization. Cryogenic systems are much more reliable but require significant energy input to operate. Physical systems, such as radiators, have generally not been used for this task, as there is a need to be able to “turn off” the rejection of heat to allow the frozen carbon dioxide to be collected. However, with working fluids pumped through a physical radiator, that aspect of operation can be achieved. The goal of this challenge is to determine the effectiveness of a variable conductance thermal radiator that can reject heat to deep space, without the use of a dedicated cryocooler to remove energy from the cabin air. The proposed design uses piping, hot and cold working fluids, and non-condensable gas to absorbl heat from the cabin air on one side of the radiator and reject the heat to deep space by means of thermal radiation. As well, the system will allow for the recovery of deposited Carbon Dioxide. The UNT X-HAB 2021 team will create a model radiator and test its performance with simulated heat sources and sinks and extrapolate those data points to analyze for real world conditions.
TiNiPt shape memory alloys are particularly promising for use as solid state actuators in environments up to 300 C, due to a reasonable balance of properties, including acceptable work output. However, one of the challenges to commercializing a viable high-temperature shape memory alloy (HTSMA) is to establish the appropriate primary and secondary processing techniques for fabrication of the material in a required product form such as rod and wire. Consequently, a Ti(50.5)Ni(29.5)Pt20 alloy was processed using several techniques including single-pass high-temperature extrusion, multiple-pass high-temperature extrusion, and cold drawing to produce bar stock, thin rod, and fine wire, respectively. The effects of heat treatment on the hardness, grain size, room temperature tensile properties, and transformation temperatures of hot- and cold-worked material were examined. Basic tensile properties as a function of temperature and the strain-temperature response of the alloy under constant load, for the determination of work output, were also investigated for various forms of the Ti(50.5)Ni(29.5)Pt20 alloy, including fine wire.
A tool is designed which facilitates the forming of wire grids used in manufacturing strain gage grids. Flattening the grid wire by a cold working process produces a stabilized grid which can be readily handled for storage or shipment.
Magnetization experiments in superimposed dc and audiofrequency ac magnetic fields on cold worked NbTi alloy samples - ac field induced flux jumps
Cold working and aging prepares nickel alloys for coiling into springs with properties acceptable in a cryogenic environment.
Shear wave refraction for ultrasonic detection of residual stress in cold-worked aluminum
Axial load fatigue endurance distributions of annealed oxygen free high conductivity copper specimens with cold worked surface layer tested at four stress levels
Crack tolerance factors for titanium alloys including cryogenic temperatures, heat treatment, cold working, etc
Cold work and heat treatment effects on Hastelloy X grain size and properties
Superconducting properties of polycrystalline disordered cold worked Nb-Ti-V alloys showing unexpected sensitivity to fast neutron irradiation
Plastic deformation effects on superconductivity of wire specimens of high purity Pb, In and Tl cold worked at liquid He and annealed
The elastic and plastic deformation behavior of high-purity aluminum and of dilute aluminum alloys is reviewed. Reliable property data, including elastic moduli, elastic coefficients, tensile, creep, fatigue, hardness, and impact are presented. Single crystal tensile results are discussed. Rather comprehensive reference lists, containing publications of the past 20 years, are included for each of the above categories. Defect structures and mechanisms responsible for mechanical behavior are presented. Strengthening techniques (alloys, cold work, irradiation, quenching, composites) and recovery are briefly reviewed.
Metallurgical condition was shown to have a significant effect on the creep properties of ASTAR-811C (Ta-8W-1Re-0.7Hf-0.025C) sheet. Cold worked material exhibited creep rates 30 times higher than solution annealed material and 10 times greater than for recrystallized material. Both grain size and the carbide morphology changes as the final annealing temperature was raised from 3000 F to 3600 F. However, the lowest creep rates were achieved for material which retained the high temperature form of the Ta2C precipitate. Samples with GTA weldments had essentially identical properties as recrystallized base metal. Cooling rates from 3600 F of 5, 50, and 800 F deg/min. had little effect on the 2000 and 2400 F creep behavior of ASTAR-811C.
The deformation and annealing response of TD-nickel chromium (TD-NiCr) 0.1 inch thick sheet was examined using various cold-rolling and annealing treatments. Upon annealing (above 816 C (1500 F), the as-received material was converted from an initially ultra-fine grain size (average grain dimension 0.51 micron) to a large grain structure. Increases in grain size by a factor of 100 to 200 were observed for this transformation. However, in those material states where the large grain transformation was absent, a fine grain recrystallized structure formed upon annealing (above 732 C (1350 F)). The deformation and annealing response of TD-NiCr sheet was evaluated with respect to the processing related variables as mode and severity of deformation and annealing temperature. Results indicate that the large grain transformation, classical primary recrystallization occurs. Using selected materials produced during the deformation and annealing study, the elevated temperature tensile properties of TD-NiCr sheet were examined in the temperature range 593 C (1100 F) to 1093 C (2000 F). It was observed that the elevated temperature tensile properties of TD-NiCr sheet could be optimized by the stabilization of a large grain size in this material using the cold working and/or annealing treatments developed during the present investigation.
Deformation processing has not been seriously considered as applicable to composite fabrication, particularly if the filament (e.g., boron) lacks plasticity. When, however, the brittle filament is clad with a ductile matrix such as 6061 Al, the underlying filament is protected from damage even when cold worked severely as in drawing and rolling. These two metal-working processes have been applied successfully to produce seven ply aluminum 50 vol % boron tubes up to 2 in. O.D. by 3 feet in length and flats 1 in. in width by 2 feet in length respectively. Although adequate densification is achieved via drawing and rolling, the former has been given major emphasis. Mechanical properties of rolled and drawn flats and tubes compare favorably with those prepared by static methods. However, the objective of the presentation is to focus on lower processing costs. In specific terms, 2 in. tubes in lengths up to 12 feet can be produced for as little as $150/lb. This is possible only because standard drawbench and carbide dies can be utilized. Furthermore, the major steps including cladding, preform preparation and drawing are conducive to automation.