Development and tests of small fused silica models of transparent walls for the nuclear light bulb engine
Developing test program for small fused silica models of transparent walls for nuclear light bulb engine
Vogt, P. G.↗
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Dimensional stability of fused silica and several ultralow expansion materials
Description of a program of measurements of the dimensional stability of fused silica and several ultralow thermal expansion materials. The two techniques used are: (1) Fizeau interferometry employed by NBS-Corning, and (2) Fabry-Perot interferometry employed by the Optical Science Center, University of Arizona. In the latter, a measurement accuracy of one part in a billion is sought.
Jacobs, S. F.↗
Hypervelocity impact damage tolerance of fused silica glass
A test program was conducted at the NASA/Johnson Space Center (JSC) concerning hypervelocity impact damage in fused silica glass. The objectives of this test program were: to expand the penetration equation data base in the velocity range between 2 and 8 km/s; to determine how much strength remains in a glass pane that has sustained known impact damage; and to develop a relationship between crater measurements and residual strength predictions that can be utilized in the Space Shuttle and Space Station programs. The results and conclusions of the residual strength testing are discussed below. Detailed discussion of the penetration equation studies will follow in future presentations.
Edelstein, K. S.↗
Pulse-length dependence of the laser-induced damage behavior of a fused-silica antireflective metasurface
A broadband, antireflective metasurface optic on a silica substrate is subjected to laser-induced damage-threshold measurements to quantify its performance under exposure to high-intensity/fluence laser pulses in the near-infrared at four pulse durations, ranging from 20 fs to 1.4 ns. The performance of the metasurface is benchmarked against that obtained from an equivalent bare fused-silica substrate that did not receive reactive-ion-etching metasurface treatment. Results showed that the damage threshold of the antireflective metasurface was always lower than the input-surface damage threshold of the untreated substrate. The damage initiations with nanosecond and picosecond pulses resulted in localized modification and removal of the nanostructures, whereas the onset of laser-induced modification with 20-fs pulses in a vacuum environment manifested as changes in the optical and electronic properties without significant material removal. The broader goal of this work is to develop a preliminary understanding of the laser-induced failure mechanisms of silica-based metasurface optics.
antireflection↗
Literary review and modeling outlook for radiation damage in fused-silica optical fibers
The purpose of this document is to distill, from literature, the effects of radiation damage in fused-silica optical fibers. This information will be used to design a theoretical framework capable of predictive modeling that will be published elsewhere. By inspection of the relevant literature, the devised method is calculation of defect amorphous structures by molecular dynamic techniques, and computation of the macroscopic dielectric function using density functional theory. The dielectric function is then used to directly compute the transmittance of the core material before and after irradiation via solution of Maxwell’s equations in a homogeneous medium.
73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
Optical absorption coefficients of fused silica in the wavelength range 0.17 to 3.5 microns from room temperature to 980 deg C
Optical absorption coefficient of fused silica in wavelength range 0.17 to 3.5 microns from room temperature to 980 deg. C
SPECTROPHOTOMETRY↗
Performance of fused silica as a filter in a wide field-of-view earth radiation budget radiometer
The thermal response of the fused silica dome filter in an earth radiation budget WFOV shortwave channel conceptual design and the impact of that response on the channel measurement, is described. Attention is given to results from design definition and performance analysis studies. Consideration is given to problems associated with achieving the desired levels of confidence in a high accuracy filtered earth radiation budget WFOV radiometer. Finally, design approaches, ground calibration, and data reduction techniques that minimize measurement uncertainties are covered.
Cooper, J. E.↗
Repair strategy for fused silica wedged focus lens with high-density filamentary damage
The National Ignition Facility (NIF) is intentionally operated with the final fused silica glass (SiO2) optics exposed to fluences and intensities with the potential to induce damage that will grow with additional laser exposure. Therefore, the NIF operates a recycle loop to refurbish final optics by mitigating any initiated surface damage to arrest its growth. However, the morphology of filamentary damage, caused by local self-focusing in the bulk of a silica optic, adds complexity to optics mitigation and provides a limitation to optic reusability. Here, we evaluate techniques for mitigating isolated and clustered filamentary damage. Optical microscopy before and after installation on NIF was used to determine the efficacy of filamentary mitigation after a series of high fluence and intensity laser exposures. The challenges and success rate of the methods are compared for various filamentary damage mitigation strategies.
National Ignition Facility↗
Optical transmittance of fused silica during irradiation processes.
The level of irradiation-induced optical absorption and the resulting heat deposition in the transparent fused-silica wall of a nuclear light bulb engine during normal operation are investigated by means of a series of related experiments using available radiation sources, each of which simulates some aspect of the radiation flux or dose of the engine. A comparison of the results obtained in electron and reactor experiments indicates that the generation of optical absorption is due to ionizing effects and that neutron-caused displacement effects do not contribute significantly to optical absorption. The implications of these and other results obtained are discussed.
Palma, G. E.↗
Subsurface mechanical damage of fused silica glass during grinding by various sub-aperture tools with and without ultrasonics
The subsurface mechanical damage (SSD) depth after grinding fused silica glass with a comprehensive set of sub-aperture fixed abrasive grinding tools [cup, wheel, belt, pad, and rotary face mill (with and without ultrasonics)] and process parameters has been statistically measured using the taper wedge technique and evaluated. Consistent with a previously reported grinding model [J. Non-Cryst. Solids 352, 5601–5617 (2006) Crossref , Materials Science and Technology of Optical Fabrication (Wiley & Sons, 2018)], based on the sliding indentation fracture by sliding particles or asperities where the normal load per particle determines the depth of the fracture (and ultimately the overall SSD depth), the dominant factor controlling SSD depth was found to be the abrasive size regardless of the tool type and process conditions. Compared to full aperture grinding methods, the overall SSD depth was higher using the sub-aperture tools, likely due to the higher effective pressure and higher load per particle distribution. Here, in addition to abrasive size, a significant reduction in SSD depth was achieved by: (1) reducing the load distribution on the abrasive particles via increase in contact area and/or decrease in mechanical loading; (2) using a more compliant host tool medium; and (3) in what we believe is a more novel way, using ultrasonics. Combining low abrasive size, larger contact area, and a compliant host, the 6 µm diamond in a resin matrix (Trizact) on a foam pad led to very low SSD depth (~ 4.6 µm), relatively fast grinding rate (186 mm 3 /h), and little or no figure degradation. This grinding tool/process is an attractive choice for final grind, resulting in significantly reduced polish out (i.e., “grey out”) times. With the rotary face mill tool, the use of ultrasonics consistently led to a SSD depth reduction (ranging from 17%–34%). A new fracture mechanics-based model, to the best of our knowledge, where the relevant normal load is parallel to the feed direction, has been developed to explain how ultrasonics leads to lower SSD depth. The key factors, supported by finite element stress analysis and load measurements, are (1) the initiation of fractures at higher z heights during the tool’s ultrasonic vertical oscillations, thus propagating less deep into workpiece; (2) reduction in load (and therefore reduction in fracture propagation distance) due to smaller tool-workpiece feed direction contact area (again caused by higher heights relative to depth of cut); (3) upward movement of the tool during oscillation leads to fracturing toward the surface instead into the depth; and finally (4) at tool’s lowest point of oscillation cycle, there may not be enough time for the fracture to propagate to its full length.
Optics and optical instruments↗
Dependence of growth rate of quartz in fused silica on pressure and impurity content
The effects of pressure, temperature, and some variations in impurity content on the growth rate u of quartz into fused silica were measured. Under all conditions the growth rate was interface controlled and increased exponentially with pressure with an activation volume averaging -21.2 cu cm/mole. The activation enthalpy for all specimens is extrapolated to a zero pressure value of 64 kcal/mole, within the experimental uncertainty. At a given stoichiometry the effect of hydroxyl content on growth rate is described entirely by a linear term C(OH) in the prefactor of the equation for the growth rate. The effect of chlorine impurity can be described similarly. Also u is increased as the ideal stoichiometry is approached from the partially reduced state.
Fratello, V. J.↗
Fused silica diaphragm module for high temperature pressure transducers
A high temperature pressure transducer and sensing apparatus to determine the deflection of the transducer diaphragm is disclosed. The pressure transducer utilizes a fused silica diaphragm (12) which is illuminated at selected locations by a coherent laser source (52) via optical fibers (38, 46). The light reflected by the diaphragm (12) forms interference fringe patterns which are focused by gradient index rod lenses (36) on the ends of optical fibers (40, 48) for transmission to a fringe counting circuit (54). By digital techniques, the fringe count is converted into a determination of diaphragm deflection.
Berthold, III, John W.↗
Impact of fused silica debris shields and enhanced mitigation techniques on large-aperture beam-sampling optics for the National Ignition Facility
Here, we show that the large-scale routine use of the fused silica debris shield (FSDS) maintains the ∼100× reduction in damage initiation rate and 70% increase in the install lifetime of a new grating debris shield (GDS) observed during pilot operations. Furthermore, we show that the install lifetimes of recycled GDS optics are nearly tripled using additional mitigation strategies such as expanding mitigation processing to include all damage sites larger than 10 μm (LT10) rather than just larger than 50 μm (LT50) and FSDS. We note that there is still a 50% difference between new and recycled optic installation lifetimes. We show that recycled optics have a 3.5× higher apparent initiation rate than new optics when exposed to nominally identical laser conditions.
FSDS↗
Effect of a Silicone Contaminant Film on the Transmittance Properties of AR-coated Fused Silica
We present the results of a laboratory test to determine the effects of bulk deposited, DC-704 silicone contaminant film on the transmittance properties of an anti-reflective (AR) coated fused silica optical substrate. Testing and optical measurements were performed in vacuum in the Boeing Combined Effects Test Facility (CETF). The test and measurement procedures are described herein. Measurement results are presented showing the change in transmittance characteristics as a function of contaminant deposit thickness and vacuum ultra-violet (vuv) exposure levels. Measurement results show an initial degradation in the transmittance of the contaminated sample. This is followed by a partial recovery in sample transmittance as the sample is exposed to additional VUV radiation. Transmittance results also show a loss of transmission in the ultraviolet portion of the spectrum and an increase in transmission in the infrared portion of the spectrum. These transmittance results are characteristic of thin-film interference effects. Thin-film analyses indicate that some of the observed transmittance results can be successfully modeled, but only if the contaminant film is assumed to be SiO2 rather than DC-704 silicone. Post-test Scanning Electron Microscope (SEM) scans of the test sample indicate the formation of contaminant islands and the presence of a thin uniform coating of contaminant deposit on the sample
Boeder, Paul A.↗
Temperature-dependent Absolute Refractive Index Measurements of Synthetic Fused Silica
Using the Cryogenic, High-Accuracy Refraction Measuring System (CHARMS) at NASA's Goddard Space Flight Center, we have measured the absolute refractive index of five specimens taken from a very large boule of Corning 7980 fused silica from temperatures ranging from 30 to 310 K at wavelengths from 0.4 to 2.6 microns with an absolute uncertainty of plus or minus 1 x 10 (exp -5). Statistical variations in derived values of the thermo-optic coefficient (dn/dT) are at the plus or minus 2 x 10 (exp -8)/K level. Graphical and tabulated data for absolute refractive index, dispersion, and thermo-optic coefficient are presented for selected wavelengths and temperatures along with estimates of uncertainty in index. Coefficients for temperature-dependent Sellmeier fits of measured refractive index are also presented to allow accurate interpolation of index to other wavelengths and temperatures. We compare our results to those from an independent investigation (which used an interferometric technique for measuring index changes as a function of temperature) whose samples were prepared from the same slugs of material from which our prisms were prepared in support of the Kepler mission. We also compare our results with sparse cryogenic index data from measurements of this material from the literature.
Leviton, Douglas B.↗
Investigation on nanoscale material removal process of BK7 and fused silica glass during chemical‐mechanical polishing
Abstract Understanding the nanoscale material removal process in chemical mechanical polishing (CMP) is of fundamental importance for the operation and further development of CMP. In this study, the nanoscale material removal processes of both fused silica glass and BK7 glass were investigated based on single‐pad‐asperity polishing experiments. The results indicate that the material removal characteristics are highly dependent on the composition and structure of glass materials. In the mechanically induced chemical bonding removal mode, only atoms locate near the outermost several layers can participate in the formation and breakage of interfacial bridge bonds. Moreover, the force on the abrasive particle must exceed a threshold value to induce significant removal of Si atoms from the glass substrate, because as the breakage of Si glass –O backbonds does not occur in low‐stress conditions. We reveal for the first time that the chemical and mechanical properties of the topmost layer, which is recognized as densification, hydrated, or redeposition layer, have not been significantly affected by the mechanical action of the abrasive particles when polishing in this kind of material removal mode. The results are expected to provide a deeper insight into the nanoscale material removal mechanism during glass CMP.
Wang, Lin↗
Change in transmittance of fused silica as a means of detecting material sputtered from components on a 5-cm ion thruster
Two endurance tests of a 5-cm mercury bombardment thruster are reported. Both tests used a translational screen-grid system with the beam vectored 10 degrees. The first test lasted 141 hours and the second test operated for 2026 hours. In each test two fused silica samples (solar cell covers), 2.0 cm by 2.1 cm, were placed in shielded holders to detect materials sputtered from the thruster. Spectral optical properties between 0.398 and 2.16 microns were measured on each sample, both before and after the endurance tests. The deposition on each sample was spectrographically analyzed to determine the type of materials sputtered from the thruster. It was found that sputtering from the neutralizer is highly dependent on its position with respect to the beam edge. The sputtering from the accelerator grid of the translational screen-grid system of the 2026 hour test was sufficient to form an opaque film on the sample located in the direction opposite to the vectored beam.
Weigand, A. J.↗
Fracture Strength of Fused Silica From Photonic Signatures Around Collision Sites
Impact sites in glass affect its fracture strength. An analytical model that predicts fracture strength from grey-field polariscope (GFP) readings (photoelastic retardations) has been developed and reported in the literature. The model is suggestive that stress fields, resulting from impact damage, destablizes sites within the glass, which lead to pathways that cause strength degradation. Using data collected from fused silica specimens fabricated from outer window panes that were designed for the space shuttle, the model was tested against four categories of inflicted damage. The damage sites were cored from the window carcasses, examined with the GFP and broken using the ASTM Standard C1499-09 to measure the fracture strength. A correlation is made between the fracture strength and the photoelastic retardation measured at the damage site in each specimen. A least-squares fit is calculated. The results are compared with the predictions from the model. A plausible single-sided NDE damage site inspection method (a version of which is planned for glass inspection in the Orion Project) that relates photoelastic retardation in glass components to its fracture strength is presented.
Yost, William T.↗