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NASA NTRS2008

Modification of Roberts' Theory for Rocket Exhaust Plumes Eroding Lunar Soil

Roberts' model of lunar soil erosion beneath a landing rocket has been updated in several ways to predict the effects of future lunar landings. The model predicts, among other things, the number of divots that would result on surrounding hardware due to the impact of high velocity particulates, the amount and depth of surface material removed, the volume of ejected soil, its velocity, and the distance the particles travel on the Moon. The results are compared against measured results from the Apollo program and predictions are made for mitigating the spray around a future lunar outpost.

Metzger, Philip T.↗
NASA NTRS2011

Fluids and their Effect on Measurements on Lunar Soil Particle size Distribution

From the late 1960s until now, lunar soil particle size distributions have typically been determined by sieving sometimes dry, and at other times with fluids such as water or Freon. Laser diffraction instruments allow rapid assessment of particle size distribution, and eventually may replace sieve measurements. However, when measuring lunar soils with laser diffraction instruments, care must be taken in choosing a carrier fluid that is compatible with lunar material. Distilled water is the fluid of choice for laser diffraction measurements of substances when there is no concern about adverse effects of water on the material being measured. When we began our analyses of lunar soils using laser diffraction, our first measurements were made with distilled water. Although the medians that we measured were comparable to earlier sieve data, the means tended to be significantly larger than expected. The effect of water vapor on lunar soil has been studied extensively. The particles interact strongly with water vapor, and subsequent adsorptions of nitrogen showed that the specific surface area increased as much as threefold after exposure to moisture. It was observed that significant porosity had been generated by this exposure to water vapor. The possibility of other physical changes in the surfaces of the grains was not studied.

Cooper, B. L.↗
NASA NTRS1993

Multiple nitrogen components in lunar soil sample 12023

Nitrogen is one of the enigmatic elements in lunar soils and breccias. The large range in (delta)N-15 values found within lunar soils was initially attributed to a secular increase in the N-15/N-14 ratio of 50 percent within the solar corona, and hence in the implanted nitrogen within the lunar regolith. However, more recent explanations have proposed a two (or many) component mixing model of solar wind nitrogen with some hypothetical non-solar components. Such components could include indigenous lunar nitrogen, nitrogen contained in interstellar grains in primitive meteorites, and magnetospheric nitrogen from the terrestrial atmosphere. To understand the makeup of multi-component mixtures it is advantageous to have carbon and noble gas data measured simultaneously, particularly in the case of lunar soils, where the solar wind is a likely fundamental contributor of nitrogen. To this end, a new nitrogen instrument was adapted to give some of the desired data in parallel. Conjoint measurements of N abundance and (delta)N-15 together with N/Ar-36 and Ar-36/Ar-38 ratios obtained during a stepped combustion of lunar soil 12023. The results are preliminary to a much more comprehensive investigation of well characterized fractions of the sample which we still have available from a previous study. Stepped combustion of a sample of 12023,7 yielded 94 ppm nitrogen with a (delta)N-15 = +22.2 percent, as well as the characteristic heavy-light-heavy pattern observed for lunar samples. The low temperature maximum was +75.1 percent at 550 C, the minimum at 800 C with (delta)N-15 = -16.7 percent and the high temperature (delta)N-15 peak is +90.6 percent at 1250 C. The major releases of nitrogen occurred between 650 C - 800 C in the form of a double peak; a third, substantial release occurred at 1150 C yielding 14.2 ppm of nitrogen coinciding with a small but recognizable drop in (delta)N-15 against a regularly increasing trend.

Brilliant, D. R.↗
NASA NTRS1988

Methods of extracting hydrogen from lunar soil

Increasing interest in establishing a lunar base has generated considerable study on the utilization of lunar resources. Because of its importance in producing water, reducing oxides, and serving as a fuel for orbital tranfer vehicles, hydrogen is of prime importance as a resource. Lowman (1985) states that hydrogen would greatly facilitate the establishment of an autonomous permanent colony, and he calls hydrogen the most valuable lunar resource. Through the centuries, hydrogen has been embedded in lunar soil by the solar wind. The hydrogen can be extracted by heating the soil to 900 C (Carr et al, 1987). In order to obtain hydrogen on the lunar surface, an extraction method must be developed which will not only be reliable but also economically feasible. Three heating methods are examined for possible use in extracting hydrogen from lunar soil.

Bustin, Roberta↗
NASA NTRS2007

Predicting the Blast of Lunar Soil Under a Rocket's Exhaust Jet

The blast of lunar soil represents a problem for the future missions planned for the moon. When the lander approached the ground during the Apollo missions, huge showers of dust particles were sent in all directions at extremely high velocities - including upwards towards the landing spacecraft. This represents a clear danger to the lander because the loss of visibility and the damage that can be produced to the vehicle itself. If there had been equipment on the ground, these showers of particles would have created a sand blasting effect over the equipment, possibly damaging optics and contaminating the equipment and depending on the size and velocity of the particles maybe even more extensive damage as the particles penetrated the outer surface of the equipment. Since the there is no air on the moon to slow down the particles, they can travel large distances at high speeds, in fact in some instances they can reach near escape velocity and go into an orbit around the moon and come all the way back to almost the same point where they were at the beginning; meaning that some of the lunar dust that came up during landing will shower back over the site. Once on the surface, the extremely fine dust had a habit of getting itself everywhere. During the Apollo missions it not only covered the astronauts' suits, but managed to work its way inside, damaging airtight joints and scratching up glass visors. The dust found its way inside the spacecraft, contaminating the floor and electronic systems inside, clogging air filters in the process. This is due to the fact that the lunar soil is extremely cohesive. The Lunar soil causes all of the same problems as sand does on Earth but unlike sand particles on Earth, which have smooth spherical shapes, the dust on the Moon is more like small particles of glass with sharper edges since there is no erosion on the lunar surface. During the Apollo missions the dust problem did not cause a big problem due to the fact of the length of duration of the missions. But as NASA plans to have long term missions to the moon the dust problem becomes an issue, due to multiple landings and the equipment that will be accumulated on the site. In order to mitigate these problems it is needed first to understand the physics of the problem in order to find the most suitable solution to protect equipment and vehicles during the next lunar missions..

Diaz, Carlos J. Sanchez↗
NASA NTRS2010

A Review of Discrete Element Method (DEM) Particle Shapes and Size Distributions for Lunar Soil

As part of ongoing efforts to develop models of lunar soil mechanics, this report reviews two topics that are important to discrete element method (DEM) modeling the behavior of soils (such as lunar soils): (1) methods of modeling particle shapes and (2) analytical representations of particle size distribution. The choice of particle shape complexity is driven primarily by opposing tradeoffs with total number of particles, computer memory, and total simulation computer processing time. The choice is also dependent on available DEM software capabilities. For example, PFC2D/PFC3D and EDEM support clustering of spheres; MIMES incorporates superquadric particle shapes; and BLOKS3D provides polyhedra shapes. Most commercial and custom DEM software supports some type of complex particle shape beyond the standard sphere. Convex polyhedra, clusters of spheres and single parametric particle shapes such as the ellipsoid, polyellipsoid, and superquadric, are all motivated by the desire to introduce asymmetry into the particle shape, as well as edges and corners, in order to better simulate actual granular particle shapes and behavior. An empirical particle size distribution (PSD) formula is shown to fit desert sand data from Bagnold. Particle size data of JSC-1a obtained from a fine particle analyzer at the NASA Kennedy Space Center is also fitted to a similar empirical PSD function.

Lane, John E.↗
NASA NTRS1999

Space Weathering in the Fine Size Fractions of Lunar Soils: Soil Maturity Effects

The effects of space weathering on the optical properties of lunar materials have been well documented. These effects include a reddened continuum slope, lowered albedo, and attenuated absorption features in reflectance spectra of lunar soils as compared to finely comminuted rocks from the same Apollo sites. However, the regolith processes that cause these effects are not well known, nor is the petrographic setting of the products of these processes fully understood. A Lunar Soil Characterization Consortium has been formed with the purpose of systematically integrating chemical and mineralogical data with the optical properties of lunar soils. Understanding space-weathering effects is critical in order to fully integrate the lunar sample collection with remotely-sensed data from recent robotic missions (e.g., Lunar Prospector, Clementine, and Galileo) We have shown that depositional processes (condensation of impact-derived vapors, sputter deposits, accreted impact material, e.g., splash glass, spherules, etc.) are a major factor in the modification of the optical surfaces of lunar regolith materials. In mature soils, it is the size and distribution of the nanophase metal in the soil grains that has the major effect on optical properties. In this report, we compare and contrast the space-weathering effects in an immature and a mature soil with similar elemental compositions. For this study, we analyzed <10 micron sieve fractions of two Apollo 17 soils, 79221 (mature, Is/FeO = 81) and 71061 (immature, Is/FeO = 14). Details of the sieving procedures and allocation scheme are given else where. The results of other detailed chemical, mineralogical, and spectroscopic analyses of these soil samples are reported elsewhere. A representative sample of each soil was embedded in low-viscosity epoxy, and thin sections (about 70nm thick) were obtained through ultra microtomy. The thin sections used for these analyses typically contained cross sections of up to 500 individual grains. The thin sections were studied using a JEOL 2010 transmission electron microscope (TEM) equipped with a thin window energy-dispersive X-ray (EDX) spectrometer. An individual thin section was selected from each soil, and for each grain in the section we determined (1) the elemental composition by EDX; (2) whether the grain was crystalline or glassy using electron diffraction and darkfield imaging; (3) the presence or absence of rims and accreted material; and (4) the distribution of nanophase Fe where present. Most of the categories are self-evident; however, we divide the agglutinate derived material into agglutinitic glass (glass with approximately the same composition as the bulk soil that contains nanophase Fe with or without vesicles) and agglutinate fragments, which are composed of crystalline grains and agglutinitic glass. Lithic fragments are defined as polymineralic grains with no glass. Pyroxene grains have been divided into high- and low-Ca groups. As expected, there are a number of differences in the petrography of the <10-microns fractions of 79221 and 71061 given the great difference in their respective maturities, but we focus here on two major distinctions: agglutinate content and the number of grains with micropatina. Slightly over 50% of the particles in 79221 consist of agglutinitic glass and agglutinate fragments, while the remainder are predominantly crystalline mineral grains. The agglutinic glass particles contain abundant nanophase Fe and vesicles. Angular particles are rare, with most showing smooth, rounded exteriors, Of the mineral grains analyzed thus far, over 90% of the grains have amorphous rims that contain nanophase Fe (these rims are believed to have formed by vapor deposition and irradiation effects). The nanophase Fe in these rims probably accounts for a significant fraction of the increase in Is/FeO measured in these size fractions. In addition to the rims, the majority of particles also show abundant accreted material in the form of glass splashes and spherules that also contain nanophase Fe. In stark contrast, the surfaces of the mineral grains in the 71061 sample are relatively prisitine, as only about 14% of the mineral grains in the sample exhibited amorphous rims. Furthermore, the mineral particles are more angular and show greater surface roughness than in the mature sample. Accreted material on particle surfaces is rare. Agglutinitic material is a major component of the 71061 sample; however, nanophase Fe and vesicles are not as well developed as in the 79221 sample. It is now recognized that nanophase Fe is probably the main agent in modifying the optical properties of lunar soil grains. The most important result of this study is the observation that in the fine size fractions of mature soils, nearly every grain has nanophase Fe within 100 run of the particle surface. (Additional Information contained in original)

Keller, L. P.↗
NASA NTRS2011

Using Microwaves to Heat Lunar Soil

This slide presentation reviews the use of microwaves to heat lunar soil in order to obtain water. There appears to be large amounts of water in the lunar poles, in Martian areas in lower latitudes and some of the Moons of Jupiter. The presence of water in the south lunar polar region was demonstrated by the Lunar CRater Observation and Sensing Satellite (LCROSS) mission. Microwaves can be used to extract water from lunar soil without excavation. Using microwaves on a lunar soil simulant at least 95% of the water from the regolith permafrost simulant was extracted (2 minutes). The process is modeled using COMSOL Multiphysics Finite Element analysis microwave physics module and demonstrated usingan experiment of an microwave apparatus on a rover.

Ethridge, Edwin C.↗
NASA NTRS1985

Guide to using lunar soil and simulants for experimentation

It is pointed out that lunar soil can be described as well-graded silty sands or sandy silts with an average particle size by weight in the range from 0.040 to 0.130 mm. The density of in situ bulk lunar soil is typically 1.4 to 1.9 g/cu cm. Changes in soil from moon to laboratory are considered along with some critical differences between simulants and lunar soil. Attention is given to agglutinates, iron metal distributed throughout the agglutinatic glass, solar wind hydrogen, and major lunar minerals (anorthite, pyroxene, ilmenite, olivine). The use of lunar fines as experimental samples is discussed, and the characteristics of simulants for experiments are examined, taking into account grain size distribution, particle type distribution, a highlands simulant, and a high titanium mare simulant. Simulants for testing equipment and structures are also described.

Allton, J. H.↗
NASA NTRS1969

Lunar soil coefficient of friction determined from Surveyor data and laboratory tests

A series of laboratory tests on simulated soils was conducted to evaluate some of these physical properties. Using soils similar to lunar soil composition, particle size distribution, and cohesion as determined from the Surveyor mission, the coefficient of friction and bulk density were evaluated by reproducing soils with the same force vs penetration characteristics as demonstrated at the Surveyor landing sites. The determination of soil coefficient of friction is presented in this paper; the soil density is treated separately in the previous paper’ of this report.

Choate, R.↗
NASA NTRS2011

Microwave Permittivity and Permeability Measurement on Lunar Soils

There has been interest in finding ways to process the lunar regolith since the early analyses of lunar samples returned from the Apollo moon missions. This fact has led to proposals for using microwaves to perform in-situ processing of the lunar soil to support future colonization of the moon. More recently, there has been speculation that the excellent microwave absorption of lunar soil came from the nanophase iron content in the regolith. The motivation for the present study was to begin obtaining a more fundamental understanding of the dielectric and magnetic properties of the regolith at microwave frequencies. A major objective of this study was to obtain information that would help answer the question about whether nanophase iron plays a major role in heating lunar soils. These new measurements over a wide frequency range can also determine the magnitude of the dielectric and magnetic absorption and if there are any resonant features that could be used to enhance processing of the regolith in the future. In addition, these microwave measurements would be useful in confirming that new simulants being developed, particularly those containing nanophase iron, would have the correct composition to simulate the lunar regolith. The results of this study suggest that nanophase iron does not play a major role in heating lunar regolith.

Barmatz, Martin↗
NASA NTRS1981

Electrophoretic separation of lunar soils in a space manufacturing facility

The feasibility of electrophoretic separation of lunar soil into its mineral constituents is discussed in this paper. The process and its applicability to lunar soil separation are considered in light of the special requirements of a space manufacturing effort. Data generated in studies at NASA-Marshall Space Flight Center, which assess the efficiency of electrophoretic separation of lunar soil, are discussed and evaluated.

Dunning, J. D.↗
NASA NTRS1986

Studies of light noble gases in mineral grains from lunar soils: A status report

Among the lunar soil constituents, monomineralic grains deserve special attention. Noble gases of carefully prepared mineral separates from lunar bulk soils were studied. The major results and conclusions of these investigations are summarized, in the context of both the regolith evolution and the history of the solar corpuscular radiation. With regard to the most abundant noble gas component in the regolith samples (the solar gases) the mineral grains have mainly two properties giving these particles among all soil constituents the best characteristics as sensors for solar gases, despite the fact, that the noble gas concentrations in a mineral separate are 10 to 60 times lower that those in a bulk sample of the same grain size. The first of these properties is the mineral dependent retentivity of the light gases He and Ne, the second property concerns the relatively short time during which a mineral grain acquires it solar gases. These two points are briefly discussed.

Wieler, R.↗
NASA NTRS1994

Remote determination of exposure degree and iron concentration of lunar soils using VIS-NIR spectroscopic methods

On the Moon, space weathering processes such as micrometeorite bombardment alter the optical properties of lunar soils. As a consequence, lunar soil optical properties are a function not only of composition, but of degree of exposure on the lunar surface as well. In order to accurately assess the compositional properties of the lunar surface using remotely acquired visible and near-infrared spectroscopic data, it is thus necessary either (1) to compare optical properties only of soils characterized by similar degrees of exposure or (2) to otherwise normalize or remove the optical effects due to exposure. Laboratory spectroscopic data for lunar soils are used to develop and test remote spectrocopic methods for determining degree of exposure and for distinguishing between the optical effects due to exposure and those due to composition. A method employing a ratio between reflectances within and outside of the 1 micrometer Fe(2+) crystal field absorption band was developed for remotely identifying highland soils that have reached a steady-state maturity. The relative optical properties of these soils are a function solely of composition and as such can be directly compared. Spectroscopic techniques for accurate quantitative determination of iron content for lunar highland soils are investigated as well. It is shown that approximations of the 1 micrometer Fe(2+) absorption band depth using few to several channel multispectral data or spectroscopic data of inadequate spectral range cannot be used with confidence for compositional analysis. However, band depth measurements derived from continuum-removed high spectral resolution data can be used to calculate the weight percent FeO and relative proportion of iron-bearing silicates in mature lunar highland and mare/highland mixture soils. A preliminary effort to calibrate telescopic band depth to laboratory soil measurements is described.

Fischer, Erich M.↗
NASA NTRS1998

Surface-Correlated Nanophase Iron Metal in Lunar Soils: Petrography and Space Weathering Effects

Space weathering is a term used to include all of the processes that act on material exposed at the surface of a planetary or small body. In the case of the Moon, it includes a variety of processes that formed the lunar regolith, caused the maturation of lunar soils, and formed patina on rock surfaces. The processes include micrometeorite impact and reworking, implantation of solar wind and flare particles, radiation damage and chemical effects from solar particles and cosmic rays, interactions with the lunar atmosphere, and sputtering erosion and deposition. Space weathering effects collectively result in a reddened continuum slope, lowered albedo, and attenuated absorption features in reflectance spectra of lunar soils as compared to finely comminuted rocks from the same Apollo sites. Understanding these effects is critical in order to fully integrate the lunar sample collection with remotely sensed data from recent robotic missions (e.g., Lunar Prospector, Clementine, Galileo). Our objective is to determine the origin of space weathering effects in lunar soils through combined electron microscopy and microspectrophotometry techniques applied to individual soil particles from <20 pm size factions (dry-sieved) of mature lunar soils. It has been demonstrated that it is the finest size fraction (<25 pm) of lunar soils that dominates the optical properties of the bulk soils.

Keller, Lindsay P.↗
NASA NTRS2005

Extracting Quantitative Data from Lunar Soil Spectra

Using the modified Gaussian model (MGM) developed by Sunshine et al. [1] we compared the spectral properties of the Lunar Soil Characterization Consortium (LSCC) suite of lunar soils [2,3] with their petrologic and chemical compositions to obtain quantitative data. Our initial work on Apollo 17 soils [4] suggested that useful compositional data could be elicited from high quality soil spectra. We are now able to expand upon those results with the full suite of LSCC soils that allows us to explore a much wider range of compositions and maturity states. The model is shown to be sensitive to pyroxene abundance and can evaluate the relative portion of high-Ca and low-Ca pyroxenes in the soils. In addition, the dataset has provided unexpected insights into the nature and causes of absorption bands in lunar soils. For example, it was found that two distinct absorption bands are required in the 1.2 m region of the spectrum. Neither of these bands can be attributed to plagioclase or agglutinates, but both appear to be largely due to pyroxene.

Noble, S. K.↗