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NASA NTRS1989

Small Displacement, Long Life On-Orbit Compressor Design and Fabrication

The focus is the generation of technology and fabrication of prototype hardware applicable to seven Space Station compressor system applications. The compressors are of the single acting reciprocating piston type and, in general, may be termed miniature in size compared with normal commercially available equipment. The initial technology development is focused on improved valve designs, and the control of pulsations and heating effects in order to increase compressor efficiency and reduce cycle temperatures, thus permitting significantly increased stage pressure ratios. The initial test compressor was successfully operated at pressure ratios of up to 50:1, and this significant extension of allowable pressure ratio will result in a reduction of the number of required stages and, hence, total hardware thereby reducing system weight and volume. These experiments have also identified the need to employ low shaft speeds, on the order of 250 to 500 rpm, to enhance heat transfer and increase life. The prototype compressor currently being designed, is to be driven by a low-speed brushless dc motor sealed in a case common to the compressor drive mechanism case. The compressor and motor case will communicate with stage suction pressure so that any minor gas leakage past the piston rings will be returned to the suction. Emphasis in this prototype design is being placed on simplicity, durability, commonality of components, and high efficiency.

Gerlach, C. R.↗

NASA NTRS2015

Sample Acquisition and Analytical Chemistry Challenges to Verifying Compliance to Aviators Breathing Oxygen (ABO) Purity Specification

NASA has been developing and testing two different types of oxygen separation systems. One type of oxygen separation system uses pressure swing technology, the other type uses a solid electrolyte electrochemical oxygen separation cell. Both development systems have been subjected to long term testing, and performance testing under a variety of environmental and operational conditions. Testing these two systems revealed that measuring the product purity of oxygen, and determining if an oxygen separation device meets Aviator's Breathing Oxygen (ABO) specifications is a subtle and sometimes difficult analytical chemistry job. Verifying product purity of cryogenically produced oxygen presents a different set of analytical chemistry challenges. This presentation will describe some of the sample acquisition and analytical chemistry challenges presented by verifying oxygen produced by an oxygen separator - and verifying oxygen produced by cryogenic separation processes. The primary contaminant that causes gas samples to fail to meet ABO requirements is water. The maximum amount of water vapor allowed is 7 ppmv. The principal challenge of verifying oxygen produced by an oxygen separator is that it is produced relatively slowly, and at comparatively low temperatures. A short term failure that occurs for just a few minutes in the course of a 1 week run could cause an entire tank to be rejected. Continuous monitoring of oxygen purity and water vapor could identify problems as soon as they occur. Long term oxygen separator tests were instrumented with an oxygen analyzer and with an hygrometer: a GE Moisture Monitor Series 35. This hygrometer uses an aluminum oxide sensor. The user's manual does not report this, but long term exposure to pure oxygen causes the aluminum oxide sensor head to bias dry. Oxygen product that exceeded the 7 ppm specification was improperly accepted, because the sensor had biased. The bias is permanent - exposure to air does not cause the sensor to return to its original response - but the bias can be accounted for by recalibrating the sensor. After this issue was found, continuous measurements of water vapor in the oxygen product were made using an FTIR. The FTIR cell is relatively large, so response time is slow - but moisture measurements were repeatable and accurate. Verifying ABO compliance for oxygen produced by commercial cryogenic processes has a different set of sample acquisition and analytical chemistry challenges. Customers want analytical chemists to conserve as much as possible. Hygrometers are not exposed to hours of continuous flow of oxygen, so they don't bias, but small amounts of contamination in valves can cause a "fail". K bottles are periodically cleaned and recertified - after cleaning residual moisture can cause a "fail". Operators let bottle pressure drop to room pressure, introduce outside air into the bottle, and the subsequent fill will "fail". Outside storage of K‐bottles has allowed enough in‐leakage, so contents will "fail".

Graf, John↗

NASA NTRS2010

Nearly Seamless Vacuum-Insulated Boxes

A design concept, and a fabrication process that would implement the design concept, have been proposed for nearly seamless vacuum-insulated boxes that could be the main structural components of a variety of controlled-temperature containers, including common household refrigerators and insulating containers for shipping foods. In a typical case, a vacuum-insulated box would be shaped like a rectangular parallelepiped conventional refrigerator box having five fully closed sides and a hinged door on the sixth side. Although it is possible to construct the five-closed-side portion of the box as an assembly of five unitary vacuum-insulated panels, it is not desirable to do so because the relatively high thermal conductances of the seams between the panels would contribute significant amounts of heat leakage, relative to the leakage through the panels themselves. In contrast, the proposal would make it possible to reduce heat leakage by constructing the five-closed-side portion of the box plus the stationary portion (if any) of the sixth side as a single, seamless unit; the only remaining seam would be the edge seal around the door. The basic cross-sectional configuration of each side of a vacuum-insulated box according to the proposal would be that of a conventional vacuum-insulated panel: a low-density, porous core material filling a partially evacuated space between face sheets. However, neither the face sheets nor the core would be conventional. The face sheets would be opposite sides of a vacuum bag. The core material would be a flexible polymer-modified silica aerogel of the type described in Silica/Polymer and Silica/Polymer/Fiber Composite Aero - gels (MSC-23736) in this issue of NASA Tech Briefs. As noted in that article, the stiffness of this core material against compression is greater than that of prior aerogels. This is an important advantage because it translates to greater retention of thickness and, hence, of insulation performance when pressure is applied across the thickness, in particular, when the space between the face sheets is evacuated, causing the core material to be squeezed between the face sheets by atmospheric pressure. Fabrication of a typical vacuum-insulated box according to the proposal would begin with fabrication of a cross-shaped polymer-modified aerogel blanket. The dimensions of the cross would be chosen so that (1) the central rectangular portion of the cross would form the core for the back of the box and (2) the arms of the cross could be folded 90 from the back plane to form the cores of the adjacent four sides of the box. Optionally, the blanket could include tabs for joining the folded sides of the blanket along mating edges and tabs that could serve as hinges for the door. Vacuum bags in the form of similar five-sided boxes would be made of a suitable polymeric film, one bag to fit the outer core surface, the other to fit the inner core surface. By use of commercially available film-sealing equipment, these box-shaped bags would be seamed together to form a single vacuum bag encasing the box-shaped core. Also, a one-way valve would be sealed to the bag. Through this valve, the interior of the bag would be evacuated to a pressure between 1 and 10 torr (approximately between 0.13 and 1.3 kPa). The polymer-modified aerogel core material is known to perform well as a thermal insulator in such a partial vacuum.

Stepanian, Christopher J.↗

NASA NTRS2009

Pressure-Energized Seal Rings to Better Withstand Flows

Pressure-energized seal rings intended to withstand flows better than do conventional pressure-energized seal rings have been conceived. The concept applies, more specifically, to seal rings used on some valve stems, pistons, and the like. A conventional pressure-energized seal ring generally has a U-shaped cross section and consists of an elastomer or other suitable polymer with an embedded metal energizing spring (see Figure 1). The working fluid from the high-pressure side that one seeks to seal is allowed into the U-shaped cavity, so that the pressure pushes the sides of the seal ring tighter against the gland and body sealing surfaces, thereby increasing the degree of sealing. Unfortunately, when the seal ring is exposed to flow of the working fluid, under some conditions, the flow grabs the lip of the U-shaped cross section and ejects or deforms the seal ring so that, thereafter, a proper seal is not obtained. Figure 2 depicts one of several alternative seal rings according to the present concept. One element of the concept is to modify the U-shaped cross section from that of the corresponding conventional seal ring to eliminate the exposed lip and prevent entry of the working fluid into the U-shaped cavity. Unlike in the conventional seal, pressurized fluid would not push the seal ring directly against the both gland and body sealing surfaces. Instead, the pressure would directly push the seal ring against a gland sealing surface only. In so doing, the pressure would squash the seal ring into a smaller volume bounded by the gland and body sealing surfaces, and would thereby indirectly press the seal ring more tightly against the body sealing surface. To enhance the desired squashing deformation, a spring having an approximately parallelogram cross section would be embedded in the modified U-shaped cavity. As the pressure pushed two corners of the approximate parallelogram closer together along the axis of the seal ring, the other two corners of the approximate parallelogram would be pushed farther apart along a radius of the ring, thereby causing the polymeric ring material to push radially harder against the body sealing surface. From the radially innermost corner of the approximate parallelogram, the spring material would extend radially, then axially into recesses in the seal gland. These extensions would help to restrain the seal ring against ejection. A seat retainer would hold the sealing ring in the gland and form a mechanical compression seal to prevent or at least reduce leakage of pressurized fluid into the cavity behind the seal. However, because there would likely be a little leakage, the cavity behind the seal should be vented to the low pressure side to prevent buildup of pressure in the cavity over time; otherwise, the built-up pressure could cause ejection of the seal ring when the pressure on the high-pressure side was reduced. Polymeric seal-ring materials may not be able to withstand working conditions in applications that involve abrasive and/or hot working fluids. For such applications, all-metal seal rings may be preferred. The bottom part of Figure 2 shows one example of an alternative gland configuration with an all-metal seal ring.

Farner, Bruce↗