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All sourcesNASA NTRSDOE OSTI
NASA NTRS1999

Dynamics of the Molten Contact Line

The purpose of this program is to develop a basic understanding of how a molten material front spreads over a solid that is below its melting point, arrests, and freezes. Our hope is that the work will contribute toward a scientific knowledge base for certain new applications involving molten droplet deposition, including the "printing" of arbitrary three-dimensional objects by precise deposition of individual molten microdrops that solidify after impact. Little information is available at this time on the capillarity-driven motion and arrest of molten contact line regions. Schiaffino and Sonin investigated the arrest of the contact line of a molten microcrystalline wax spreading over a subcooled solid "target" of the same material. They found that contact line arrest takes place at an apparent liquid contact angle that depends primarily on the Stefan number S=c(T(sub f) -T(sub t)/L based on the temperature difference between the fusion point and the target temperature, and proposed that contact line arrest occurs when the liquid's dynamic contact angle approaches the angle of attack of the solidification front just behind the contact line. They also showed, however, that the conventional continuum equations and boundary conditions have no meaningful solution for this angle. The solidification front angle is determined by the heat flux just behind the contact line, and the heat flux is singular at that point. By comparing experiments with numerical computations, Schiaffino and Sonin estimated that the conventional solidification model must break down within a distance of order 0.1 - 1 microns of the contact line. The physical mechanism for this breakdown is as yet undetermined, and no first-principles theory exists for the contact angle at arrest. Schiaffino and Sonin also presented a framework for understanding how to moderate Weber number molten droplet deposition in terms of similarity laws and experimentation. The study is based on experiments with three molten materials- molten wax on solid wax, water on ice, and mercury on frozen mercury- which between them span a considerable range of the deposition/solidification similarity parameters. Correlations are obtained for the spreading velocity, spreading time scales, the spreading factor (i.e. ratio of deposited drop's final footprint radius and the drop's initial radius), post-spreading liquid oscillation amplitudes and time scales, and bulk solidification time scales. Duthaler carried out an experimental and theoretical investigation of the relationship between the liquid's apparent contact angle and the Capillary number Ca=mu U/sigma based on contact line speed, for molten materials spreading over subcooled solids. This relationship is required for modeling of melt spreading. We have adapted Voinov's methodology to the molten contact line and formulated a theoretical model for the Ca vs. contact angle relationship, based Schiaffino and Sonin#s (1997a,b) wedge-like solidification front model. With the solidification front angle taken from Schiaffino and Sonin, the model is in good agreement with the experimental results for Ca vs. contact angle. Duthaler also extended the experimental investigation of droplet deposition and contact line freezing to more materials, including solder on glass, solder on solder, water on ice, and molten microcrystalline wax on wax. The latter also included tests on inclined targets. Deposition tests have also been done with molten octacosane (C28H58) on various targets. An important objective of our program has been the development of micron-scale sensors for measuring the transient temperature at a point on the substrate surface as a molten contact line moves over it. The expectation is that this temperature history will yield a better understanding of the thermal process in the contact line region. The sensors are of the thermistor type, either 2.5 microns or 1.5 microns square, microfabricated with silicon-based technology on either pure silicon or amorphous silicon dioxide chips. Each chip has 32 sensors distributed on its surface in arrays. The time response is better than 10 ms. At the time of writing, sensor calibration is in progress. Results on thermal transients during contact line passage will be discussed at the conference. While we expect that the data will provide information on the near-contact-line heat transfer process, we also foresee possible problems. First, the spatial resolution of the sensors may be insufficient to resolve the near-contact-line region. Second, the sensors protrude about 0.5 microns above the substrate surface, and may affect the contact line motion. Third, a sensor's temperature history depends on both the heat flux distribution into it from the fusion front and the thermal properties of the substrate below it and the solidified melt between it and the fusion front. The heat flux distribution in the contact line region must therefore be unfolded from computations of the overall system's transient thermal response.

Sonin, Ain A.↗
NASA NTRS1994

Reactive Melt Infiltration of Silicon-Niobium Alloys in Microporous Carbons

Studies of the reactive melt infiltration of silicon-niobium alloys in microporous carbon preforms prepared by the pyrolysis of a polymer precursor have been carried out using modeling, Differential Thermal Analysis (DTA), and melt infiltration. Mercury porosimetry results indicate a very narrow pore size distribution with virtually all the porosity within the carbon preforms open to infiltrants. The morphology and amount of the residual phases (niobium disilicide and silicon) in the infiltrated material can be tailored according to requirements by careful control of the properties (pore size and pore volume) of the porous carbon preforms and alloy composition. The average room temperature four-point flexural strength of a reaction-formed silicon carbide material (made by the infiltration of medium pore size carbon preform with Si - 5 at. % Nb alloy) is 290 +/- 40 MPa (42 +/- 6 ksi) and the fracture toughness is 3.7 +/- 0.3 MPa square root of m. The flexural strength decreases at high temperatures due to relaxation of residual thermal stresses and the presence of free silicon in the material.

Singh, M.↗
NASA NTRS1980

Advanced methods for preparation and characterization of infrared detector materials

Mercury cadmium telluride crystals were prepared by the Bridgman method with a wide range of crystal growth rates and temperature gradients adequate to prevent constitutional supercooling under diffusion-limited, steady state, growth conditions. The longitudinal compositional gradients for different growth conditions and alloy compositions were calculated and compared with experimental data to develop a quantitative model of the crystal growth kinetics for the Hg(i-x)CdxTe alloys, and measurements were performed to ascertain the effect of growth conditions on radial compositional gradients. The pseudobinary HgTe-CdTe constitutional phase diagram was determined by precision differential thermal analysis measurements and used to calculate the segregation coefficient of Cd as a function of x and interface temperature. Computer algorithms specific to Hg(1-x)CdxTe were developed for calculations of the charge carrier concentrations, charge carrier mobilities, Hall coefficient, optical absorptance, and Fermi energy as functions of x, temperature, ionized donor and acceptor concentrations, and neutral defect concentrations.

Lehoczky, S. L.↗
NASA NTRS2012

Bright and Dark Polar Deposits on Mercury: Evidence for Surface Volatiles

Measurements of surface reflectance of permanently shadowed areas near Mercury's north pole reveal regions of anomalously dark and bright deposits at 1064-nanometer wavelength. These reflectance anomalies are concentrated on poleward-facing slopes and are spatially collocated with areas of high radar backscatter postulated to be the result of near-surface water ice. Correlation of observed reflectance with modeled temperatures indicates that the optically bright regions are consistent with surface water ice, whereas dark regions are consistent with a surface layer of complex organic material that likely overlies buried ice and provides thermal insulation. Impacts of comets or volatile-rich asteroids could have provided both dark and bright deposits.

Polar Deposits↗
NASA NTRS2012

Dark Material at the Surface of Polar Crater Deposits on Mercury

Earth-based radar measurements [1-3] have yielded images of radar-bright material at the poles of Mercury postulated to be near-surface water ice residing in cold traps on the permanently shadowed floors of polar impact craters. The Mercury Laser Altimeter (MLA) on board the MErcury Surface, Space ENvironment, GEochemistry, and Ranging (MESSENGER) spacecraft has now mapped much of the north polar region of Mercury [4] (Fig. 1). Radar-bright zones lie within polar craters or along poleward-facing scarps lying mainly in shadow. Calculations of illumination with respect to solid-body motion [5] show that at least 0.5% of the surface area north of 75deg N lies in permanent shadow, and that most such permanently shadowed regions (PSRs) coincide with radar-bright regions. MLA transmits a 1064-nm-wavelength laser pulse at 8 Hz, timing the leading and trailing edges of the return pulse. MLA can in some cases infer energy and thereby surface reflectance at the laser wavelength from the returned pulses. Surficial exposures of water ice would be optically brighter than the surroundings, but persistent surface water ice would require temperatures over all seasons to remain extremely low (<110 K). Thermal models [6,7] incorporating direct and scattered radiation, Mercury s eccentric orbit, 3:2 spin-orbit resonance, and near-zero obliquity generally do not support such conditions in all permanently shadowed craters but suggest that water ice buried near the surface (<0.5 m depth) could survive for > 1 Gy. We describe measurements of reflectivity derived from MLA pulse returns. These reflectivity data show that surface materials in the shadowed regions are darker than their surroundings, enough to strongly attenuate or extinguish laser returns. Such measurements appear to rule out widespread surface exposures of water ice. We consider explanations for the apparent low reflectivity of these regions involving other types of volatile deposit.

Neumann, Gregory A.↗
NASA NTRS1993

Largest impact features on Venus: Non-preserved or non-recognizable?

Conventional explanation of a lack of impact craters with diameters greater than 300 km on Venus is that they formed during the intense bombardment era and had lunar-like morphology, but they are not preserved now because of rapid viscous relaxation of their topograpy and/or high endogenous reworking of surface. Other explanation invokes failure to recognize these larger craters because of their non-lunar-like morphology from the moment of formation, since larger gravity of Venus relatively to the Moon results in that largest craters on Venus may form within the mass of shock melted material while comparably sized lunar craters would be still almost 'dry'. To test this hypothesis, morphologies and rim-crest diameters of the largest peak-ring and Orientale-type basins and all larger impact features on Moon, Mercury, Mars, and Venus were compiled and compared to rim crest diameters of model craters with different melt volume/transient-cavity volume ratios. Results show that the final diameters of model craters formed at depth of melting about twice of transient cavity depth correspond to changeover from a planet-similar morphology of all the smaller basins on any terrestrial planet to a planet-specific morphology of all the larger basins on the Moon, Mercury, and Mars. On Venus, these largest impact features are not found and instead, a Venus-specific morphology of the largest concentric coronae appears in this size range. The coronae were suggested to form over sites of mantle upwelling and modified by subsequent volcanism and gravitational relaxation. The results here suggest that mantle upwelling - the first and necessary step of the corona formation models - may be induced by impact event (as a result of transient cavity collapse) and operated under cover of hot, slowly cooled impact melt in the areas of thinned crust and/or thermally active regions.

Nikolaeva, Olga V.↗
NASA NTRS2022

New Constraints on the Volatile Deposit in Mercury’s North Polar Crater, Prokofiev

We present new high-resolution topographic, illumination, and thermal models of Mercury’s 112 km-diameter north polar crater, Prokofiev. The new models confirm previous results that water ice is stable at the surface within the permanently shadowed region (PSR) of Prokofiev for geologic timescales. The largest radar-bright region in Prokofiev is confirmed to extend up to several kilometers past the boundary of its PSR making it unique on Mercury for hosting a significant radar-bright area outside a PSR. The near-infrared normal albedo distribution of Prokofiev’s PSR suggests the presence of a darkening agent rather than pure surface ice. Linear mixture models predict at least roughly half of the surface area to be covered with this dark material. Using improved altimetry in this crater, we place an upper limit of 26 m on its ice deposit thickness. The 1 km-baseline topographic slope and roughness of the radar-bright deposit are lower than the non-radar-bright floor although the difference is not statistically significant when compared to the non-radar-bright floor’s natural topographic variations. These results place new constraints on the nature of Prokofiev’s volatile deposit that will inform future missions, such as BepiColombo.

Michael K Barker↗
DOE OSTI2021

Incorporating bubble growth volume feedback to improve simulation of the response of a structure containing liquid and gas to sudden energy input

The SNS target module is a stainless-steel structure that contains and directs mercury. The mercury is struck with short, intense proton pulses to create neutrons. The pulses deposit energy and cause loads on the target structure and mercury cavitation. Helium bubbles are introduced into the mercury to reduce loads and cavitation. This gas complicates the prediction of the target module’s physical response. The current method used to simulate the structural response to the proton pulse incorporates a simple but effective approach to approximate mercury cavitation effects. This method cannot account for the changes from injected non-condensable gas. The ability to model the target vessel response is a prerequisite for estimating its life. Known approaches for simulating a bubbly fluid mixture’s response are computationally expensive and impractical for detailed engineering models. A constitutive model is proposed for target mercury with injected gas bubbles, with the intent of providing more accurate mercury–vessel response behavior without the computing costs required to track individual bubbles. The model’s assumptions and a computational model embodiment are described. The bubbly mercury computational model is subjected to test problems to assess its potential utility. Here, the model was able to better predict the effect of gas on wave propagation.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
NASA NTRS1992

Subsurface emissions from Mercury - VLA radio observations at 2 and 6 centimeters

Radio observations of Mercury made with the VLA; once in 1986, and on two dates in February of 1988 are presented. These observations are the first to spatially map both hot regions associated with the theoretical hot poles. These 'hot poles' are separated by 180 deg and are a result of the unusual diurnal heating from Mercury's 3/2 spin-orbit resonance and eccentric orbit. The highest resolution data maps areas of the planet as small as 330 km. Maps of total intensity, brightness temperature, polarized intensity, fractional polarization, depolarization, and spectral index are included. It is found that the subsurface thermal emissions from Mercury are characteristic of blackbody reradiation from the solar insolation over a diurnal cycle. These observations to produce full-disk thermophysical models are used. The one-dimensional, time-dependent heat-diffusion equation for all observed disk elements at each epoch in order to constrain thermophsyical parameters and properties of the subsurface material are solved. Using typical lunar values for several of the parameters, it is possible to reproduce the temperature morphology and most of the observed temperature values. It is found that the best-fit models require a substantial contribution of the heat transport in the subsurface to be radiative in nature. The primary difficulty in the models is in predicting the observed temperature differences as a function of frequency.

Ledlow, Michael J.↗
NASA NTRS1979

Photopolarimetry of scattering surfaces and their interpretation by computer model

Wolff's computer model of a rough planetary surface was simplified and revised. Close adherence to the actual geometry of a pitted surface and the inclusion of a function for diffuse light resulted in a quantitative model comparable to observations by planetary satellites and asteroids. A function is also derived to describe diffuse light emitted from a particulate surface. The function is in terms of the indices of refraction of the surface material, particle size, and viewing angles. Computer-generated plots describe the observable and theoretical light components for the Moon, Mercury, Mars and a spectrum of asteroids. Other plots describe the effects of changing surface material properties. Mathematical results are generated to relate the parameters of the negative polarization branch to the properties of surface pitting. An explanation is offered for the polarization of the rings of Saturn, and the average diameter of ring objects is found to be 30 to 40 centimeters.

Wolff, M.↗
NASA NTRS2011

MESSENGER Searches for Less Abundant or Weakly Emitting Species in Mercury's Exosphere

Mercury's exosphere is composed of material that originates at the planet's surface, whether that material is native or delivered by the solar wind and micrometeoroids. Many exospheric species have been detected by remote sensing, including H and He by Mariner 10, Na, K, and Ca by ground-based observations, and H, Na, Ca, Mg, and Ca+ by the MErcury Surface, Space ENvironment, GEochemistry, and Ranging (MESSENGER) spacecraft. Other exospheric species, including Fe, AI, Si, 0, S, Mn, CI, Ti, OH, and their ions, are expected to be present on the basis of MESSENGER surface measurements and models of Mercury's surface chemistry. Here we report on searches for these species made with the Ultraviolet and Visible Spectrometer (UVVS) channel of the Mercury Atmospheric and Surface Composition Spectrometer (MASCS). No obvious signatures of the listed species have yet been observed in Mercury's exosphere by the UVVS as of this writing. It is possible that detections are elusive because the optimum regions of the exosphere have not been sampled. The Sun-avoidance constraints on MESSENGER place tight limits on instrument boresight directions, and some regions are probed infrequently. If there are strong spatial gradients in the distribution of weakly emitting species, a high-resolution sampling of specific regions may be required to detect them. Summing spectra over time will also aid in the ability to detect weaker emission. Observations to date nonetheless permit strong upper limits to be placed on the abundances of many undetected species, in some cases as functions of time and space. As those limits are lowered with time, the absence of detections can provide insight into surface composition and the potential source mechanisms of exospheric material.

Vervack, Ronald J., Jr.↗
NASA NTRS2022

Solar Wind Ion Sputtering of Sodium from Silicates Using Molecular Dynamics Calculations of Surface Binding Energies

For nearly 40 yr, studies of exosphere formation on airless bodies have been hindered by uncertainties in our understanding of the underlying ion collisional sputtering by the solar wind (SW). These ion impacts on airless bodies play an important role in altering their surface properties and surrounding environment. Much of the collisional sputtering data needed for exosphere studies come from binary collision approximation (BCA) sputtering models. These depend on the surface binding energy (SBE) for the atoms sputtered from the impacted material. However, the SBE is not reliably known for many materials important for planetary science, such as plagioclase feldspars and sodium pyroxenes. BCA models typically approximate the SBE using the cohesive energy for a monoelemental solid. We use molecular dynamics (MD) to provide the first accurate SBE data we are aware of for Na sputtered from the above silicate minerals, which are expected to be important for exospheric formation at Mercury and the Moon. The MD SBE values are ∼8 times larger than the Na monoelemental cohesive energy. This has a significant effect on the predicted SW ion sputtering yield and energy distribution of Na and the formation of the corresponding Na exosphere. We also find that the SBE is correlated with the coordination number of the Na atoms within the substrate and with the cohesive energy of the Na-bearing silicate. Our MD SBE results will enable more accurate BCA predictions for the SW ion sputtering contribution to the Na exosphere of Mercury and the Moon.

Lunar surface↗
NASA NTRS1976

Sputtering phenomena of discharge chamber components in a 30-cm diameter Hg ion thruster

Sputtering and deposition rates were measured for discharge chamber components of a 30-cm diameter mercury ion thruster. It was found that sputtering rates of the screen grid and cathode baffle were strongly affected by geometry of the baffle holder. Sputtering rates of the baffle and screen grid were reduced to 80 and 125 A/hr, respectively, by combination of appropriate geometry and materials selections. Sputtering rates such as these are commensurate with thruster lifetimes of 15,000 hours or more. A semiempirical sputtering model showed good agreement with the measured values.

Mantenieks, M. A.↗
NASA NTRS1976

Sputtering phenomena of discharge chamber components in a 30-cm diameter Hg ion thruster

Sputtering and deposition rates have been measured for discharge chamber components of a 30-cm diameter mercury ion thruster. It was found that sputtering rates of the screen grid and cathode baffle were strongly affected by geometry of the baffle holder. Sputtering rates of the baffle and screen grid were reduced to 80 and 125 A/hr, respectively, by combination of appropriate geometry and materials selections. Sputtering rates such as these are commensurate with thruster lifetimes of 15,000 hours or more. A semiempirical sputtering model showed good agreement with the measured values.

Mantenieks, M. A.↗
NASA NTRS2022

The Influence of surface binding energy on sputtering in models of the sodium exosphere of Mercury

We have simulated the sodium (Na) exosphere of Mercury to show how the exosphere is affected by the assumed surface binding energy (SBE) of Na in the sputtered component. We constrained ion precipitation onto the surface using distributions for the cusp regions that are consistent with measurements by the MErcury Surface, Space ENvironment, GEochemistry, and Ranging Fast Imaging Plasma Spectrometer instrument. We have simulated sputtering with SBEs of 0.27, 2.6, 4.4, and 7.9 eV, with the lowest value commonly used in exosphere models and the highest from recent molecular dynamics calculations for the Na-bearing feldspar end-member, albite. A gradual change in the exosphere is seen as the yield decreases and the ejecta energy increases with increasing SBE. We describe the corresponding exosphere source functions for ion sputtering (IS), as well as for the previously studied processes of micrometeoroid impact vaporization and photon-stimulated desorption (PSD), along with their release energy distributions and spatial distributions. We have summed the contributions of the various source processes to explain how and when the different sources can be distinguished by observations. The modeled exosphere scale heights range from 72 km for PSD to over 1000 km for IS using a SBE of 7.9 eV. We find that the processes responsible for generating Mercury's Na exosphere are separable by measuring line-of-sight column densities tangent to the planet at various altitudes and positions around the planet. Our initial results are consistent with the Na being sputtered from a high-SBE material such as feldspar, which has been predicted to be abundant on the Mercury's surface.

Rosemary M. Killen↗
NASA NTRS2022

Tidal Insights into Rocky and Icy Bodies: An Introduction and Overview

Solid body tides provide key information on the interior structure, evolution, and origin of the planetary bodies. Our Solar system harbours a very diverse population of planetary bodies, including those composed of rock, ice, gas, or a mixture of all. While a rich arsenal of geophysical methods has been developed over several years to infer knowledge about the interior of the Earth, the inventory of tools to investigate the interiors of other Solar-system bodies remains limited. With seismic data only available for the Earth, the Moon, and Mars, geodetic measurements, including the observation of the tidal response, have become especially valuable and therefore, has played an important role in understanding the interior and history of several Solar system bodies. To use tidal response measurements as a means to obtain constraints on the interior structure of planetary bodies, appropriate understanding of the viscoelastic reaction of the materials from which the planets are formed is needed. Here, we review the fundamental aspects of the tidal modeling and the information on the present-day interior properties and evolution of several planets and moons based on studying their tidal response. We begin with an outline of the theory of viscoelasticity and tidal response. Next, we proceed by discussing the information on the tidal response and the inferred structure of Mercury, Venus, Mars and its moons, the Moon, and the largest satellites of giant planets, obtained from the analysis of the data that has been provided by space missions. We also summarise the upcoming possibilities offered by the currently planned missions.

Tides↗
NASA NTRS2022

Regional Variations of Mercury's Crustal Density and Porosity From MESSENGER Gravity Data

A new solution of Mercury's gravity field to degree and order 160, named HgM009, is retrieved through a reprocessing of MESSENGER radio science measurements. By combining our latest gravity field with topography data, localized spectral admittance analyses are carried out to investigate Mercury's crustal and lithospheric properties across the northern hemisphere. The measured spectra are compared with admittances predicted by lithospheric flexure models. The localized gravity/topography admittance analyses yield key information on the lateral variations of the bulk density of the upper crust. Elastic and crustal thicknesses are also adjusted in our study, but the local admittance spectra allow us to constrain these parameters only over a few regions. The average bulk density across the observed areas in the northern hemisphere is 2540 ±60 kg m −3 . The crustal porosity is then constrained by using an estimate of the pore-free grain density of surface materials with our measured bulk density. Our estimate of the mean porosity is 14.7 ±1.6 %, which is comparable to, but slightly higher than, the average value measured on the Moon. Larger crustal porosities are observed over heavily cratered regions, suggesting that impact bombardment is the main cause of the crustal porosity.

Mercury's crust↗
NASA NTRS2016

Comparison of Areas in Shadow from Imaging and Altimetry in the North Polar Region of Mercury and Implications for Polar Ice Deposits

Earth-based radar observations and results from the MESSENGER mission have provided strong evidence that permanently shadowed regions near Mercury's poles host deposits of water ice. MESSENGER's complete orbital image and topographic datasets enable Mercury's surface to be observed and modeled under an extensive range of illumination conditions. The shadowed regions of Mercury's north polar region from 65 deg N to 90 deg N were mapped by analyzing Mercury Dual Imaging System (MDIS) images and by modeling illumination with Mercury Laser Altimeter (MLA) topographic data. The two independent methods produced strong agreement in identifying shadowed areas. All large radar-bright deposits, those hosted within impact craters greater than or equal to 6 km in diameter, collocate with regions of shadow identified by both methods. However, only approximately 46% of the persistently shadowed areas determined from images and approximately 43% of the permanently shadowed areas derived from altimetry host radar-bright materials. Some sizable regions of shadow that do not host radar-bright deposits experience thermal conditions similar to those that do. The shadowed craters that lack radar-bright materials show a relation with longitude that is not related to the thermal environment, suggesting that the Earth-based radar observations of these locations may have been limited by viewing geometry, but it is also possible that water ice in these locations is insulated by anomalously thick lag deposits or that these shadowed regions do not host water ice.

MESSENGER↗