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At least 55 records · Page 3

Correction-free radiometry on specular spheres for containerless processing in microgravity

An analysis is presented that establishes how correction-free radiance measurements or pyrometry can be performed on targets in furnaces where there may be significant additional radiance from heated furnace walls or from reflecting surfaces close to the target. These configurations are common in microgravity and containerless processing applications where a specular target is radiantly heated in a hot-wall furnace, or inductively heated from the fields arising from nearby closely spaced electromagnetic coils. Proper design requires that the pyrometer does not view any images of the background features in the specular target so that stray radiation will not be reflected into the viewing optics of the pyrometer. To analyze the problem, conventional paraxial optics analysis is shown to be significantly in error. Instead a method of nonparaxial ray tracing, based on the derivatives of the ray paths, shows how the images must be located. This leads to analytical results that can be used to design such systems. The findings are applied to the furnace geometries that are presently being considered for flight in LEO.

Thomas, A. S. W.↗

Noncontact temperature measurement in glass and other transparent materials

The relationship between the optical properties of glass and temperature measurements in it by radiation pyrometry are described. Equations for the calculation of emissivity are presented and the transmittance, surface reflection and absorption characteristics of glass are defined. Recommendations are given regarding the selection of pyrometer wavelength sensitivity and the use of a blackbody radiator.

Doremus, Robert H.↗

Full-spectrum multiwavelength pyrometry for nongray surfaces

A full-spectrum (encompassing radiation on both sides of the Wien displacement peak) multiwavelength pyrometer was developed. It measures the surface temperature of arbitrary nongray ceramics by curve fitting a spectrum in this spectral region to a Planck function of temperature T. This function of T is modified by the surface spectral emissivity. The emissivity function was derived experimentally from additional spectra that were obtained by using an auxiliary radiation source and from application of Kirchhoff's law. This emissivity was verified by results that were obtained independently by using electromagnetic and solid-state theories. In the presence of interfering reflected radiation this general pyrometry improves the accuracy of the measured temperature by measuring an additional spectrum that characterizes the interfering radiation source.

Ng, Daniel↗

NCTM of liquids at high temperatures using polarization techniques

Temperature measurement and control is extremely important in any materials processing application. However, conventional techniques for non-contact temperature measurement (mainly optical pyrometry) are very uncertain because of unknown or varying surface emittance. Optical properties like other properties change during processing. A dynamic, in-situ measurement of optical properties including the emittance is required. Intersonics is developing new technologies using polarized laser light scattering to determine surface emittance of freely radiating bodies concurrent with conventional optical pyrometry. These are sufficient to determine the true surface temperature of the target. Intersonics is currently developing a system called DAPP, the Division of Amplitude Polarimetric Pyrometer, that uses polarization information to measure the true thermodynamic temperature of freely radiating objects. This instrument has potential use in materials processing applications in ground and space based equipment. Results of thermophysical and thermodynamic measurements using laser reflection as a temperature measuring tool are presented. The impact of these techniques on thermophysical property measurements at high temperature is discussed.

Krishnan, Shankar↗

Multiwavelength Pyrometer Developed for Use at Elevated Temperatures in Aerospace Applications

Researchers at the NASA Glenn Research Center have developed a unique multiwavelength pyrometer for aerospace applications. It has been shown to be a useful and versatile instrument for measuring the surface temperatures of ceramic zirconia thermal barrier coatings (TBCs) and alumina, even when their emissivity is unknown. The introduction of fiber optics into the pyrometer has greatly increased the ease of using this instrument. Direct comparison of measurements obtained using the pyrometer and thin film thermocouples on a sample provided independent verification of pyrometry temperature measurement. Application of the pyrometer has also included simultaneous surface and bulk temperature measurement in a transparent material, the measurement of combustion gas temperatures in the flames of an atmospheric burner, the measurement of the temperature distribution appearing on a large surface from the recording of just a single radiation spectrum emitted from this nonuniform temperature surface, and the measurement of some optical properties for special aeronautical materials-such as nanostructured layers. The multiwavelength pyrometer temperature is obtained from a radiation spectrum recorded over a broad wavelength region by transforming it into a straight line segment(s) in part or all of the spectral region. The intercept of the line segment(s) with the vertical axis at zero wavelength gives the inverse of the temperature. In a two-color pyrometer, the two data points are also amenable to this analysis to determine the unknown temperature. Implicit in a two-color pyrometer is the assumption of wavelength-independent emissivity. Its two (and minimum) pieces of data are sufficient to determine this straight line. However, a multiwavelength pyrometer not only has improved accuracy but also confirms that the wavelength-independent emissivity assumption is valid when a multitude of data points are shown to lie on a simple straight line.

Ng, Daniel L.↗

Dynamic response for thermal control and measurement and fast radiation thermometry

A preliminary evaluation was made by ORNL of a two-color ratio pyrometer (TCRP) for temperature control in the Modular Electromagnetic Levitation (MEL) experiment. A discussion was presented by Eric Spjut at the 1987 NASA Non-Contact Temperature Measurement Workshop (NASA Conf. Publ. 2503, pp. 182-213) in which he described the non-linear characteristics of the time response of TCPs. Researchers replicated his model and results and note that the non-linear response behavior is minimized for small temperature steps at high temperatures. They then used the predicted response in a model for a proportional or integral feedback controller and predicted the control characteristics for heating and cooling a 5-mm diameter sphere of niobium at high (1500 to 2750 K) temperatures. The analysis shows that for a slow (25-ms) time response for a commercial RCRP, overshoots of several hundred kelvins will result from a 100-K decrease in the setpoint, and temperature tracking errors of 14 to 45 K will occur for control temperature ramps of 1000K/s. For a fast (greater than 0.1 ms) time response, the overshoot and ramp response errors are largely eliminated.

Shepard, R. L.↗

Temperature measurement involving nanostructured thermal barrier coating using a multiwavelength pyrometer

It has been reported that erroneous results were obtained when a conventional pyrometer was used to measure the surface temperature of turbine engine components. Temperatures discrepancies were observed in components which were identical, except that one had its measured surface covered by a nanostructured thermal barrier coating (TBC) whereas the other component's surface was not so coated. These components were placed in an identical environment, receiving identical heat fluxes. A pyrometer measured the TBC covered surface hundreds degrees lower. These coatings were about 25 (mu)m thick, consisting of hundreds of layers of finer structures. The TBC's had very low thermal conductivity, heat flux calculations indicated that the temperatures of the coated surface should exhibit much higher temperature than the uncoated surface. Because these coatings were transparent to radiation from the visible to the infrared region, the temperatures measured by the pyrometer should be the temperature of the covered surface. Turbo components' performance and service life depend critically on the temperatures that it would experience; it is therefore important to know accurately and confidently the real surface temperature. Out of these concerns, an investigation into the measurement of nanostructured material surface temperature was carried out.

Ng, Daniel↗

Beam Director For Optical Pyrometer

Optical-fiber pyrometer under development observes fields of view as much as 31 degree off axis. Prismlike end fitting bends viewing angle so pyrometer can "look" at object off axis. Angled face directs thermal radiation from object into optical-fiber cable along axis.

Wyett, Lynn M.↗

Vapor deposited emittance/catalysis coatings for superalloys in heatshield applications

Statically oxidized Inconel 617 and MA 956 superalloys were prepared with vapor deposited aluminosilicate layers and exposed to temperatures which simulated reentry conditions. The aluminosilicate layers were 1-2 microns thick. The trials consisted of exposures to 1500-2300 F heat while surface temperatures were monitored with pyrometers. Analyses were then performed of the catalytic activity, oxidation phenomena, and radiative properties after thermal cycling the specimens for 8 hr. Both alloys were found to be catalytic to the recombination processes of dissociated species in the reentry environment. The coatings reduced the catalytic activity by 40 percent for both alloys but did not change the emittance. An enhanced Cr depletion zone was detected in the Inconel samples, implying that the coating did not prevent diffusion loss of Cr. The coated MA 956, on the other hand, gained weight over the course of the trials.

Clark, R. K.↗

High resolution color band pyrometer ratioing

The sensing head of a two-color band ratioing pyrometer of a known type using a fiber optic cable to couple radiation to dual detector photodiodes is improved to have high spatial resolution by focusing the radiation received through an objective lens (i.e., by focusing the image of a target area) onto an opaque sheet spaced in front of the input end of the fiber optic cable. A two-mil hole in that sheet then passes radiation to the input end of the cable. The detector has two channels, one for each color band, with an electronic-chopper stabilized current amplifier as the input stage followed by an electronic-chopper stabilized voltage amplifier.

Bickler, Donald B.↗

Noncontact measurement of high temperature using optical fiber sensors

The primary goal of this research program was the investigation and application of noncontact temperature measurement techniques using optical techniques and optical fiber methods. In particular, a pyrometer utilizing an infrared optical light pipe and a multiwavelength filtering approach was designed, revised, and tested. This work was motivated by the need to measure the temperatures of small metallic pellets (approximately 3 mm diameter) in free fall at the Microgravity Materials Processing Drop Tube at NASA Marshall Space Flight Center. In addition, research under this program investigated the adaptation of holography technology to optical fiber sensors, and also examined the use of rare-earth dopants in optical fibers for use in measuring temperature. The pyrometer development effort involved both theoretical analysis and experimental tests. For the analysis, a mathematical model based on radiative transfer principles was derived. Key parameter values representative of the drop tube system, such as particle size, tube diameter and length, and particle temperature, were used to determine an estimate of the radiant flux that will be incident on the face of an optical fiber or light pipe used to collect radiation from the incandescent falling particle. An extension of this work examined the advantage of inclining or tilting the collecting fiber to increase the time that the falling particle remains in the fiber field-of-view. Those results indicate that increases in total power collected of about 15 percent may be realized by tilting the fiber. In order to determine the suitability of alternative light pipes and optical fibers, and experimental set-up for measuring the transmittance and insertion loss of infrared fibers considered for use in the pyrometer was assembled. A zirconium fluoride optical fiber and several bundles of hollow core fiber of varying diameters were tested. A prototype two-color pyrometer was assembled and tested at Virginia Tech, and then tested on the Drop Tube at Marshall Space Flight Center. Radiation from 5 mm diameter niobium drops falling in the Drop Tube was successfully detected, and recorded for later analysis. Subsequent analysis indicated that the imaging of light output from the light pipe onto the detector active areas was not identical for both detectors.

Claus, R. O.↗

Common but unappreciated sources of error in one, two, and multiple-color pyrometry

The most common sources of error in optical pyrometry are examined. They can be classified as either noise and uncertainty errors, stray radiation errors, or speed-of-response errors. Through judicious choice of detectors and optical wavelengths the effect of noise errors can be minimized, but one should strive to determine as many of the system properties as possible. Careful consideration of the optical-collection system can minimize stray radiation errors. Careful consideration must also be given to the slowest elements in a pyrometer when measuring rapid phenomena.

Spjut, R. Erik↗

Internal Heterogeneous Processes in Aluminum Combustion

This paper discusses the aluminum particle combustion mechanism which has been expanded by inclusion of gas dissolution processes and ensuing internal phase transformations. This mechanism is proposed based on recent normal and microgravity experiments with particles formed and ignited in a pulsed micro-arc. Recent experimental findings on the three stages observed in Al particle combustion in air and shows the burning particle radiation, trajectory (streak), smoke cloud shapes, and quenched particle interiors are summarized. During stage I, the radiation trace is smooth and the particle flame is spherically symmetric. The temperature measured using a three-color pyrometer is close to 3000 K. Because it exceeds the aluminum boiling point (2730 K), this temperature most likely characterizes the vapor phase flame zone rather than the aluminum surface. The dissolved oxygen content within particles quenched during stage I was below the detection sensitivity (about 1 atomic %) for Wavelength Dispersive Spectroscopy (WDS). After an increase in the radiation intensity (and simultaneous decrease in the measured color temperature from about 3000 to 2800 K) indicative of the transition to stage II combustion, the internal compositions of the quenched particles change. Both oxygen-rich (approx. 10 atomic %) and oxygen-lean (< 1 %) regions are identified within the particles using back-scattered electron imaging and WDS. During stage II, oscillations are observed in particle radiation and the flame and smoke cloud are distorted from their original spherically-symmetric shape. In stage III, particle radiation continues to exhibit oscillations, but its radiation intensity drops and remains at a nearly constant level. The measured temperature decreases to about 2300 K. Also, larger changes in particle velocities are observed, and oxide caps are found on quenched particle surfaces. While these results showed the correlation between the aluminum particle combustion behavior and the evolution of its internal composition, the change from the spherically symmetric to asymmetric flame shape occurring upon the transition from stage I to stage II combustion could not be understood based only on the fact that dissolved oxygen is detected in the particles. The connection between the two phenomena appeared even less significant because in earlier aluminum combustion studies carried in O2/Ar mixtures, flame asymmetry was not observed as opposed to experiments in air or O2/CO mixtures. It has been proposed that the presence of other gases, i.e., hydrogen, or nitrogen causes the change in the combustion regime.

Dreizin, E. L.↗

Radiation thermometry at NIST: An update of services and research activities

An overview of activities at the National Institute of Standards and Terminology (NIST) in radiation thermometry and related temperature scale research is presented. An expansion of calibration services for pyrometers will be described as well as efforts to develop calibration services for blackbody simulators. Research relevant to the realization of the new international temperature scale (ITS 90) will be discussed.

Hillard, G. Barry↗

Non-contact heat flux measurement using a transparent sensor

A working non-contact heat flux sensor was demonstrated using a transparent material (sapphire) and a multiwavelength pyrometer. The pyrometer is used to measure the temperatures of the two surfaces of the sensor from the spectrum of radiation originating from them. The heat conducted through the material is determined from the temperature difference of the two surfaces and the thermal conductivity of the material. The measured heat flux is equal to the incident heat flux within experimental error indicating that no calibration would be necessary. A steady state heat flux of 100 kW/sq m was easily achieved.

Ng, Daniel↗