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At least 55 records · Page 3

Development of lightweight reinforced plastic laminates for spacecraft interior applications

Lightweight, Kevlar - reinforced laminating systems that are non-burning, generate little smoke in the space shuttle environment, and are physically equivalent to the fiberglass/polyimide system used in the Apollo program for non-structural cabin panels, racks, etc. Resin systems representing five generic classes were screened as matrices for Kevlar 49 reinforced laminates. Of the systems evaluated, the polyimides were the most promising with the phenolics a close second. Skybond 703 was selected as the most promising resin candidate. With the exception of compression strength, all program goals of physical and mechanical properties were exceeded. Several prototype space shuttle mobility and translation handrail segments were manufactured using Kevlar/epoxy and Kevlar-graphite/epoxy. This application shows significant weight savings over the baseline aluminum configuration used previous. The hybrid Kevlar-graphite/epoxy is more suitable from a processing standpoint.

Hertz, J.↗

Fire test method for graphite fiber reinforced plastics

A potential problem in the use of graphite fiber reinforced resin matrix composites is the dispersal of graphite fibers during accidential fires. Airborne, electrically conductive fibers originating from the burning composites could enter and cause shorting in electrical equipment located in surrounding areas. A test method for assessing the burning characteristics of graphite fiber reinforced composites and the effectiveness of the composites in retaining the graphite fibers has been developed. The method utilizes a modified rate of heat release apparatus. The equipment and the testing procedure are described. The application of the test method to the assessment of composite materials is illustrated for two resin matrix/graphite composite systems.

Bowles, K. J.↗

Fire test method for graphite fiber reinforced plastics

A potential problem in the use of graphite fiber reinforced resin matrix composites is the dispersal of graphite fibers during accidental fires. Airborne, electrically conductive fibers originating from the burning composites could enter and cause shorting in electrical equipment located in surrounding areas. A test method for assessing the burning characteristics of graphite fiber reinforced composites and the effectiveness of the composites in retaining the graphite fibers has been developed. The method utilizes a modified Ohio State University Rate of Heat Release apparatus. The equipment and the testing procedure are described. The application of the test method to the assessment of composite materials is illustrated for two resin matrix/graphite composite systems.

Bowles, K. J.↗

Carbon Fiber Reinforced Plastic with Substantially Improved Through-plane Thermal Conductivity

Thermal conductivity of carbon fiber support structures that also serve as cooling substrates is of increasing importance for high energy physics detectors. One of the shortcomings of current carbon fiber laminates is that they exhibit excellent thermal conductivity of order several hundred W/(m*K) along the fiber direction, whereas the through plane thermal conductivity perpendicular to the fibers is orders of magnitude lower, and at about 1 W/(m*K) more in the range of thermal insulators. This proposal aims to significantly improve the through plane thermal conductivity, by at least a factor five, changing CFRP from being a thermal insulator to a thermal conductor in the through plane direction. Between June 2021 and December 2022, a total of 36 carbon fiber laminate test samples and two carbon loaded epoxy test samples were manufactured and analyzed for thermal performance. Unfortunately, the promising results obtained with a similar sample manufactured in 2017 were not reproduced. We believe this to be mainly due the excessive age of the carbon fiber prepreg material used for this SBIR - the same material batch, produced in 2015, was used in 2017 and in 2021/2022, i.e. the material was seven years old when the final samples were produced - , and to a lesser degree to the difference in pressure attainable with the 2017 and 2021/2022 laminate curing setups. While disappointing, the results are not completely discouraging, since for the samples with the highest compression the through-plane thermal conductivities plotted as a function of per-ply thickness extrapolate well to the data point from the 2017 sample.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Fatigue crack growth in fiber reinforced plastics

Fatigue crack growth in fiber composites occurs by such complex modes as to frustrate efforts at developing comprehensive theories and models. Under certain loading conditions and with certain types of reinforcement, simpler modes of fatigue crack growth are observed. These modes are more amenable to modeling efforts, and the fatigue crack growth rate can be predicted in some cases. Thus, a formula for prediction of ligamented mode fatigue crack growth rate is available.

Mandell, J. F.↗

Designing with figer-reinforced plastics (planar random composites)

The use of composite mechanics to predict the hygrothermomechanical behavior of planar random composites (PRC) is reviewed and described. These composites are usually made from chopped fiber reinforced resins (thermoplastics or thermosets). The hygrothermomechanical behavior includes mechanical properties, physical properties, thermal properties, fracture toughness, creep and creep rupture. Properties are presented in graphical form with sample calculations to illustrate their use. Concepts such as directional reinforcement and strip hybrids are described. Typical data that can be used for preliminary design for various PRCs are included. Several resins and molding compounds used to make PRCs are described briefly. Pertinent references are cited that cover analysis and design methods, materials, data, fabrication procedures and applications.

Chamis, C. C.↗

Failure criterion of glass fabric reinforced plastic laminates

Failure criteria are derived for several modes of failure (in unaxial tensile or compressive loading, or biaxial combined tensile-compressive loading) in the case of closely woven plain fabric, coarsely-woven plain fabric, or roving glass cloth reinforcements. The shear strength in the interaction formula is replaced by an equation dealing with tensile or compressive strength in the direction making a 45 degree angle with one of the anisotropic axes, for the uniaxial failure criteria. The interaction formula is useful as the failure criterion in combined tension-compression biaxial failure for the case of closely woven plain fabric laminates, but poor agreement is obtained in the case of coarsely woven fabric laminates.

Haga, O.↗

Characterizing Char Rate and Extent in Fiber-Reinforced Plastics Using X-ray Computed Tomography

Orbital debris is a growing problem for the space industry and the world in general, and an important component of the problem is what happens when that debris reenters the Earth’s atmosphere. With more spacecraft opting for fiber-reinforced polymer (FRP) components, we need to understand the thermal destruction process of these materials during an atmospheric reentry and how much of the material can survive to impact the ground. The NASA Orbital Debris Program Office (ODPO) has developed a new charring model for FRP components to be integrated into the latest version of the Object Reentry Survival Analysis Tool (ORSAT). To validate this new model, the ODPO performed several test series using the Inductively Coupled Plasma (ICP) Torch facility at UT Austin. To measure the extent of charred material at different conditions, some of the test samples were scanned using x-ray computed tomography (CT) by the Astromaterials Curation Lab at Johnson Space Center. 3D image analysis was then used to calculate the volume and density of the char in each test sample. This paper presents the image analysis methodology, an assessment of the accuracy of the data analysis, and a comparison with calculations using the ORSAT charring model.

Benton Greene↗

Corrosion Control in Carbon Fiber Reinforced Plastic (CFRP) Composite-Aluminum Closure Panel Hem Joints

This project targeted the implementation of CFRP/Al closure panels as a drop-in replacement for all-aluminum closures used in automobile production today. The project focused on the development of corrosion fundamentals involving CFRP materials and the use of those materials in mixed-material joints. Numerous studies were completed to benchmark current materials and test mixed metal joints. Good correlation was found between outdoor exposures and laboratory cyclic corrosion testing. The insights from the corrosion testing fundamentals and benchmarking phases informed the development of low-cure adhesive and electrocoats and conductive primers for the CFRP. Adhesive and electrocoat materials were successfully developed meeting low-cure targets for bake (150C/10min). These materials were scaled-up and used to produce 5 prototype liftgates to further evaluate CFRP/Al joints in a full-scale part. The lower cure materials enabled mitigation of CTE mismatch and reduced the required bake temperature, resulting in reduced part distortion. Corrosion testing of the liftgates revealed unexpected increases in corrosion relative to the standard bake materials. While rigorous evaluation of the parts was not possible due to numerous complexities associated with prototype testing, the results provided significant insights into the material behavior of CFRP/Al joints. Key learnings from the project included a better understanding of the system complexity (interplay of substrate/primer conductivity, production of full-scale prototypes), advances in coating/adhesive design for low-cure applications involving CFRP, and advancement of corrosion test protocols for CFRP.

36 MATERIALS SCIENCE↗

Testing procedures for carbon fiber reinforced plastic components

Tests for studying the basic material are considered and quality control investigations involving preimpregnated materials (prepreg) are discussed. Attention is given to the prepreg area weight, the fiber area weight of prepregs, the resin content, volatile components, the effective thickness, resin flow, the resistance to bending strain, tensile strength, and shear strength. A description of tests conducted during the manufacturing process is also presented, taking into account X-ray methods, approaches of neutron radiography, ultrasonic procedures, resonance methods and impedance studies.

Gosse, H. J.↗

Survey of long-term durability of fiberglass reinforced plastic structures

Included are fluid containment vessels, marine structures, and aircraft components with up to 19 years of service. Correlations were obtained for the variation of static fatigue strength, cyclic fatigue strength, and residual burst strength for pressure vessels. In addition, data are presented for the effects of moisture on strength retention. Data variations were analyzed, and relationships and implications for testing are discussed. Change in strength properties for complete structures was examined for indications of the effects of environmental conditions such as moisture and outdoor exposure (ultraviolet radiation, weathering) on long term durability.

Lieblein, S.↗

Stronger Carbon Fibers for Reinforced Plastics

Process makes fibers 70 percent stronger at lower carbonization temperature. Stronger carbon fibers result from benzoic acid pretreatment and addition of acetylene to nitrogen carbonizing atmosphere. New process also makes carbon fibers of higher electrical resistance -- an important safety consideration.

Cagliostro, D. E.↗

The prediction of long term viscoelastic properties of fiber reinforced plastics

A method for the experimental and analytical accelerated characterization of long term viscoelastic properties is presented. The time-temperature-stress superposition principle (TTSSP) is shown to serve as the basis for determining long term compliance data from short term creep test results. Nonlinear viscoelastic theories are discussed to provide the framework for the mathematically modeling of such a process. A time dependent Tsai-Hill-Zhurkov failure theory is used to determine long term failure properties from short term data. Compliance and failure data are incorporated in an incremental lamination theory to make long term laminate predictions. Comparisons are made between theory and experiment.

Brinson, H. F.↗