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DOE OSTI2019

Initial Benchmarking of the Liquid Sampling-Atmospheric Pressure Glow Discharge-Orbitrap System Against Traditional Atomic Mass Spectrometry Techniques for Nuclear Applications

The integration of the liquid sampling-atmospheric pressure glow discharge (LS-APGD) ion source with Orbitrap mass spectrometers has resulted in new opportunities in the field of isotope ratio mass spectrometry. In a field that has been dominated by thermal ionization mass spectrometry (TIMS) and inductively coupled plasma mass spectrometry (ICP-MS) on quadrupole and scanning-mode sector field analyzer platforms for highly accurate and precise measurements, the LS-APGD-Orbitrap system offers a benchtop instrument capable of meeting the rigorous International Target Values for measurement uncertainty for uranium (U). In order to benchmark the LS-APGD-Orbitrap, a series of U certified reference materials with increasing {sup 235}U isotopic composition were analyzed. By using U samples ranging in enrichment from 1 to 80%, the ability of the system to measure isotope ratios over a wide range is demonstrated. This analysis represents the first time that the LS-APGD-Orbitrap system has been used to analyze highly enriched U samples, allowing for the measurement of each of the U isotopes, including {sup 234}U and {sup 236}U-related species, which had not been achieved previously. Ultimately, the LS-APGD-Orbitrap system was able to measure CRM U-800 (assayed as {sup 235}U / {sup 238}U = 4.265622) as 4.266922, with a combined uncertainty, (u{sub c}), of 0.040%. These results are compared to those obtained using traditional elemental mass spectrometers including TIMS and ICP-MS-based instruments. The effectiveness of the LS-APGD-Orbitrap MS system for measuring U isotopes shows excellent promise in nuclear forensics, safeguards, and other nuclear weapon-based applications. .

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2022

Accuracy of predictions made by machine learned models for biocrude yields obtained from hydrothermal liquefaction of organic wastes

Hydrothermal liquefaction (HTL) has potential for converting abundant wet organic wastes into renewable fuels. Because HTL consists of a complex reaction network, deterministic, physics-based prediction of its biocrude yield is prohibitively difficult. Data-driven methods provide an alternative to the physics-based approach; however, rigorous testing must be performed to ensure the accuracy of predictions made by data-driven methods. To this end, a data set was assembled consisting of 570 data points appearing in the open literature. The data set was divided into training, validation, and test sub-sets and used for evaluating different machine learning regression approaches to predict biocrude yield. Among the tested algorithms, Random Forest and eXtreme Gradient Boosting (XGBoost) predicted biocrude yields in a test set that had not been used for training with the greatest accuracy, with root mean square errors (RMSE) of 8.34 and 8.57, respectively. Further refinement of the Random Forest model reduced its RMSE to 8.07. In comparison, predictions of a series of literature models resulted in RMSE ranging from 9.16 in the most accurate case to 27.6 in the least accurate; most literature models yielded RMSE values > 10. Using biocrude yield predictions from the most accurate Random Forest model and a probabilistic economic analysis found that the model accuracy is sufficient to prioritize allocation of resources based on projected minimum fuel selling price. In our report the models and analysis represent a major advance in the ability to use readily available data to predict biocrude yields on new feedstocks that have not previously been studied.

42 ENGINEERING↗

DOE OSTI2020

Building commissioning costs and savings across three decades and 1500 North American buildings

B.V. Building commissioning (Cx) is a process for assuring efficient building operations that can be applied to new construction and existing buildings, resulting in energy and non-energy benefits. Quantifying the benefits of commissioning is challenging, but a 2009 study of 643 commercial buildings provided a solid initial data set to which we added 839 additional buildings for a significantly expanded and updated meta-analysis representing 34.7 million square meters (373 million square feet) of floor area. Since 2009 the commissioning industry has continued to grow, driven by building codes, utility programs, and rising awareness of commissioning benefits. In parallel, building controls have become more sophisticated, and analytics software has emerged to assist with commissioning. We find that delivery mechanism and market segment are key determinants of outcomes, although significant and cost-effective savings are found across the spectrum. Median primary energy savings for Cx projects in existing buildings ranged from 5 percent for those conducted under utility programs, 9 percent for monitoring-based commissioning utility programs (i.e., augmented with submetering and diagnostics), and 14 percent for Cx projects outside of utility programs. Across all project types, median savings ranged from 3 percent for the lodging market segment to 16 percent for public order and safety facilities. Outcomes did not vary significantly by building size or by market segment. Energy savings are rarely estimated for new construction commissioning. We found that the median costs of Cx were lower for the 2018 sample than for the 2009 sample—$\$$2.85 per square meter ($\$$0.26 per square foot) for existing buildings (a 33 percent reduction) and $\$$8.78 per square meter ($\$$0.82 per square foot) for new construction (a reduction of almost 50 percent). The median simple payback time for existing buildings was 1.7 years, with a 25th–75th percentile range of 0.8–3.5 years. Overall, this article summarizes these and other key findings, and discusses how the 2018 data reflects shifts in commissioning practice and outcomes.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

DOE OSTI2015

Federal policy documentation and geothermal water consumption: Policy gaps and needs

With U.S. geothermal power production expected to more than triple by 2040, and the majority of this growth expected to occur in arid and water-constrained areas, it is imperative that decision-makers understand the potential long-term limitations to and tradeoffs of geothermal development due to water availability. To this end, water consumption data, including documentation triggered by the National Environmental Policy Act (NEPA) of 1969, production and injection data, and water permit data, were collected from state and federal environmental policy sources in an effort to determine water consumption across the lifecycle of geothermal power plants. Values extracted from these sources were analyzed to estimate water usage during well drilling; to identify sourcing of water for well drilling, well stimulation, and plant operations; and to estimate operational water usage at the plant level. Nevada data were also compared on a facility-by-facility basis with other publicly available water consumption data, to create a complete picture of water usage and consumption at these facilities. This analysis represents a unique method of capturing project-level water data for geothermal projects; however, a lack of statutory and legal requirements for such data and data quality result in significant data gaps, which are also explored

Schroeder, J. N.↗

DOE OSTI2015

A Comparative Study of the Hypoxia PET Tracers [{sup 18}F]HX4, [{sup 18}F]FAZA, and [{sup 18}F]FMISO in a Preclinical Tumor Model

Purpose: Several individual clinical and preclinical studies have shown the possibility of evaluating tumor hypoxia by using noninvasive positron emission tomography (PET). The current study compared 3 hypoxia PET tracers frequently used in the clinic, [{sup 18}F]FMISO, [{sup 18}F]FAZA, and [{sup 18}F]HX4, in a preclinical tumor model. Tracer uptake was evaluated for the optimal time point for imaging, tumor-to-blood ratios (TBR), spatial reproducibility, and sensitivity to oxygen modification. Methods and Materials: PET/computed tomography (CT) images of rhabdomyosarcoma R1-bearing WAG/Rij rats were acquired at multiple time points post injection (p.i.) with one of the hypoxia tracers. TBR values were calculated, and reproducibility was investigated by voxel-to-voxel analysis, represented as correlation coefficients (R) or Dice similarity coefficient of the high-uptake volume. Tumor oxygen modifications were induced by exposure to either carbogen/nicotinamide treatment or 7% oxygen breathing. Results: TBR was stabilized and maximal at 2 hours p.i. for [{sup 18}F]FAZA (4.0 ± 0.5) and at 3 hours p.i. for [{sup 18}F]HX4 (7.2 ± 0.7), whereas [{sup 18}F]FMISO showed a constant increasing TBR (9.0 ± 0.8 at 6 hours p.i.). High spatial reproducibility was observed by voxel-to-voxel comparisons and Dice similarity coefficient calculations on the 30% highest uptake volume for both [{sup 18}F]FMISO (R = 0.86; Dice coefficient = 0.76) and [{sup 18}F]HX4 (R = 0.76; Dice coefficient = 0.70), whereas [{sup 18}F]FAZA was less reproducible (R = 0.52; Dice coefficient = 0.49). Modifying the hypoxic fraction resulted in enhanced mean standardized uptake values for both [{sup 18}F]HX4 and [{sup 18}F]FAZA upon 7% oxygen breathing. Only [{sup 18}F]FMISO uptake was found to be reversible upon exposure to nicotinamide and carbogen. Conclusions: This study indicates that each tracer has its own strengths and, depending on the question to be answered, a different tracer can be put forward.

62 RADIOLOGY AND NUCLEAR MEDICINE↗

DOE OSTI2023

BEYONDPLANCK XIV. Polarized foreground emission between 30 and 70 GHz

We constrain polarized foreground emission between 30 and 70 GHz with the Planck Low Frequency Instrument (LFI) and WMAP data within the global Bayesian BeyondPlanck framework. We combine for the first time full-resolution Planck LFI time-ordered data with low-resolution WMAP sky maps at 33, 40 and 61 GHz. Spectral parameters are fit with a likelihood defined at the native resolution of each frequency channel. This analysis represents the first implementation of true multi-resolution component separation applied to CMB observations for both amplitude and spectral energy distribution (SED) parameters. For synchrotron emission, we approximate the SED as a power-law in frequency and find that the low signal-to-noise ratio of the current data strongly limits the number of free parameters that may be robustly constrained. We partition the sky into four large disjoint regions (High Latitude; Galactic Spur; Galactic Plane; and Galactic Center), each associated with its own power-law index. We find that the High Latitude region is prior-dominated, while the Galactic Center region is contaminated by residual instrumental systematics. The two remaining regions appear to be signal-dominated, and for these we derive spectral indices of $β$ S Spur = -3.17 ± 0.06 and $β$ S Plane = -3.03 ± 0.07, in good agreement with previous results. For thermal dust emission we assume a modified blackbody model and we fit a single power-law index across the full sky. We find $β$ d = 1.64 ± 0.03, which is slightly steeper than reported from Planck HFI data, but still statistically consistent at the 2σ confidence level.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2017

Measurement of cosmic-ray reconstruction efficiencies in the MicroBooNE LArTPC using a small external cosmic-ray counter

The MicroBooNE detector is a liquid argon time projection chamber at Fermilab designed to study short-baseline neutrino oscillations and neutrino-argon interaction cross-section. Due to its location near the surface, a good understanding of cosmic muons as a source of backgrounds is of fundamental importance for the experiment. We present a method of using an external 0.5 m (L) x 0.5 m (W) muon counter stack, installed above the main detector, to determine the cosmic-ray reconstruction efficiency in MicroBooNE. Data are acquired with this external muon counter stack placed in three different positions, corresponding to cosmic rays intersecting different parts of the detector. The data reconstruction efficiency of tracks in the detector is found to be $\epsilon_{\mathrm{data}}=(97.1\pm0.1~(\mathrm{stat}) \pm 1.4~(\mathrm{sys}))\%$, in good agreement with the Monte Carlo reconstruction efficiency $\epsilon_{\mathrm{MC}} = (97.4\pm0.1)\%$. This analysis represents a small-scale demonstration of the method that can be used with future data coming from a recently installed cosmic-ray tagger system, which will be able to tag $\approx80\%$ of the cosmic rays passing through the MicroBooNE detector.

47 OTHER INSTRUMENTATION↗

DOE OSTI2019

Neutron Time-of-Flight Measurements of Charged-Particle Energy Loss in Inertial Confinement Fusion Plasmas

Neutron spectra from secondary 3 H(d,n)α reactions produced by an implosion of a deuterium-gas capsule at the National Ignition Facility have been measured with order-of-magnitude improvements in statistics and resolution over past experiments. Furthermore, these new data and their sensitivity to the energy loss of fast tritons emitted from thermal 2 H(d,p) 3 H reactions enable the first statistically significant investigation of charged-particle stopping via the emitted neutron spectrum. Radiation-hydrodynamic simulations, constrained to match a number of observables from the implosion, were used to predict the neutron spectra while employing two different energy loss models. This analysis represents the first test of stopping models under inertial confinement fusion conditions, covering plasma temperatures of k B T ≈ 1–4 keV and particle densities of n ≈ (12–2) × 10 24 cm –3 . Under these conditions, we find significant deviations of our data from a theory employing classical collisions whereas the theory including quantum diffraction agrees with our data.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2020

Involute Working Group – Validation of CFD Turbulence Models for Steady-State Safety Analysis

There are three research reactors in the world having fuel plates curved as circle-involute (a spiral generated around a circle): The Oak Ridge National Laboratory (ORNL) High Flux Isotope Reactor (HFIR) located in Tennessee, U.S.A. [ORNL, 2018]; The Laue-Langevin Institute (ILL) High Flux Reactor (RHF) located in Grenoble, France [ILL, 2018]; and, The Technical University of Munich (TUM) Research Neutron Source Heinz Maier-Leibnitz (FRM II) located in Garching, Germany [TUM, 2018]. All three reactors are currently using Highly Enriched Uranium (HEU, 235U/U ≥ 20 wt. %) as fuel and all three are actively engaged in activities to convert to Low Enriched Uranium (LEU, 235U/U < 20 wt. %) fuel. More information on these reactors can be found in Section two. For various reasons, these reactors have expressed interest in using Computational Fluid Dynamics (CFD) tools to perform their Steady-State Thermal-Hydraulic (SSTH) safety calculations. Using CFD tools for SSTH analysis represents generally a significant departure from traditional methods and requires thorough verification and validation (V&V) to be accepted by regulators. This is why Argonne National Laboratory (ANL) and the involute reactors formed an informal group to help each other in this endeavor. This so-called Involute Working Group (IWG) aims at supporting the qualification of CFD tools for SSTH safety calculations. Activities include benchmarking, code-to-code comparison, Verification and Validation (V&V) as well as technical support. More information on the IWG and the reasons why involute-plate reactors are interested in CFD can be found in Section three. The present study aims at testing three turbulence models commonly implemented in commercial software (namely K-Epsilon, K-Omega and Reynolds-Stress) and assessing their relevance for involute-plate reactor application. An experiment performed by Gambill and Bundy in 1961 was performed to measure heat transfer coefficients in conditions prototypic of the HFIR reactor [Gambill, 1961]. More details on this experiment are provided in Section four. Based on the information available, CFD models of this experiment have been created and the experimental results have been compared to the ones obtained with these CFD models. CFD models and the results of this comparison are provided in Section five.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

DOE OSTI2024

Empowering Rural Electrification in Honduras: An Integrated Assessment of PV/BESS and Productive Uses of Electricity in Gracias a Dios

Honduras faces significant challenges in its energy sector, particularly in rural areas where access to reliable and affordable electricity remains limited. The flagship rural electrification initiative for Honduras Secretary of Energy (SEN) is the Politica de Acceso Universal a la Electricidad (PAUEH - Universal Electricity Access Policy), a key solution for addressing this energy poverty is the deployment of more than 1700 distributed solar and hybrid mini-grid solutions. In late 2023 as a first step towards supporting SEN's electrification efforts, the National Renewable Energy Laboratory (NREL) developed a literature review of SEN electrification policy documents and conducted a series of technical capacity-building workshops with SEN and other energy sector stakeholders in Honduras focused on using NREL's open-source REopt tool to conduct techno-economic assessments and develop least-cost optimizations for potential solar + storage mini-grid systems. Building on some initial capacity building on mini-grid modeling, the National Renewable Energy Laboratory (NREL) worked with SEN to develop a detailed techno-economic assessment for electrifying two schools, a healthcare clinic, and a hospital in a hypothetical community within the department of Gracias a Dios. The analysis also evaluates the business case for cold storage productive use of energy (PUE) applications for the fisheries value chain and how the incorporation of these PUE loads potentially impacts both the viability of the PV+BESS solutions as well as local economic development. By assessing the potential for deployment of integrated PV/BESS systems to both support critical community services like education and healthcare, as well as potential for downstream enterprise and economic development, this analysis represents a first step that can help to inform specific strategies for development of pilot PV+BESS projects aligned with national priorities and sector level planning under PAUEH.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗

DOE OSTI2024

Fortalecimiento de la Electrificación Rural en Honduras: Una Evaluación Integrada de PV+BESS y Usos Productivos de la Electricidad en Gracias a Dios, Honduras [Empowering Rural Electrification in Honduras: An Integrated Assessment of PV/BESS and Productive Uses of Electricity in Gracias a Dios] (Spanish Translation)

14 SOLAR ENERGY↗

DOE OSTI2017

Lessons from the Onset of a Common Envelope Episode: the Remarkable M31 2015 Luminous Red Nova Outburst

This paper investigates the recent stellar-merger transient M31LRN 2015 in the Andromeda galaxy. We analyze published optical photometry and spectroscopy along with a Hubble Space Telescope detection of the color and magnitude of the pre-outburst source. The transient outburst is consistent with dynamically driven ejecta at the onset of a common envelope episode, which eventually leads to the complete merger of a binary system. The light curve appears to contain two components: first ∼10{sup −2} M{sub ⊙} of fast ejecta driven by shocks at the onset of common envelope, and later, ∼0.3 M {sub ⊙} of further ejecta as the secondary becomes more deeply engulfed within the primary. Just prior to merger, we find that the primary star is a 3–5.5 M {sub ⊙} subgiant-branch primary star with a radius of 30–40 R {sub ⊙}. Its position in the color–magnitude diagram shows that it is growing in radius, consistent with a picture where it engulfs its companion. By matching the properties of the primary star to the transient outburst, we show that the optical transient lasts less than 10 orbits of the original binary, which had a pre-merger period of ∼10 days. We consider the possible orbital dynamics leading up to the merger, and argue that if the system merged due to the Darwin tidal instability it implies a lower mass main-sequence companion of 0.1–0.6 M {sub ⊙}. This analysis represents a promising step toward a more detailed understanding of flows in common envelope episodes through direct observational constraints.

79 ASTRONOMY AND ASTROPHYSICS↗

NASA NTRS1974

An examination of injector/combustor design effects on scramjet performance

Description of a simplified one-dimensional treatment of fuel injection for supersonic combustor performance analysis. Representative mixing efficiency variations for both parallel and cross-stream injection are obtained, and approximate means for estimating the length required for complete mixing are demonstrated. Comparisons of calculated and measured data show good agreement.

Anderson, G. Y.↗

NASA NTRS1976

The longitudinal equations of motion of a tilt prop/rotor aircraft including the effects of wing and prop/rotor blade flexibility

The equations of motion for the longitudinal dynamics of a tilting prop/rotor aircraft are developed. The analysis represents an extension of the equations of motion. The effects of the longitudinal degrees of freedom of the body (pitch, heave and horizontal velocity) are included. The results of body freedom can be added to the equations of motion for the flexible wing propeller combination.

Curtiss, H. C., Jr.↗

NASA NTRS1975

Drogue parachute deployment dynamics of the space shuttle solid rocket booster

Theoretical analysis and experimental investigations are presented for two deployment concepts of the drogue parachute deployment for the space shuttle solid rocket booster. The analysis represents the motion of three coupled rigid bodies, with one of the bodies having variable mass and moment of inertia. The unfurling process of the parachute from the bag is idealized as the flow of a continuum out of a control surface. The pilot parachute or tethered nose cap is modeled as a flexible pendulum with a nonlinear spring and a moving support. Measured wind tunnel test data compare reasonably well with the theory.

Banerjee, A. K.↗

NASA NTRS1977

Photographic film and the Skylab environment

An overview is presented of an investigation which was conducted to determine the actual effects of the Skylab environment on flight films. Examples of the flight film performance data are provided. Attention is given to the Skylab film, the environmental parameters, a major events profile of the Skylab mission, and a film environmental effects analysis. Representative Skylab film environmental response data are shown in a graph.

Oldham, L. P.↗

NASA NTRS1977

Computation of nonlinear one-dimensional waves in near-sonic flows

A nonlinear analysis is developed for sound propagation in a variable area duct in which the mean flow approaches choking conditions. A quasi-one-dimensional model is used; results of the standard linear theory are compared with the nonlinear results to assess the significance of the nonlinear terms. The nonlinear analysis represents the acoustic disturbance as a sum of interacting harmonics. Numerical results show that the basic signal is unaffected by the presence of higher harmonics if the throat Mach number is not too large, but as the Mach number approaches unity more harmonics are needed to describe the acoustic propagation. The strong interactions among harmonics in the numerical results occur in a region which is generally consistent with the nonlinear inner-expansion region of Callegari and Myers.

Nayfeh, A. H.↗

NASA NTRS1980

An evaluation of a computer code based on linear acoustic theory for predicting helicopter main rotor noise

Acoustic characteristics predicted using a recently developed computer code were correlated with measured acoustic data for two helicopter rotors. The analysis, is based on a solution of the Ffowcs-Williams-Hawkings (FW-H) equation and includes terms accounting for both the thickness and loading components of the rotational noise. Computations are carried out in the time domain and assume free field conditions. Results of the correlation show that the Farrassat/Nystrom analysis, when using predicted airload data as input, yields fair but encouraging correlation for the first 6 harmonics of blade passage. It also suggests that although the analysis represents a valuable first step towards developing a truly comprehensive helicopter rotor noise prediction capability, further work remains to be done identifying and incorporating additional noise mechanisms into the code.

Davis, S. J.↗