Environmental Study of Miniature Slip Rings Quarterly Report No. 9, 1 Jul. - 1 Oct. 1965
Environmental study to evaluate slip ring materials suitable for operation in high vacuum
MATERIAL TESTING↗
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Fatigue hardening in niobium single crystals.
Nb single crystals of various orientations were cyclically deformed in tension-compression under strain control. At low strain amplitudes all crystals oriented for single slip and some oriented for multiple slip showed a two stage hardening. When present, the first stage was characterized with almost no cyclic work hardening. The rate of hardening in the second stage increased with strain amplitude and the amount of secondary slip. In crystals oriented for single slip kink bands developed on their side faces during rapid hardening stage which resulted in considerable amount of asterism in Laue spots. A cyclic stress-strain curve independent of prior history was found to exist which was also independent of crystal orientation. Furthermore, this curve differed only slightly from that of polycrystalline Nb obtained from data in literature.
Doner, M.↗
Electron Backscatter Diffraction (EBSD) Analysis and U-Pb Geochronology of the Oldest Lunar Zircon: Constraining Early Lunar Differentiation and Dating Impact-Related Deformation
The evolution of the early moon was dominated by two processes (i) crystallization of the Lunar Magma Ocean (LMO) and differentiation of potassium-rare earth element-phosphorous-rich residual magma reservoir referred to as KREEP, and (ii) an intense meteorite bombardment referred to as lunar cataclysm . The exact timing of these processes is disputed, and resolution relies on collection and interpretation of precise age data. This study examines the microstructure and geochronology of zircon from lunar impact breccias collected during the Apollo 17 mission. A large zircon clast within lunar breccia 72215,195 shows sector zoning in optical microscopy, cathodoluminescence (CL) imaging and Raman mapping, and indicates that it was a relict fragment of a much larger magmatic grain. Sensitive high resolution ion microprobe (SHRIMP) U-Pb analysis of the zircon shows that U and Th concentration correlate with sector zoning, with darkest CL domains corresponding with high-U and Th (approx.150 and approx.100 ppm respectively), and the brightest-CL sectors containing approx.30-50 ppm U and approx.10-20 ppm Th. This indicates that variations in optical CL and Raman properties correspond to differential accumulation of alpha-radiation damage in each sector. Electron backscatter diffraction (EBSD) mapping shows that the quality of electron backscatter patterns (band contrast) varies with sector zoning, with the poorest quality patterns obtained from high-U and Th, dark-CL zones. EBSD mapping also reveals a deformation microstructure that is cryptic in optical, CL and Raman imaging. Two orthogonal sets of straight discrete and gradational low-angle boundaries accommodate approx.12 misorientation across the grain. The deformation bands are parallel to the crystallographic {a}-planes of the zircon, have misorientation axes parallel to the c-axis, and are geometrically consistent with formation by dislocation creep associated with <100>{010} slip. The deformation bands are unlike curved morphology of crystal-plastic microstructures in tectonically deformed terrestrial zircon, and geometrically similar to dislocation microstructures reported in experimentally shocked zircon. We interpret these crystal-plastic deformation microstructures to have resulted from a significant impact, either directly from impact shock, or during ductile flow directly following the impact. The deformation bands appear to continue undeflected through the non-indexed, radiation-damaged areas of the grain, which suggests that the orientation variation predates any significant mechanical weakening from radiation damage in the grain, and therefore occurred early in its history.
Timms, Nick↗
Kink band formation in unidirectional composites under compression
The kink band formation in unidirectional composites under compression was studied with the help of optical and scanning electron microscopy. Materials studied included graphite/epoxy, S-2 glass/epoxy, and Kevlar 49/epoxy composites. The kink bands in the graphite/epoxy and glass/epoxy composites were initiated by fiber microbuckling while those in the Kevlar/epoxy composite were triggered by microkinking in the fibers themselves. Fracture surfaces of the graphite/epoxy composites showed fibers broken in bending and fiber segments tilted in the direction of slip. The kink band formation depended not only on the constituent material properties but also on the kinematic constraints imposed. Both primary and secondary kink bands were observed in the graphite/epoxy specimens, but only primary kink bands were present in the other two composites because of higher lateral flexibility of the specimen during testing.
Sohi, M. M.↗
Quantifying Exact Motions Along Lineaments on Europa
Evaluating the precise motions along lineaments on the surface of Jupiter's icy moon, Europa, is a valuable tool for interpreting the development and history of lineaments of various morphologies. Such morphologies include strike-slip faults, dilational bands, ridges, and convergence zones. However, the exact mode of origin and kinematic behavior of these various lineaments are not obvious based on morphology alone. In fact, the apparent motions implied by displaced crosscut features can provide misleading indications of true motions along lineaments. Identifying the precise motions (combinations of sliding and opening/closing) is critical to the accurate characterization and interpretation of each of these lineament types. Lineaments of interest (i.e., those having displaced relatively older features in some manner) are identified on Galileo spacecraft images and measurements are made of the total offset, the separation, and relative orientations of crosscut features with respect to the lineament of interest. Specifically, by using these measured quantities and a series of trigonometric equations, the precise motions (i.e., dilation, convergence, strike-slip, or a combination of strike-slip and dilation or convergence) can be determined. These measurements are, however, limited by the resolution of the available images. This study focuses on motion analysis techniques for Europan lineaments and the precise characterization of fault-orthogonal and/or strike-slip motion along lineaments of varying morphologies. We highlight potential pitfalls of cursory analyses of motion indicators. For example, lineaments with obvious lateral offsets have typically been identified simply as strike-slip faults. This assumption may actually be incorrect, as fault-orthogonal motions may contribute to apparent lateral displacements (offsets or separations). Also, variability in the amount of fault motion along the trace length should theoretically be identifiable using the outlined technique. Strike-slip faults on Europa have conventionally been presumed to have a constant slip magnitude along their lengths; however, we posit that variable distributions of slip may be common, as is typical along terrestrial strike-slip faults.
Vetter, J. C.↗
Manifestations of Dynamic Strain Aging in Soft-Oriented NiAl Single Crystals
The tensile and compressive properties of six NiAl-base single-crystal alloys have been investigated at temperatures between 77 and 1200 K. The normalized critical resolved shear stresses (CRSS/E) and work-hardening rates (Theta/E) for these alloys generally decreased with increasing temperature. However, anomalous peaks or plateaus for these properties were observed in conventional purity (CPNiAl), Si-doped (NiAl-Si), C-doped low Si (UF-NiAl1), and Mo-doped (NiAl-Mo) alloys at intermediate temperatures (600 to 1000 K). This anomalous behavior was not observed in high-purity, low interstitial material (HP-NiAl). Low or negative strain-rate sensitivities (SRS) also were observed in all six alloys in this intermediate temperature range. Coincident with the occurrence of negative strain-rate sensitivities was the observation of serrated stress-strain curves in the CPNiAl and NiAl-Si alloys. These phenomena have been attributed to dynamic strain aging (DSA). Chemical analysis of the alloys used in this study suggests that the main specie responsible for strain aging in NiAl is C but indicate that residual Si impurities can enhance the strain aging effects. The corresponding dislocation microstructures at low temperatures (300 to 600 K) were composed of well-defined cells. At intermediate temperatures (600 to 900 K), either poorly defined cells or coarse bands of localized slip, reminiscent of the vein structures observed in low-cycle fatigue specimens deformed in the DSA regime, were observed in conventional purity, Si-doped, and in Mo-doped alloys. In contrast, a well-defined cell structure persisted in the low interstitial, high-purity alloy. At elevated temperatures (greater than or equal to 1000 K), more uniformly distributed dislocations and sub-boundaries were observed in all alloys. These observations are consistent with the occurrence of DSA in NiAl single-crystal alloys at intermediate temperatures.
Weaver, M. L.↗
Low-Friction Joint for Robot Fingers
Mechanical linkage allows adjacent parts to move relative to each other with low friction and with no chatter, slipping, or backlash. Low-friction joint of two surfaces in rolling contact, held in alinement by taut flexible bands. No sliding friction or "stick-slip" motion: Only rolling-contact and bending friction within bands. Proposed linkage intended for finger joints in mechanical hands for robots and manipulators.
Ruoff, C. F.↗
Compression failure mechanisms of single-ply, unidirectional, carbon-fiber composites
A single-ply composite compression test was used to study compression failure mechanisms as a function of fiber type, matrix type, and interfacial strength. Composites made with low- and intermediate-modulus fibers (Hercules AS4 and IM7) in either an epoxy (Hercules 3501-6) or a thermoplastic (ULTEM and LARC-TPI) matrix failed by kink banding and out-of-plane slip. The failures proceeded by rapid and catastrophic damage propagation across the specimen width. Composites made with high-modulus fibers (Hercules HMS4/3501-6) had a much lower compression strength. Their failures were characterized by kink banding and longitudinal splitting. The damage propagated slowly across the specimen width. Composites made with fibers treated to give low interfacial strength had low compression strength. These composites typically failed near the specimen ends and had long kink bands.
Ha, Jong-Bae↗
Identification of geostructures of continental crust particularly as they relate to mineral resource evaluation
The author has identified the following significant results. Preliminary examination of ERTS-1 imagery in central and northern Alaska substantiates the existence of a conjugate set of northeast and northwest faults suggested by linears noted on Nimbus 4 images. Linears of both trends are well expressed and several have been mapped as faults, including the Shaw Creek fault. Imagery provides new data to support the interpretation that the Kobuk Trench is the northern margin of a broad west-trending fault zone bounded on the north and south by strike-slip faults. In northwestern Alaska, MSS band 5 imagery shows Mississippian limestone as white, while shale, sandstone, and chert of other ages appear dark. As the limestone is the basal formation of the numerous thrust plates stacked in the area, images of band 5 will assist significantly in depicting the distribution of the thrust plates. In south-central Alaska the newly described Totshunda fault is readily identified and extends into areas not yet mapped. Also shown is another fault parallel to the south of the Totshunda which has not yet been recognized in the field.
Gryc, G.↗
Slip in tungsten at high temperatures
Slip traces and direction and orientation of tensile axis, strained matrix, and deformation bands in single crystals of tungsten
SINGLE CRYSTAL↗
Patterns of fracture and tidal stresses on Europa
A comparison of dark band, triple band, and cuspate ridge orientations with the fracture patterns predicted for tidal distortion due to orbital recession and eccentricity is undertaken, to test the hypothesized identification of Europa's lineaments as tidal distortion and planetary volume change fractures. Short, reticule dark bands near the anti-Jove point could be tension cracks caused by orbital eccentricity. Long, arcuate dark bands and triple bands peripheral to the anti-Jove point may be strike-slip faults due to orbital recession. The orientation and distribution of cuspate ridges, if they are compressional, suggests their formation in response to a combination of orbital recession and planetary volume decrease. If surface fracturing is due to tidal deformation, important constraints are exerted by it on Europa's orbital evolution.
Helfenstein, P.↗
A tethering system for direct measurement of cardiovascular function in the caged baboon
A device suitable for the continuous measurement of physiological activity in large, conscious monkeys has permitted the direct recording of systemic arterial blood pressure and heart rate in caged baboons. The device comprises a lightweight fiberglass backpack, retained in place on the baboon by a thoracic elastic band and shoulder straps, and a flexible stainless steel tether connecting the pack to an electrocannular slip-ring in the top center of the baboon's cage. A chronically indwelling arterial catheter inserted retrograde into the abdominal aorta via the internal iliac artery and connected to a small pressure transducer on the pack provides direct measurement of blood pressure and heart rate. Body fluids can be sampled or drugs administered via an indwelling catheter in the inferior vena cava. Electrical and fluid connections between the fiberglass pack and recording and infusion equipment located outside the cage pass through the flexible tether and remain protected from the subject. The reliability of the tethering system has been demonstrated in physiological, pharmacological, and behavioral experiments with baboons.
Byrd, L. D.↗
A microscopic study of crack initiation mechanisms in 7075 aluminum alloy sheets.
A study of the opening mode of crack initiation in 7075-T6 aluminum alloy sheets has been conducted with the aid of a scanning electron microscope. Observations were made from several orientations, including the top view of the specimen which showed the notch profile and the edge view of the specimen which showed the entire notch front along the specimen thickness. It was found that the edge view exhibited the first signs of permanent deformation at about 55% of the breaking strength. These changes took the form of deformation bands which were aligned in the direction of the tensile axis and apparently defined limiting regions of homogeneous slip. It is felt that the appearance of microcracks at loads approaching the breaking strength was of fundamental importance in the formation of the final fracture surface. Many of these microcraks were initiated at intermetallic particles and other metallurgically weak regions on the notch surface. It was also possible to correlate the strain in the notch with the stress intensity factor for the various loads. Very large plastic strains were observed on the notch tip as compared to published values of elongation at fracture for unnotched specimens.
Jones, D. L.↗
Fault Offsets and Lateral Crustal Movement on Europa
Structural evidence is presented for tension cracking associated with strike slip faulting and crustal movement in the bright ice covered Galilean satellite Europa. The structure and morphology of wedge shaped bands argues that they formed as a result of the rotation and lateral displacement of crustal units bounded by near vertical faults penetrating through the brittle crustal layer. The significant rotation and lateral motion of crustal blocks near the anti-jove point on Europa, without graben formation, also argues that the lithosphere in the fractured area is mechanically decoupled from the solid silicate interior, by either warm ice at depth or liquid water. Ice at depth and at a large fraction of its melting temperature is expected to behave as a fluid over geologically short time intervals due to its extremely low viscosity relative to the cold, brittle ice near the surface. One proposed convection mechanism is thus considered unlikely as it would be difficult to transmit internal stress through a decoupling layer to the surface.
Schenk, P. M.↗
High purity silica reflective heat shield development
A hyperpure vitreous silica material is being developed for use as a reflective and ablative heat shield for planetary entry. Various purity grades and forms of raw materials were evaluated along with various processing methods. Slip casting of high purity grain was selected as the best processing method, resulting in a highly reflective material in the wavelength bands of interest (the visible and ultraviolet regions). The selected material was characterized with respect to optical, mechanical and physical properties using a limited number of specimens. The process has been scaled up to produce a one-half scale heat shield (18 in. dia.) (45.72 cm) for a Jupiter entry vehicle. This work is now being extended to improve the structural safety factor of the heat shield by making hyperpure silica material tougher through the addition of silica fibers.
Nachtscheim, P. R.↗
A new coherent demodulation technique for land-mobile satellite communications
An advanced coherent demodulation technique is described for land mobile satellite (LMS) communications. The proposed technique features a combined narrow/wind band dual open loop carrier phase estimator, which is effectively able to compensate the fast carrier phase fluctuation by fading with sacrificing a phase slip rate. Also included is the realization of quick carrier and clock reacquisition after shadowing by taking open loop structure. Its bit error rate (BER) performance is superior to that of existing detection schemes, showing a BER of 1 x 10(exp -2) at 6.3 dB E sub b/N sub o over the Rician channel with 10 dB C/M and 200 Hz (1/16 modulation rate) fading pitch f sub d for QPSK. The proposed scheme consists of a fast response carrier recovery and a quick bit timing recovery with an interpolation. An experimental terminal model was developed to evaluate its performance at fading conditions. The results are quite satisfactory, giving prospects for future LMS applications.
Yoshida, Shousei↗
Constitutive and Stability Behavior of Granular Materials Under Very Low Effective Stresses
The study of the behavior of granular materials such as sand is of great importance to the understanding of the response of foundations resting on surface and near-surface soil deposits. A clear understanding of the behavior of such materials can also provide insights into other related issues where low effective stresses are encountered such as liquefaction. The main sources of the constitutive and stability properties of cohesionless granular materials is interparticle friction, which in turn under low confinement stress levels is strongly affected by gravitational body forces under terrestrial (1 gravity) conditions. Under moderate-to-high stress levels, the influence of gravity on the behavior of experiments may not be pronounced and therefore the test results in a terrestrial environment may be acceptable for engineering purposes. However, the conduct of experiments on granular materials under very low stress levels and under quasi-static conditions can only be performed in a microgravity environment. A series of displacement-controlled cyclic triaxial compression experiments were performed in a SPACEHAB module on the Space Shuttle during the STS-79 mission to Mir in September, 1996, and the STS-89 mission in January, 1998. The experiments were conducted on six right cylindrical specimens 75 mm in diameter and 150 mm long at effective confining pressures of 0.05, 0.52 and 1.30 kPa. The results show very high peak strength friction angles in the range of 47.6 to 70.0 degrees, which are mainly due to overconsolidation and grain interlocking effects. It was observed that the residual strength levels were in the same range as that observed at higher confining stress levels. The dilatancy angles were unusually high in the range of 30 to 31 degrees. All specimens display substantial initial stiffnesses and elastic moduli during unloading and reloading events, which are nearly an order of magnitude higher than conventional theories predict. A periodic instability phenomenon which appears to result from buckling of multiple internal arches and columnar systems, augmented by stick-slips was observed in the experiments. Computed Tomography (CT) measurements revealed valuable data about the internal fabric and the specimens deformation patterns. Uniform diffuse bifurcation with multiple radial shear bands was observed in the specimens tested in a microgravity environment. In the axial direction, two major conical surfaces were developed. Spatial nonsymmetrical deformations were observed in specimens tested in terrestrial laboratory.
Alshibli, Khalid A.↗
Mechanics of Granular Materials (MGM) Microgravity Experiment
The second series of MGM experiment was conducted during the STS-89 mission in January 1998. The experiment was previously flow on Atlantis's STS-79 mission in September 1996. Six displacement-controlled, drained triaxial compression experiments were performed at very low effective confining stresses. The confining stresses were in the ranges 0.05, 0.52 and 1.30 kPa. Three experiments were subjected to monotonic loading and unloading cycles while the other three experiments were subjected to cyclic loading. The results show very high peak strength friction angles in the range of 47.6 to 70.0 degrees, which are mainly due to overconsolidation and grain interlocking effects. It was observed that the residual strength levels in the monotonic loading experiments were in the same range as that observed at higher confining stress levels. The dilatancy angles were unusually high in the range of 30 to 31 degrees. All specimens display substantial initial stiffnesses and elastic moduli during unloading and reloading events, which are nearly an order of magnitude higher than conventional theories predict. A periodic instability phenomenon which appears to result from buckling of multiple internal arches and columnar systems, augmented by stick-slips was observed in the experiments. Computed Tomography (CT) measurements revealed valuable data about the internal fabric and the specimens deformation patterns. Uniform diffuse bifurcation with multiple radial shear bands was observed in the specimens tested in a microgravity environment. In the axial direction, two major conical surfaces were developed. Spatial nonsymmetrical deformations were observed in specimens tested in terrestrial laboratory.
Alshibli, Khalid A.↗