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Development of Constellation-X Optics Technologies at MSFC

One of the major technological challenges for the Constellation X-ray Mission is the development of light-weight, high-resolution, grazing-incidence optics. NASA's Marshall Space Flight Center is developing and evaluating candidate technologies, based upon full-shell replication off precision mandrels. Here we report on recent progress in meeting the weight and imaging-performance requirements, using very thin, high-strength electroformed nickel alloys. In addition, we briefly describe MSFC's optics fabrication, metrology, and x-ray test facilities.

Odell, S. L.↗

Development of Constellation-X Optics Technologies at MSFC

One of the major technological challenges for the Constellation X-ray Mission is the development of light-weight, high-resolution, grazing-incidence optics. NASA's Marshall Space Flight Center is developing and evaluating candidate technologies, based upon full-shell replication off precision mandrels. Here we report on recent progress in meeting the weight and imaging-performance requirements, using very thin, high-strength electroformed nickel alloys. In addition, we briefly describe MSFC's optics fabrication, metrology, and x-ray test facilities.

ODell, S. L.↗

Improving X-ray Optics Through Differential Deposition

The differential deposition technique can in theory correct shell figures to approximate arcsecond value. We have received APRA funding and are building two custom system to demonstrate the technique on full shell and segmented optics. We hope to be able to demonstrate < 5 arcsec performance in < 2 years. To go beyond this, (arcsecond level) is very difficult to judge as we have not yet discovered the problems. May necessitate in-situ metrology, stress reduction investigations, correcting for gravity effects, correcting for temperature effects. Some of this will become obvious in early parts of the investigation.

Ramsey, Brian↗

X-Ray Optics for the 2020's

X-ray optics is an essential and enabling technology for x-ray astronomy. This slide presentation presents the authors views on the requirements for x-ray optics as progress is made toward building IXO and preparing for the 2020's. The presentation reviews the status of several technologies that are being developed and outlines the steps that we as a community needs to take to move toward x-ray optics meeting the five key requirements: (1) high angular resolution, (2) large effective area, (3) low mass, (4) fast production, and (5) low cost. There is discussion of segmentation vs full shell, size of the mirror segment, mirror segment frabrication, post-slumping figure improvement, and characterization of coating quality.

Zhang, Will↗

HERO: A Balloon-Borne Hard-X-Ray Focusing Telescope

HERO, for High Energy Replicated Optics, is an evolutionary balloon payload featuring hard-x-ray grazing-incidence nickel optics. The HERO payload is designed to perform high-sensitivity, fine spatial resolution observations of galactic and extragalactic sources in an energy range that is as yet unexplored with grazing-incidence optics. A proof-of-concept flight with just 6 x-ray mirrors was completed in 2001 and captured the first focused hard-x-ray images galactic sources. Since that time, the payload has been greatly expanded and now features 100, in-house-fabricated mirror shells with an attendant large increase in sensitivity. In its current form, HERO was flown in 2007, from Fort Sumner, NM, and is schedules to fly again in September 2009, from Alice Springs, NT. Full details of the HERO payload will be provided in this presentation together with a discussion of the challenges of flying moderate resolution x-ray optics from a balloon platform.

Ramsey, Brian↗

The role of the dopant in the electronic structure of erbium-doped TiO 2 for quantum emitters

Erbium-doped TiO 2 materials are promising candidates for advancing quantum technologies, necessitating a thorough understanding of their electronic and crystal structures to tailor their properties and enhance coherence times. This study explored epitaxial erbium-doped rutile TiO 2 films deposited on r-sapphire substrates using molecular beam epitaxy. Photoluminescence excitation spectroscopy demonstrated decreasing photoluminescence lifetimes with erbium doping, indicating limited optical coherence times. Lattice distortions associated with Er 3+ were probed by x-ray absorption spectroscopy, indicating that erbium primarily occupies Ti 4+ sites and influences oxygen vacancies. Significant lattice distortions in the higher-order shells and apparent full coordination around erbium suggest that additional defects are likely prevalent in these regions. These findings indicate that defects contribute to limited coherence times by introducing alternative decay pathways, leading to shorter photoluminescence lifetimes.

Crystallographic defects↗

Shrink Tape Technique for Heat Forming Aluminum Substrates for Thin Foil X-Ray Mirrors and the Neutron Star Interior Composition Explorer X-Ray Concentrators

Consistent improvements in the design and fabrication of thin-foil, epoxy-replicated x-ray mirrors for astronomical telescopes have yielded increasingly higher quality and more precise astrophysical data. The Neutron Star Interior Composition Explorer (NICER) x-ray timing mission optics continues this tradition and introduces design elements that promise even more accurate measurements and precise astrophysical parameters. The singly reflecting concentrators have a curved axial profile to improve photon concentration and a sturdy full shell structure for enhanced module stability. These design elements introduced the challenge of reliably forming mirror substrates at an acceptable production rate. By developing a technique using heat shrink tape to compress and conform thin aluminum mirror substrates to shaping mandrels, production rate improved with successful fabrication. The technique's efficiency was analyzed by measuring hundreds of substrate profiles postforming, performance testing completely assembled concentrators composed of every size substrate, and comparing the results to simulated fabrication scenarios. On average, the profiles were copied within 4.6 plus or minus 3.7 percent. These measurements and the overall success of NICER's optics, via ground calibration, have shown that the heat-shrink tape method is reliable, repeatable, and could be used in future missions to increase production rate and improve performance.

Balsamo, Erin↗

Preliminary Parametric Cost Model for X-Ray Grazing Incidence Optics for Space Flight

Parametric cost models offer a lot of utility in planning and comparing different missions and concepts. Furthermore, they have a significant advantage over other estimating methodologies as they can be quickly and easily replicated. The cost model presented in this paper focuses on estimating the most likely cost for the X-ray Mirror Assembly (XMA) of space-based X-ray telescopes with grazing incidence optics. The authors recognize the complexities of generating a single cost model that covers multiple fabrication techniques, so they have limited this preliminary study to techniques used on previous and current missions, such as direct polished glass full shell, replicated, and foil optics

Space Telescope Cost Model↗

Investigate zero-stress replicated optics

The contracted activities for the procurement of 'Investigate Zero-Stress Replicated Optics' to support the AXAF-S x-ray spectrometer mirrors has been completed. To date four large Wolter I grazing incidence x-ray optical shells have been electroformed from nickel. The mirrors were fabricated utilizing each of two nickel alloy plated aluminum substrates twice. A wide variety of testing has been completed by NASA MSFC and UAH. This testing includes heat treatment control tests, subscale plating and fixture testing, alloy control of the electroless nickel, adhesion and release testing of the gold to electroless nickel, electroforming instrumentation and software and fabrication of subscale models. The full scale shells are one millimeter thick nickel electrodeposited over a thin gold layer which in turn has the optical surface on the inside. The optical surface is the replicate of the surface prepared on the substrate. Appendix I briefly outlines the fabrication process. Major objectives which were shared by UAH and MSFC include the design of facilities, equipment and tooling and procurement of materials and equipment. Process development followed with the fabrication of small scale pilot units. Procurement commenced immediately and equipment and materials were ordered to implement the fabrication of first surface full scale substrates (mandrels) and the second surface electroformed optical components. All principal objectives have been achieved. Inspection of the mirrors in visible and x-ray modes validates that the required performance and the quality can be achieved by an electroforming replication process. A very distinct progressive improvement has been achieved with each of the four mirrors produced. The final mirror exceeded the original goals and set an improved standard for flight hardware. The future goal of a 30 arc second resolution at 8 KEV x-ray appears to be achievable by this process when proper cleanliness and process control is utilized.

Engelhaupt, Darell↗

CCD mosaic images of the supernova remnant 3C 400.2

We have constructed CCD mosaic images of the old Galactic supernova remnant 3C 400.2 in lines of H-alpha + forbidden N II, forbidden S II, and forbidden O III, plus a continuum band. These are the first CCD images covering the full extent of this remnant, and they reveal significantly more nebulosity than the deepest photographic plates. Comparison with radio and X-ray images indicates dramatically different morphology in the three regimes. The optical images both in H-alpha + forbidden N II and in forbidden S II show an almost complete, irregular shell of emission, with a diameter of about 16 arcmin, little over half that of the radio shell, while the X-ray structure is a centrally peaked ellipsoid. Approximate values for optical line fluxes are obtained; we estimate L(H-alpha) about 3 x 10 exp 35 ergs/s, roughly three times the X-ray luminosity. We also report a previously uncataloged planetary nebula southwest of 3C 400.2.

Winkler, P. F.↗

Constellation-X Spectroscopy X-Ray Telescope Requirements and Development Program: MSFC Research Program

The Constellation-X Spectroscopy X-ray Telescope (SXT) will provide high-throughput, high-resolution spectroscopy of cosmic sources, from 0.25 keV to 10 keV. Key to this capability is the development of large (1.6 m diameter), lightweight optics for the SXT mirror assembly. Teams led by NASA's Marshall Space Flight Center (MSFC), by NASA's Goddard Space Flight Center (GSFC), and by Italy's Osservatorio Astronomico di Brera (OAB) are currently developing competing mirror technologies for this planned mission. Each team is making significant research progress in developing mirror technologies which satisfy the SXT requirements for lightweight optics, consistent with a system-level optical performance of better than 15 arcsec half-power diameter. The NASA Marshall Space Flight Center (MSFC), in collaboration with the Smithsonian Astrophysical Observatory (SAO), has focussed its efforts on full-shell replicated optics, of electroformed nickel alloys. Recent progress in identifying a surface treatment to effect low, controlled adhesion and, more significantly, in developing new high-strength nickel alloys make this a viable, low cost approach to satisfying the SXT requirements.

O'Dell, S. L.↗

Metrology Mount and Optics Mandrels

This document is the Final Report for NASA Grant NAG8-1198 from NASA Marshall Space Flight Center (MSFC) to the Smithsonian Astrophysical Observatory (SAO). The Grant is entitled "Metrology Mount and Optics Materials." This final report is required by the terms of the Grant. The period of performance was from September 15, 1995 through January 14, 1999. Total funding received by SAO from MSFC for this effort was, $254,000. Mr. Lester Cohen carried out most of the work at SAO, but received limited support from other engineers, technicians, and designers. Dr. Harvey Tananbaum, the Principal Investigator for the grant provided overall direction and work- assessment. The Grant has had two funding augmentations to its basic amount and has, over time, emphasized three different research areas - each of which has been an extension of earlier research. The research activity was in 2 areas: (1) Expert opto-structural studies related to separation mechanics and effects of electro formed nickel X-ray mirrors. and (2) Design, fabrication and evaluation of a low force metrology and assembly station for light weight full shell electroformed X-ray mirrors.

Tananbaum, H.↗

Toward the fabrication of a 5 μm resolution Wolter microscope for the National Ignition Facility

Advancements in computer-controlled polishing, metrology, and replication have led to a x-ray mirror fabrication process that is capable of producing high-resolution Wolter microscopes. The mirror is a nickel-cobalt replicated full-shell mirror that was electroformed from a finely figured and polished mandrel. This mandrel was designed and fabricated for a 8 m source-to-detector distance microscope, with 10× magnification. A computer controlled polishing process corrected the low-frequency mandrel figure to < 2.0 nm RMS error. The mandrel design was optimized to reduce shell distortions that occur mainly < 20 mm from the shell ends. This design, in combination with improved replication tooling design and refined bath parameters informed by a detailed COMSOL model, have led to reductions in replication errors in the mirror shell. X-ray tests performed on a pair of mirror shells replicated from the mandrel have demonstrated < 10 μm FWHM source plane imaging resolution. Here we discuss the development process, highlight results from metrology and x-ray testing, and define a path for achieving 5 μm FWHM resolution.

Grazing Incidence, Wolter Microscope, X-ray Optics↗

Genesis Concentrator Target Particle Contamination Mapping and Material Identification

The majority of surface particles were found to be < 5 microns in diameter with increasing numbers close to the optical resolution limit of 0.3 microns. Acceleration grid EDS results show that the majority of materials appear to be from the SRC shell and SLA materials which include carbon-carbon fibers and Si-rich microspheres in a possible silicone binder. Other major debris material from the SRC included white paint, kapton, collector array fragments, and Al. Image analysis also revealed that SRC materials were also found mixed with the Utah mud and salt deposits. The EDS analysis of the acceleration grid showed that particles < 1 m where generally carbon based particles. Chemical cleaning techniques with Xylene and HF in an ultrasonic bath are currently being investigated for removal of small particles by the Genesis science team as well as ultra-pure water megasonic cleaning by the JSC team [4]. Removal of organic contamination from target materials is also being investigated by the science team with the use of UV-ozone cleaning devices at JSC and Open University [5]. In preparation for solar wind oxygen analyses at UCLA and Open University [1, 2], surface particle contamination on three Genesis concentrator targets was closely examined to evaluate cleaning strategies. Two silicon carbide (Genesis sample # 60001 and 60003) and one chemical vapor deposited (CVD) 13C concentrator target (60002) were imaged and mosaic mapped with optical microscopes. The resulting full target mosaic images and particle feature maps were subsequently compared with non-flight, but flight-like, concentrator targets and sample return capsule (SRC) materials. Contamination found on the flown concentrator acceleration grid was further examined using a scanning electron microscope (SEM). Energy dispersive X-ray spectroscopy (EDS) for particle identification was subsequently compared with the optical images from the flown targets. Figure 1 show that all three targets imaged in this report are fully intact and do not show any signs of material fractures. However, previous ellipsometry results and overview imaging of both flown SiC targets show a solar wind irradiation gradient from the center focal point to the outer edge [3]. In addition, due to the hard landing, each target has experienced varying degrees of impacts, scratches, and particle debris from the spacecraft and Utah impact site.

Calaway, Michael J.↗

The x ray reflectivity of the AXAF VETA-I optics

The x-ray reflectivity of the VETA-I optic, the outermost shell of the AXAF x-ray telescope, with a bare Zerodur surface, is measured and compared with theoretical predictions. Measurements made at energies of 0.28, 0.9, 1.5, 2.1, and 2.3 keV are compared with predictions based on ray trace calculations. The data were obtained at the x-ray calibrations facility at Marshall Space Flight Center with an electron impact x-ray source located 528 m from the grazing incidence mirror. The source used photoelectric absorption filters to eliminate bremsstrahlung continuum. The mirror has a diameter of 1.2 m and a focal length of 10 m. The incident and reflected x-ray flux are detected using two proportional counters, one located in the incident beam of x-rays at the entrance aperture of the VETA-I, and the other in the focal plane behind an aperture of variable size. Results on the variation of the reflectivity with energy as well as the absolute value of the reflectivity are presented. We also present a synchrotron reflectivity measurement with high energy resolution over the range 0.26 to 1.8 keV on a flat Zerodur sample, done at NSLS. We present evidence for contamination of the flat by a thin layer of carbon on the surface, and the possibility of alteration of the surface composition of the VETA-I mirror perhaps by the polishing technique. The overall agreement between the measured and calculated effective area of VETA-I is between 2.6 percent and 10 percent, depending on which model for the surface composition is adopted. Measurements at individual energies deviate from the best-fitting calculation to 0.3 to 0.8 percent, averaging 0.6 percent at energies below the high energy cutoff of the mirror reflectivity, and are as high as 20.7 percent at the cutoff. We also discuss the approach to the final preflight calibration of the full AXAF flight mirror.

Kellogg, Edwin M.↗

First Images from HERO: A Hard-X-Ray Focusing Telescope

We are developing a balloon-borne hard-x-ray telescope that utilizes grazing incidence optics. Termed HERO, for High-Energy Replicated Optics, the instrument will provide unprecented sensitivity in the hard-x-ray region and will achieve milliCrab-level sensitivity in a typical 3-hour balloon-flight observation and 50 microCrab sensitivity on ultra-long-duration flights. A recent proof-of-concept flight, featuring a small number of mirror shells captured the first focused hard-x-ray images of galactic x-ray sources. Full details of the payload, its expected future performance and its recent measurements are provided.

Ramsey, Brian D.↗

X-Ray Vision

We are fabricating optics for the hard-x-ray region using electroless nickel replication. The attraction of this process, which has been widely used elsewhere, is that the resulting full shell optics are inherently stable and thus can have very good angular resolution. The challenge with this process is to develop lightweight optics (nickel has a relatively high density of 8.9 g/cu cm), and to keep down the costs of mandrel fabrication. We accomplished the former through the development of high-strength nickel alloys that permit very thin shells without fabrication- and handling-induced deformations. For the latter, we have utilized inexpensive grinding and diamond turning to figure the mandrels and then purpose-built polishing machines to finish the surface. In-house plating tanks and a simple water-bath separation system complete the process. To date we have built shells ranging in size from 5 cm diameter to 50 cm, and with thickness down to 100 micron. For our HERO balloon program, we are fabricating over 200 iridium-coated shells, 250 microns thick, for hard-x-ray imaging up to 75 keV. Early test results on these have indicated half-power-diameters of 15 arcsec. The status of these and other hard-x-ray optics will be reviewed.

Ramsey, B. D.↗