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DOE OSTI2021

Characterizing the Effect of Capillary Heterogeneity on Multiphase Flow Pulsation in an Intermediate–Scale Beadpack Experiment using Time Series Clustering and Frequency Analysis

An intermediate-scale beadpack drainage experiment was conducted to investigate how simple layered lamination heterogeneity affects CO 2 flow. Two simple layers of capillary barriers are manually packed in the tank and slow drainage was carried out using analog fluids to mimic the capillary- and gravity-dominated CO 2 upward migration process in deep saline aquifers. Nonwetting phase saturation time series clustering analysis and frequency analysis have been conducted on the experimental data. Additionally, modified invasion percolation numerical simulations were done on a digital model of the beadpack to compare to experimental results. Results show that capillary barriers can lead to strong pulsation behavior, which in turn can cause unexpected early breaching through other barriers. The inlet pressure is found to be able to respond to saturation changes in far regions of the domain, indicating that the wetting phase can transmit pressure changes from the other phase. Although static simulations were not able to capture all the dynamic behavior observed in the experiment, Monte Carlo composite simulation results combining many different realizations can better illustrate how the nonwetting phase will behave in the heterogeneous domain. Furthermore, our results suggest the need for CO 2 storage site selection with preference given to aquifers with more capillary barriers with finer grain sizes to avoid flow pulsation and to retard plume upward migration.

58 GEOSCIENCES↗

DOE OSTI2020

Laser-heated capillary discharge plasma waveguides for electron acceleration to 8 GeV

A plasma channel created by the combination of a capillary discharge and inverse Bremsstrahlung laser heating enabled the generation of electron bunches with energy up to 7.8 GeV in a laser-driven plasma accelerator. The capillary discharge created an initial plasma channel and was used to tune the plasma temperature, which optimized laser heating. Although optimized colder initial plasma temperatures reduced the ionization degree, subsequent ionization from the heater pulse created a fully ionized plasma on-axis. The heater pulse duration was chosen to be longer than the hydrodynamic timescale of ≈ 1 ns, such that later temporal slices were more efficiently guided by the channel created by the front of the pulse. Here, simulations are presented which show that this thermal self-guiding of the heater pulse enabled channel formation over 20 cm. The post-heated channel had lower on-axis density and increased focusing strength compared to relying on the discharge alone, which allowed for guiding of relativistically intense laser pulses with a peak power of 0.85 PW and wakefield acceleration over 15 diffraction lengths. Electrons were injected into the wake in multiple buckets and times, leading to several electron bunches with different peak energies. To create single electron bunches with low energy spread, experiments using localized ionization injection inside a capillary discharge waveguide were performed. A single injected bunch with energy 1.6 GeV, charge 38 pC, divergence 1 mrad, and relative energy spread below 2% full-width half-maximum was produced in a 3.3 cm-long capillary discharge waveguide. This development shows promise for mitigation of energy spread and future high efficiency staged acceleration experiments.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2022

Life Expectancy of Evaporating Capillary Bridges Predicted by Tertiary Creep Modeling

The evaporation of capillary bridges is experimentally investigated at the microscale through a three-grain capillary cluster. This setting provides the minimum viable description of Haines jumps during evaporation, that is, capillary instabilities stemming from air entry into a saturated granular material. The displacement profile of a meniscus is obtained via digital image correlation for different grain materials, geometries, and separations. While it is well known that Haines jumps are triggered at the pore throat, we find that these instabilities are of three types depending on the separation. We also provide a temporal characterization of Haines jumps; we find that they are accurately described, as tertiary creep instabilities, by Voight’s relation, similarly to landslides and volcanic eruptions. This finding extends the description of capillary instabilities beyond their onset predicted by Laplace equilibrium. Our contribution also paves the way for a microscopically-informed description of desiccation cracks, of which Haines jumps are the precursors.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

NASA NTRS1971

Study of a heat rejection system using capillary pumping

Results of an analytical study investigating the application of capillary pumping to the heat rejection loop of an advanced Rankine cycle power conversion system are presented. The feasibility of the concept of capillary pumping as an alternate to electromagnetic pumping is analytically demonstrated. Capillary pumping is shown to provide a potential for weight and electrical power saving and reliability through the use of redundant systems. A screen wick pump design with arterial feed lines was analytically developed. Advantages of this design are high thermodynamic and hydrodynamic efficiency, which provide a lightweight easily packaged system. Operational problems were identified which must be solved for successful application of capillary pumping. The most important are the development of start up and shutdown procedures, and development of a means of keeping noncondensibles from the system and of earth-bound testing procedures.

Neal, L. G.↗

NASA NTRS1977

On two-dimensional packets of capillary-gravity waves

The motion of a two-dimensional packet of capillary-gravity waves on water of finite depth is studied. The evolution of a packet is described by two partial differential equations: the nonlinear Schroedinger equation with a forcing term and a linear equation, which is of either elliptic or hyperbolic type depending on whether the group velocity of the capillary-gravity wave is less than or greater than the velocity of long gravity waves. These equations are used to examine the stability of the Stokes capillary-gravity wave train. The analysis reveals the existence of a resonant interaction between a capillary-gravity wave and a long gravity wave. The interaction requires that the liquid depth be small in comparison with the wavelength of the (long) gravity waves and the evolution equations describing the dynamics of this interaction are derived.

Djordjevic, V. D.↗

NASA NTRS1980

Capillary acquisition devices for high-performance vehicles: Executive summary

Technology areas critical to the development of cryogenic capillary devices were studied. Passive cooling of capillary devices was investigated with an analytical and experimental study of wicking flow. Capillary device refilling with settled fluid was studied using an analytical and experimental program that resulted in successful correlation of a versatile computer program with test data. The program was used to predict Centaur D-1S LO2 and LH2 start basket refilling. Comparisons were made between the baseline Centaur D-1S propellant feed system and feed system alternatives including systems using capillary devices. The preferred concepts from the Centaur D-1S study were examined for APOTV and POTV vehicles for delivery and round trip transfer of payloads between LEO and GEO. Mission profiles were determined to provide propellant usage timelines and the payload partials were defined.

Blatt, M. H.↗

NASA NTRS1985

The Capillary Pumped Loop (CPL) GAS experiment G-471

The Capillary Pumped Loop (CPL) experiment, 6-471 is a thermal control system with high density heat acquisition and transport capability. The CPL consists of two capillary pumped evaporators with integral heaters, a fluid loop charged with ammonia (NH3), a condenser plate (heat sink), and various control electronics. The purpose of the experiment is to demonstrate the capability of a capillary pumped system under zero gravity conditions for use in the thermal control of large scientific instruments, advanced orbiting spacecraft, and space station components. A unique feature of the CPL is the capillary pumps, which contain no moving parts. Each pump contains a wick of porous material which is saturated with the working fluid (anhydrous ammonia). As heat is added to the fluid, it evaporates and travels to the condenser, thus transporting the heat (via the latent heat of vaporization) from the heat source to its sink at nearly a constant temperature. The evaporation process produces the pressure gradient or pumping action that circulates the fluid. This is the same principal that plants and trees use to transport water and nutrients from their roots to their leaves against gravity. The difference is that the CPL employs a closed system to return the fluid directly to the pumps, whereas "Mother Nature'' has an open system where the fluid is indirectly returned to the roots by condensation of water from the clouds in the form of rain. It should be noted that the CPL experiment was the first flight of a thermal control system of this type. It was also the first shuttle experiment from the Space Station Advanced Development Program.

Dan Butler↗

NASA NTRS1989

Capillary-Condenser-Pumped Heat-Transfer Loop

Heat being transferred supplies operating power. Capillary-condenser-pumped heat-transfer loop similar to heat pipe and to capillary-evaporator-pumped heat-transfer loop in that heat-transfer fluid pumped by evaporation and condensation of fluid at heat source and sink, respectively. Capillary condenser pump combined with capillary evaporator pump to form heat exchanger circulating heat-transfer fluids in both loops. Transport of heat more nearly isothermal. Thermal stress in loop reduced, and less external surface area needed in condenser section for rejection of heat to heat sink.

Silverstein, Calvin C.↗

NASA NTRS1993

Transient studies of capillary-induced flow

This paper presents the numerical and experimental results of a study performed on the transient rise of fluid in a capillary tube. The capillary tube problem provides an excellent mechanism from which to launch an investigation into the transient flow of a fluid in a porous wick structure where capillary forces must balance both adverse gravitational effects and frictional losses. For the study, a capillary tube, initially charged with a small volume of water, was lowered into a pool of water. The behavior of the column of fluid during the transient that followed as more water entered the tube from the pool was both numerically and experimentally studied.

Reagan, M. K.↗

NASA NTRS1999

Capillary Pumped Loop 3 Flight Experiment Overview

The Capillary Pumped Loop 3 (CAPL 3) Experiment is a follow on to the CAPL 1 and CAPL 2 experiments which flew on STS-60 (2/94) and STS-69 (9/95), respectively. CAPL 3 is tentatively scheduled to fly on the Space Shuttle in late 2000 as part of the Hitchhiker Experiments Advancing Technology (HEAT) payload. The experiment is a joint Naval Research Laboratory (NRL)/Goddard Space Flight Center (GSFC) payload which will meet technology objectives for both the Department of Defense and NASA. The primary objective of CAPL 3 is to demonstrate in space a multiple evaporator capillary pumped loop system, capable of reliable start-up, reliable continuous operation, and at least 50% heat load sharing with hardware for a deployable radiator. CAPL 3 is a full scale CPL system with four parallel capillary evaporators. The loop also contains a capillary starter pump, 8 parallel direct condensation condensers with associated flow regulators, a back pressure regulator, a two-phase reservoir, and various headers and transport tubing. A variable conductance heat pipe is located between one of the evaporators and the experiment radiator to provide a cooling source for the demonstration of heat load sharing. The experiment has an operating power range of 100 W to approximately 1400 W. The experiment ammonia charge will cause it to transition to a fixed conductance mode of operation if the radiator usage reaches 85%. Ambient functional tests have been performed on the experiment. Tests performed included start-up, low power, power cycles, high power, heat load sharing, variable/fixed conductance transition, saturation temperature changes, and pressure primes while the system was operating. The majority of the testing was performed at an ammonia saturation temperature of 30C, but a few tests were done at temperatures above and below this. The testing was highly successful. Details of the tests performed and a discussion of the results will be given in the presentation.

Ottenstein, Laura↗

NASA NTRS2001

Capillary Flow in Containers of Polygonal Section: Theory and Experiment

An improved understanding of the large-length-scale capillary flows arising in a low-gravity environment is critical to that engineering community concerned with the design and analysis of spacecraft fluids management systems. Because a significant portion of liquid behavior in spacecraft is capillary dominated it is natural to consider designs that best exploit the spontaneous character of such flows. In the present work, a recently verified asymptotic analysis is extended to approximate spontaneous capillary flows in a large class of cylindrical containers of irregular polygonal section experiencing a step reduction in gravitational acceleration. Drop tower tests are conducted using partially-filled irregular triangular containers for comparison with the theoretical predictions. The degree to which the experimental data agree with the theory is a testament to the robustness of the basic analytical assumption of predominantly parallel flow. As a result, the closed form analytical expressions presented serve as simple, accurate tools for predicting bulk flow characteristics essential to practical low-g system design and analysis. Equations for predicting corner wetting rates, total container flow rates, and transient surfaces shapes are provided that are relevant also to terrestrial applications such as capillary flow in porous media.

Weislogel, Mark M.↗

NASA NTRS2001

Investigation of Capillary Limit in a Loop Heat Pipe

This paper presets an experimental study on the capillary limit of a loop heat pipe (LHP) at low powers. The slow thermal response of the loop at low powers made it possible to observe interactions among various components after the capillary limit was exceeded. The capillary limit at low powers was achieved by imposing additional pressure drops on the vapor line through the use of a metering valve. A differential pressure transducer was also used to measure the pressure drop across the evaporator and the compensation chamber (CC). Test results show that when the capillary limit is exceeded, vapor will penetrate the primary wick, resulting in a partial dry-out of the evaporator and a rapid increase of the CC temperature. Because the evaporator can tolerate vapor bubbles, the LHP will continue to function and may reach a new steady state at the higher temperature. Thus, the LHP will exhibit a graceful degradation in performance rather than a complete failure. Moreover, the loop can recover from a partial dry-out by reducing the heat load without a re-start.

Ku, Jentung↗

NASA NTRS1992

Short-term reversibility of ultrastructural changes in pulmonary capillaries caused by stress failure

We previously showed that when the pulmonary capillaries in anesthetized rabbits are exposed to a transmural pressure (Ptm) of approximately 40 mmHg, stress failure of the walls occurs with disruption of the capillary endothelium, alveolar epithelium, or sometimes all layers. The present study was designed to determine whether some of the ultrastructural changes are rapidly reversible when the capillary pressure is reduced. To test this, the Ptm was raised to 52.5 cmH2O for 1 min of blood perfusion and then reduced to 12.5 cmH2O for 3 min of saline-dextran perfusion, followed by intravascular fixation at the same pressure. In another group of animals, the pressure was elevated for 1 min of blood and 3 min of saline-dextran before being reduced. The results were compared with previous studies in which the capillary pressures were maintained elevated at 52.5 cmH2O during the entire procedure. Control studies were also done at sustained low pressures. The results showed that the number of endothelial and epithelial breaks per millimeter and the total fraction area of the breaks were reduced when the pressure was lowered. For example, the number of endothelial breaks per millimeter decreased from 7.1 +/- 2.1 to 2.4 +/- 0.7, and the number of epithelial breaks per millimeter fell from 11.4 +/- 3.7 to 3.4 +/- 0.7. There was evidence that the breaks that closed were those that were initially small and were associated with an intact basement membrane. The results suggest that cells can move along their underlying matrix by rapid disengagement and reattachment of cell adhesion molecules, causing breaks to open or close within minutes.(ABSTRACT TRUNCATED AT 250 WORDS).

Non-NASA Center↗

NASA NTRS2009

The Capillary Flow Experiments Aboard the International Space Station: Increments 9-15

This report provides a summary of the experimental, analytical, and numerical results of the Capillary Flow Experiment (CFE) performed aboard the International Space Station (ISS). The experiments were conducted in space beginning with Increment 9 through Increment 16, beginning August 2004 and ending December 2007. Both primary and extra science experiments were conducted during 19 operations performed by 7 astronauts including: M. Fincke, W. McArthur, J. Williams, S. Williams, M. Lopez-Alegria, C. Anderson, and P. Whitson. CFE consists of 6 approximately 1 to 2 kg handheld experiment units designed to investigate a selection of capillary phenomena of fundamental and applied importance, such as large length scale contact line dynamics (CFE-Contact Line), critical wetting in discontinuous structures (CFE-Vane Gap), and capillary flows and passive phase separations in complex containers (CFE-Interior Corner Flow). Highly quantitative video from the simply performed flight experiments provide data helpful in benchmarking numerical methods, confirming theoretical models, and guiding new model development. In an extensive executive summary, a brief history of the experiment is reviewed before introducing the science investigated. A selection of experimental results and comparisons with both analytic and numerical predictions is given. The subsequent chapters provide additional details of the experimental and analytical methods developed and employed. These include current presentations of the state of the data reduction which we anticipate will continue throughout the year and culminate in several more publications. An extensive appendix is used to provide support material such as an experiment history, dissemination items to date (CFE publication, etc.), detailed design drawings, and crew procedures. Despite the simple nature of the experiments and procedures, many of the experimental results may be practically employed to enhance the design of spacecraft engineering systems involving capillary interface dynamics.

Jenson, Ryan M.↗

NASA NTRS2016

Demonstration of Nautilus Centripetal Capillary Condenser Technology

This paper describes the results of a proof of concept effort for development of a Nautilus Centripetal Capillary Condenser (NCCC or NC3) used for microgravity compatible water recovery from moist air with integral passive phase separation. Removal of liquid condensate from the air stream exiting a condenser is readily performed here on Earth. In order to perform this function in space however, without gravity or mechanical action, other tactics including utilization of inertial, drag and capillary forces are required. Within the NC3, liquid water forms via condensation on cold condenser surfaces as humid air passes along multiple spiral channels, each in its own plane, all together forming a stacked plate assembly. Non-mechanical inertial forces are employed to transfer condensate, as it forms, via centripetal action to the outer perimeter of each channel. A V-shaped groove, constructed on this outer edge of the spiral channel, increases local capillary forces thereby retaining the liquid. Air drag then pulls the liquid along to a collection region near the center of the device. Dry air produced by each parallel spiral channel is combined in a common orthogonal, out-of-plane conduit passing down the axial center of the stacked device. Similarly, the parallel condensate streams are combined and removed from the condenser/separator through yet another out-of-plane axial conduit. NC3 is an integration of conventional finned condenser operation, combined with static phase separation and capillary transport phenomena. A Mars' transit mission would be a logical application for this technology where gravity is absent and the use of vibrating, energy-intensive, motor-driven centrifugal separators is undesired. Here a vapor stream from either the Heat Melt Compactor or the Carbon dioxide Reduction Assembly, for example, would be dried to a dew point of 10 deg using a passive NC3 condenser/separator with the precious water condensate recycled to the water bus.

Separator↗

DOE OSTI2021

Capillary flow in UHPFRC with synthetic fibers, under high tensile stresses

A novel Ultra High-Performance Fiber Reinforced Concrete (UHPFRC) mix with synthetic fibers and a low clinker matrix, henceforth referred to as PE-UHPFRC, has been developed for structural applications. It exhibits a high tensile elastic limit above 7 MPa, a tensile strength of more than 10 MPa, and a very high tensile hardening domain of above 3.5%. In order to effectively use this material, its protective properties have been investigated on the basis of the effect of tensile deformation and subsequent cracking on water transport properties, for a wide range of tensile strain. A special setup was developed to measure the capillary absorption of liquids while the specimen is under tension. The results show a considerable reduction in capillary absorption in case of PE-UHPFRC compared with Strain Hardening Cement-based Composites (SHCC). Moreover, the results highlight the considerable effect of the onset of cracking on capillary absorption.

36 MATERIALS SCIENCE↗

DOE OSTI2024

An integrated approach to derive relative permeability from capillary pressure

Surface tension affects all aspects of fluid flow in porous media. Through measurements of surface tension interaction under multiphase conditions, a relative permeability curve can be determined. Relative permeability is a numerical description of the interaction between two or more fluids and the porous media. It is a critical parameter for various tools that characterize subsurface multiphase flow systems, such as numerical simulation for carbon sequestration, oil and gas development, and groundwater contamination remediation. Therefore, it is critical to get a good statistical distribution of relative permeability in the porous media under study. Empirical formula for determining relative permeability from capillary pressure are already well established but do not provide the needed flexibility that is required to match laboratory-derived relative permeability curves. By expanding the existing methods for calculating relative permeability from capillary pressure data, it is possible to create both two and three-phase relative permeability curves. Mercury intrusion capillary pressure (MICP) data from the Morrow 'B' Sandstone coupled with interfacial tension and contact angle measurements were used to create a suite of relative permeability curves. Furthermore, these curves were then calibrated to a small sample of existing laboratory curves to elucidate common fitting parameters for the formation that were then used to create relative permeability curves from MICP data that does not have an associated laboratory-measured relative permeability curve.

58 GEOSCIENCES↗

DOE OSTI2024

Development of a Hybrid Single/Two-Phase Capillary-Based Micro-Cooler using Copper Inverse Opals Wick with Silicon 3D Manifold for High-Heat-Flux Cooling Application

Previously, we reported two-phase capillary-based cooling using narrow (200 to 1000 ..mu..m) heater bridge copper inverse opal (CIO) wicks with heat flux level of 1400 Wcm -2 and superheat ~ 10 degrees C. Here, we demonstrate the area scaling of the proposed technology to a large-area micro-cooler for high-heat-flux cooling of microprocessors and power electronics. We developed a hybrid single/two-phase micro-cooler that relies on capillary-wicking in a 25-..mu..m-thick CIO with an open silicon microchannel 3D-manifold for liquid delivery and vapor extraction, achieving a high heat flux ~ 400 Wcm -2 over a heated area of 10 x 10 mm 2 . For a range of inlet water flowrates from 5 to 60 g(min) -1 , we achieved total thermal resistances and vapor qualities of 0.68 cm 2 degrees CW -1 to 0.2 cm 2 degrees CW -1 and 0.55 to 0.12, respectively. The flowrates are 10x smaller than those of conventional single- or two-phase microchannel cooling technology. The corresponding two-phase thermal resistances ranges from 0.05 to 0.02 cm 2 degrees CW -1 with temperature superheat of 8 to 6 degrees C, respectively. While the overall performance of the large-area (10 x 10 mm 2 ) capillary-based micro-cooler degraded compared to the previous demonstration of the technology for a heated area of 5 x 5 mm 2 , however, preliminary CFD modeling indicates that an improved manifold design will be able to achieve comparable performance.

capillary flow↗