Large-scale plane wave shock experiments designed for sample recovery
Planar shock wave test assembly for simulating meteoritic impact on planetary rock surface
METEORITE COLLISION↗
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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
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Experiment design session: Sampling and aggregation in LACIE
There are no author-identified significant results in this report.
Hallum, C.↗
Superflux I, II, and III experiment designs: Water sampling and analyses
Both airborne remote sensors and seagoing research vessels were used to study the effects of man's continual use of the Chesapeake Bay offshore environments. The major focus of the study was to: (1) advance the development and transfer of improved remote sensing systems and techniques for monitoring environmental quality and effects on living marine resources; (2) increase understanding of the influence of estuarine outwellings (plumes) on contiguous shelf ecosystems; and (3) provide a synoptic, integrated and timely data base for application to problems of marine resources and environmental quality.
Thomas, J. P.↗
Nationwide Forestry Applications Program. Renewable Resources Inventory Project. Multiresource Inventory Methods Pilot Test (phase 1): Multiresource Inventory Design and Sampling Network, volume 1
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Hot stage and sample cell design for the solidification of transparent materials with and without forced convection
A temperature gradient stage design for optical microscopy is described. Exceptional thermal stability is the major feature. The stage is used to study crystal growth phenomena occurring at the solid-liquid interface. The apparatus is designed to use transparent organic solutions as models for the study of metal-like solidification. The stage provides a controlled thermal environment for unidirectional solidification of low melting temperature materials. Freezing rate is regulated by mechanically sliding in the stage a thin glass cell containing the materials being studied. Two cell assemblies are described. One type is used for convection-free and the other for controlled forced convection studies of the solidification interface.
Kaukler, W. F.↗
Laboratory Reflectance Spectra of 160 Minerals, 0.4 to 2.5 Micrometers
This reports provides reflectance spectra of 160 minerals in both digital and printed form. In order to demonstrate the effect of particle size on reflectance, the spectral data for 135 of the minerals are presented at three different grain sizes. These are 125-500 microns, 45-125 microns and less than 45 microns. Ancillary information is provided with each mineral spectrum, which includes the mineral name, minerology, supplier, sampling locality and our designated sample number. The purity of every mineral sample was evaluated by X-ray diffraction (XRD). The composition of certain minerals known to deviate strongly from idealized end-member compositions was determined by electron microprobe analysis. The compositional information obtained by microbe analysis and accessory minerals identified by XRD are noted with the ancillary information. In addition, the spectrum acquired from the coarsest grain size available for each sample was processed with a feature-finding algorithm to quantify the characteristics of the spectral absorption features. All the reflectance spectra presented here are provided in digital form on IBM-compatible 3.5" diskettes. Also included on diskette is a program for displaying the spectral data and searching for spectral features that runs on an IBM-compatible PC with standard VCA graphics.
reflectance spectra↗
Compact, portable, automatic sample changer stick for cryostats and closed-cycle refrigerators
Beamlines are facilities that produce and deliver highly focused and intense beams of radiation, typically x rays, synchrotron radiation, or neutrons, for scientific research purposes. Millions of dollars are spent annually to maintain and operate these scientific beamlines, oftentimes running continuously between cycles. To reduce human intervention and improve productivity, mechanical sample changers are often commissioned for use. Designing sample changers is difficult because mechanical parts can be bulky, expensive, and challenging to design for instruments with low volume access, high radiation, and cryogenic environments. We present a portable and inexpensive sample changer stick that can hold and manipulate up to four samples, specifically designed for use with cryogenic closed-cycle refrigerators. The sample changer stick enables rapid and efficient exchange of samples without manual intervention, and is compatible with standard sample mounts such as vanadium cans. The sample changer stick includes a motorized rotation and lancing mechanism, which enables the precise positioning of each sample in the neutron beam, while ensuring compatibility with the operating temperatures and vacuum conditions required for closed-cycle refrigerators. The design has been successfully tested at the VISION beamline at the Spallation Neutron Source. The mechanical action and software controls are detailed. Furthermore, the sample changer stick is a valuable tool for scientists working with cryogenic closed-cycle refrigerators.
36 MATERIALS SCIENCE↗
Statistical methods for efficient design of community surveys of response to noise: Random coefficients regression models
Research studies of residents' responses to noise consist of interviews with samples of individuals who are drawn from a number of different compact study areas. The statistical techniques developed provide a basis for those sample design decisions. These techniques are suitable for a wide range of sample survey applications. A sample may consist of a random sample of residents selected from a sample of compact study areas, or in a more complex design, of a sample of residents selected from a sample of larger areas (e.g., cities). The techniques may be applied to estimates of the effects on annoyance of noise level, numbers of noise events, the time-of-day of the events, ambient noise levels, or other factors. Methods are provided for determining, in advance, how accurately these effects can be estimated for different sample sizes and study designs. Using a simple cost function, they also provide for optimum allocation of the sample across the stages of the design for estimating these effects. These techniques are developed via a regression model in which the regression coefficients are assumed to be random, with components of variance associated with the various stages of a multi-stage sample design.
Tomberlin, T. J.↗
Triton Field Trials - Changes in Habitats, a Literature Review of Monitoring Technologies
Marine energy devices are installed in highly dynamic environments and have the potential to affect benthic and pelagic habitats around them. Regulatory bodies often require baseline characterization and/or post-installation monitoring to determine whether changes in these habitats are being observed. However, a great diversity of technologies is available for surveying and sampling marine habitats. Selecting the most suitable instrument to identify and measure changes in habitats at marine energy sites can become a daunting task. We conducted a thorough review of journal articles, survey reports, and grey literature to extract information about the technologies used, the data collection and processing methods, and the performance and effectiveness of these instruments. We examined documents related to marine energy development, offshore wind farms, oil and gas offshore sites, and other marine industries around the world over the last 20 years, as well as national and international guidelines for surveying habitats around offshore activities. A total of 120 different technologies were identified across six main habitat categories: seafloor, sediment, infauna, epifauna, pelagic, and biofouling. The technologies were organized into 12 broad technology classes: acoustic, corer, dredge, grab, hook and line, net and trawl, plate, remote sensing, scrape samples, trap, visual, and others. Visual was the most common and the most diverse technology class, with applications across all six habitat categories. Sampling designs varied considerably among the reviewed studies but transect was the predominant design for surveying seafloor, epifauna, and pelagic habitats. The most common data analyses were univariate and multivariate statistical analyses aimed at calculating and comparing biodiversity indices, characterizing faunal assemblages or sediment classes, or modeling the distribution of animals related to abiotic parameters. Technologies and sampling methods adaptable and designed to work efficiently in energetic environments have greater success at marine energy sites. In addition, sampling designs and statistical analyses should be carefully thought through to identify differences in faunal assemblages and spatiotemporal changes in habitats.
16 TIDAL AND WAVE POWER↗
High Frequency Monitoring and Nitrate Sourcing Reveals Baseflow and Stormflow Controls on Total Dissolved Nitrogen and Carbon Export Along a Rural‐Urban Gradient
Abstract Efforts to reduce nitrogen and carbon loading from developed watersheds typically target specific flows or sources, but across gradients in development intensity there is no consensus on the contribution of different flows to total loading or sources of nitrogen export. This information is vital to optimize management strategies leveraging source reductions, stormwater controls, and restorations. We investigate how solute loading and sources vary across flows and land‐use using high frequency monitoring and stable nitrate isotope analysis from five catchments with different sanitary infrastructure, along a gradient in development intensity. High frequency monitoring allowed estimation of annual loading and attribution to storm versus baseflows. Nitrate loads were 16 kg/km 2 /yr. from the forested catchment and ranged from 68 to 119 kg/km 2 /yr., across developed catchments, highest for the septic served site. Across developed catchments, baseflow contributions ranged from 40% of N loading to 75% from the septic served catchment, and the contribution from high stormflows increased with development intensity. Stormflows mobilized and mixed many surface and subsurface nitrate sources while baseflow nitrate was dominated by fewer sources which varied by catchment (soil, wastewater, or fertilizer). To help inform future sampling designs, we demonstrate that grab sampling and targeted storm sampling would likely fail to accurately predict annual loadings within the study period. The dominant baseflow loads and subsurface stormflows are not treated by surface water management practices primarily targeted to surface stormflows. Using a balance of green and gray infrastructure and stream/riparian restoration may target specific flow paths and improve management.
Delesantro, Joseph M.↗
Stress constraints in optimality criteria design
Procedures described emphasize the processing of stress constraints within optimality criteria designs for low structural weight with stress and compliance constraints. Prescreening criteria are used to partition stress constraints into either potentially active primary sets or passive secondary sets that require minimal processing. Side constraint boundaries for passive constraints are derived by projections from design histories to modify conventional stress-ratio boundaries. Other procedures described apply partial structural modification reanalysis to design variable groups to correct stress constraint violations of unfeasible designs. Sample problem results show effective design convergence and, in particular, advantages for reanalysis in obtaining lower feasible design weights.
Levy, R.↗
Converter design techniques and applications
Transistorized direct current voltage converters offer a number of advantages over other types because of their small size, low weight, high efficiency, high reliability, precision accuracy and wide range of control. There are three basic types of converter subsystems: series converter in which a voltage-controlled component is placed in series with the load; shunt converter in which a current-controlled component is placed in shunt with the load; and a switching converter in which a voltage-controlled component is turned on and off in series with the load. Converters employing any of these three types of subsystems can provide constant voltage, constant current, or constant impedance across the load. Design and application considerations, step-by-step design procedures, and the solution to sample design problems for the series, shunt, and switching types are presented.
Lalli, V. R.↗
A remote sensing-aided small grains inventory using sequential Landsat imagery
A procedure for manual acreage estimation from Landsat imagery is proposed which involves a stepwise sequence of area stratification, simple size estimation, acreage estimation, and acreage precision calculation. The sample design consists of a systematic point sample of the Landsat imagery for crop type presence calibrated by a double sample of several image points having crop season-coincident ground data. The sample point layout chosen for cost-efficiency in manual sampling is a doubly aligned point matrix. The significant advantage of this sampling approach is that crop information is available from throughout the agricultural reporting unit. For technique demonstration purposes three strata were selected for sampling. The proposed technique can complement more sophisticated computer-based acreage estimation methodologies, and refinements in the sampling techniques promise significant improvements for operational utility.
Thomas, R. W.↗
Equations for the design of two-dimensional supersonic nozzles
Equations are presented for obtaining the wall coordinates of two-dimensional supersonic nozzles. The equations are based on the application of the method of characteristics to irrotational flow of perfect gases in channels. Curves and tables are included for obtaining the parameters required by the equations for the wall coordinates. A brief discussion of characteristics as applied to nozzle design is given to assist in understanding and using the nozzle-design method of this report. A sample design is shown.
Pinkel, I Irving↗
Mars Orbiter Sample Return Power Design
The NASA/JPL 2003/2005 Mars Sample Return (MSR) Missions will each have a sample return canister that will be filled with samples cored from the surface of MARS. These spherical canisters will be 14.8 cm in diameter and must be powered only by solar cells on the surface and must communicate using RF transmission with the recovery vehicle that will be coming in 2006 or 2009 to retrieve the canister. This paper considers the aspect and conclusion that went into the design of the power system that achieves the maximum power with the minimum risk. The power output for the spherical orbiting canister was modeled and plotted in various views of the orbit by the SOAP program developed by JPL. The requirements and geometry for a solar array on a sphere are unique and place special constraints on the design. These requirements include 1) accommodating a lid for sample loading into the canister, surface area was restricted from use on the Northern pole of the spherical canister. 2) minimal cell surface coverage (maximum cell efficiency), less than 40%, for recovery vehicle to locate the canister by optical techniques. 3) a RF transmission during 50% of MARS orbit time on any spin axis, which requires optimum circuit placement of the solar cell onto the spherical canister. The best configuration would have been a 4.5 volt round cell, but in the real world we compromised with six triangular silicon cells connected in series to form a hexagon. These hexagon circuits would be mounted onto a flat facet cut into the spherical canister. The surface flats are required in order to maximize power, the surface of the cells connected in series must be at the same angle relative to the sun. The flat facets intersect each other to allow twelve circuits evenly spaced just North and twelve circuits South of the equator of the spherical canister. Connecting these circuits in parallel allows sufficient power to operate the transmitter at minimum solar exposure, Northern pole of the canister facing the sun. Additional power, as much as 20%, is also generated by the circuits facing MARS due to albedo of MARS.
Mardesich, N.↗
NASA/BLM APT, phase 2. Volume 2: Technology demonstration
Techniques described include: (1) steps in the preprocessing of LANDSAT data; (2) the training of a classifier; (3) maximum likelihood classification and precision; (4) geometric correction; (5) class description; (6) digitizing; (7) digital terrain data; (8) an overview of sample design; (9) allocation and selection of primary sample units; (10) interpretation of secondary sample units; (11) data collection ground plots; (12) data reductions; (13) analysis for productivity estimation and map verification; (14) cost analysis; and (150) LANDSAT digital products. The evaluation of the pre-inventory planning for P.J. is included.
Source record↗
Thermal Design and Analysis for the Cryogenic MIDAS Experiment
The Materials In Devices As Superconductors (MIDAS) spaceflight experiment is a NASA payload which launched in September 1996 on the Shuttle, and was transferred to the Mir Space Station for several months of operation. MIDAS was developed and built at NASA Langley Research Center (LaRC). The primary objective of the experiment was to determine the effects of microgravity and spaceflight on the electrical properties of high-temperature superconductive (HTS) materials. The thermal challenge on MIDAS was to maintain the superconductive specimens at or below 80 K for the entire operation of the experiment, including all ground testing and 90 days of spaceflight operation. Cooling was provided by a small tactical cryocooler. The superconductive specimens and the coldfinger of the cryocooler were mounted in a vacuum chamber, with vacuum levels maintained by an ion pump. The entire experiment was mounted for operation in a stowage locker inside Mir, with the only heat dissipation capability provided by a cooling fan exhausting to the habitable compartment. The thermal environment on Mir can potentially vary over the range 5 to 40 C; this was the range used in testing, and this wide range adds to the difficulty in managing the power dissipated from the experiment's active components. Many issues in the thermal design are discussed, including: thermal isolation methods for the cryogenic samples; design for cooling to cryogenic temperatures; cryogenic epoxy bonds; management of ambient temperature components self-heating; and fan cooling of the enclosed locker. Results of the design are also considered, including the thermal gradients across the HTS samples and cryogenic thermal strap, electronics and thermal sensor cryogenic performance, and differences between ground and flight performance. Modeling was performed in both SINDA-85 and MSC/PATRAN (with direct geometry import from the CAD design tool Pro/Engineer). Advantages of both types of models are discussed. Correlation of several models to ground testing and flight data (where available) is presented. Both SINDA and PATRAN models predicted the actual thermal performance of the experiment well, even without post-flight correlation adjustments of the models.
Amundsen, Ruth McElroy↗
The use of gas chromatography – high resolution mass spectrometry for suspect screening and non-targeted analysis of per- and polyfluoroalkyl substances
This study is a workflow development for the analysis, identification, and categorization of per- and polyfluoroalkyl substances (PFAS) using gas chromatography-high resolution mass spectrometry (GC-HRMS) with non-targeted analysis (NTA) and suspect screening techniques. The behavior of various PFAS in a GC-HRMS was studied with regards to retention indices, ionization susceptibility, fragmentation patterns, etc. A custom PFAS database was constructed from 141 diverse PFAS. The database contains mass spectra from electron ionization (EI) mode, as well as MS and MS/MS spectra from positive and negative chemical ionization (PCI and NCI, respectively) modes. Common fragments of PFAS were identified across a diverse set of 141 PFAS analyzed. A workflow for suspect screening of PFAS and partially fluorinated products of incomplete combustion/destruction (PICs/PIDs) was developed which utilized both the custom PFAS database and external databases. PFAS and other fluorinated compounds were identified in both a challenge sample (designed to test the identification workflow) and incineration samples suspected to contain PFAS and fluorinated PICs/PIDs. The challenge sample resulted in a 100% true positive rate (TPR) for PFAS which were present in the custom PFAS database. In conclusion, several fluorinated species were tentatively identified in the incineration samples using the developed workflow.
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗