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Spectral Measurements of PMCs from SBUV/2 Instruments

The SBUV/2 (Solar Backscattered Ultraviolet, model 2) instrument is designed to monitor ozone stratospheric profile and total column ozone using measurements of the Earth's backscattered ultraviolet albedo. We have previously demonstrated that the normal radiance measurements from SBUV/2 instruments, which sample 12 discrete wavelengths between 252 and 340 nm during each scan, can be used to identify polar mesospheric clouds (PMCs). Some SBUV/2 instruments also periodically view the earth in continuous scan mode, covering the wavelength range 160-400 nm with 0.15 nm sampling. Analysis of these data show PMC occurrence rates similar to the normal discrete scan results, although the observation technique reduces the number of daily measurements by a factor of six. PMC observed by SBUV/2 instruments show a monotonic variation in the residual spectral albedo over the wavelength range 250 300 nm, with maximum enhancements of 10 15% at 250 nm. This result is consistent with microphysical model predictions from Jensen [1989. A numerical model of polar mesospheric cloud formation and evolution, Ph. D. Thesis, University of Colorado]. We find no evidence for a systematic localized increase in PMC residual albedo for wavelengths near 260 nm, in contrast to the recently reported results from the MSX UVISI instrument [Carbary J.F., et al., 2004. Evidence for bimodal particle distribution from the spectra of polar mesospheric clouds. Geophysics Research. Letters 31, L13108]. This result is observed for three different SBUV/2 instruments in both Northern and Southern Hemisphere data over a 13-year span. Our Mie scattering calculations show that the location and magnitude of the 260 nm hump feature is dependent upon the specific scattering angles appropriate to the MSX measurements. Although it explains the MSX spectrum, the bimodal size distribution proposed by Carbary et al. (2004), cannot explain the lack of scattering angle dependence of the SBUV/2 spectral shapes. The spectral signature of the SBUV/2 continuous scan PMC data is thus inconsistent with the bimodal particle size distribution suggested by Carbary et al. (2004).

DeLand, Matthew T.↗

Failure of the ERBE scanner instrument aboard NOAA 10 spacecraft and results of failure analysis

The Earth Radiation Budget Experiment (ERBE) scanner instrument on the NOAA 10 spacecraft malfunctioned on May 22, 1989, after more than 4 years of in-flight operation. After the failure, all instrument operational mode commands were tested and the resulting data analyzed. Details of the tests and analysis of output data are discussed therein. The radiometric and housekeeping data appear to be valid. However, the instrument will not correctly execute operational scan mode commands or the preprogrammed calibration sequences. The data indicate the problem is the result of a failure in the internal address decoding circuity in one of the ROM (read only memory) chips of the instrument computer.

Miller, J. B.↗

A Multisensor Investigation of Convection During HyMeX SOP1 IOP13

A multisensor analysis of the convective precipitation event occurred over Rome during the IOP13 (October 15th, 2012) of the HyMeX (Hydrological cycle in the Mediterranean eXperiment) Special Observation Period (SOP) 1 is presented. Thanks to the cooperation among Italian meteorological services and scientific community and a specific agreement with NASA-GSFC, different types of devices for meteorological measurements were made available during the HyMeX SOP.1. For investigating this event, used are the 3-D lightning data provided by the LINET, the CNR ISAC dual-pol C-band radar (Polar 55C), located in Rome, the Drop Size Distributions (DSD) collected by the 2D Video Disdrometer (2DVD) and the collocated Micro Rain Radar (MRR) installed at the Radio Meteorology Lab. of "Sapienza" University of Rome, located 14 km from the Polar 55C radar. The relation between microphysical structure and electrical activity during the convective phase of the event was investigated using LINET lightning data and Polar 55C (working both in PPI and RHI scanning mode) observations. Location of regions of high horizontal reflectivity (Zh) values ( > 50 dBz), indicating convective precipitation, were found to be associated to a high number of LINET strokes. In addition, an hydrometeor classification scheme applied to the Polar 55C scans was used to detect graupel and to identify a relation between number of LINET strokes and integrated IWC of graupel along the event. Properties of DSDs measured by the 2DVD and vertical DSD profiles estimated by MRR and their relation with the lighting activity registered by LINET were investigated with specific focus on the transition from convective to stratiform regimes. A good agreement was found between convection detected by these instruments and the number of strokes detected by LINET.

Roberto, N.↗

Nimbus 7 Solar Backscatter Ultraviolet (SBUV) spectral scan solar irradiance and Earth radiance product user's guide

The archived tape products from the spectral scan mode measurements of solar irradiance (SUNC tapes) and Earth radiance (EARTH tapes) by the Solar Backscatter UV (SBUV) instrument aboard Nimbus 7 are described. Incoming radiation from 160 to 400 nm is measured at intervals of 0.2 nm. The scan-to-scan repeatability of the solar irradiance measurements ranges from approximately 0.5 to 1 percent longward of 280 nm, to 2 percent around 210 nm and 4 percent near 175 nm. The repeatability of the Earth radiance values ranges from 2 to 3 percent at longer wavelengths and low zenith angles to 10 percent at shorter wavelengths and high zenith angles. The tape formats are described in detail, including file structure and contents of each type of record. Catalogs of the tapes and the time period covered are provided, along with lists of the days lacking solar irradiance measurements and the days dedicated to Earth radiance measurements. The method for production of the tapes is outlined and quality control measures are described. How radiances and irradiances are derived from the raw counts, the corrections for changes in instrument sensitivity, and related uncertainties are discussed.

Schlesinger, Barry M.↗

Design of the PIXIE Adiabatic Demagnetization Refrigerators

The Primordial Inflation Explorer (PIXIE) is a proposed mission to densely map the polarization of the cosmic microwave background. It will operate in a scanning mode from a sun-synchronous orbit, using low temperature detectors (at 0.1 K) and located inside a teslescope that is cooled to approximately 2.73 K - to match the background temperature. A mechanical cryocooler operating at 4.5 K establishes a low base temperature from which two adiabatic demagnetization refrigerator (ADR) assemblies will cool the telescope and detectors. To achieve continuous scanning capability, the ADRs must operate continuously. Complicating the design are two factors: 1) the need to systematically vary the temperature of various telescope components in order to separate the small polarization signal variations from those that may arise from temperature drifts and changing gradients within the telescope, and 2) the orbital and monthly variations in lunar irradiance into the telescope barrels. These factors require the telescope ADR to reject quasi-continuous heat loads of 2-3 millwatts, while maintaining a peak heat reject rate of less than 12 milliwatts. The detector heat load at 0.1 K is comparatively small at 1-2 microwatts. This paper will describe the 3-stage and 2-stage continuous ADRs that will be used to meet the cooling power and temperature stability requirements of the PIXIE detectors and telescope.

adiabatic demagnetization refrigerator↗

X-Ray Diffraction Techniques for a Field Instrument: Patterns of Lithologic Provences

Future exploration of Mars will attempt to shed light on the mineralogy of surface materials. Instruments deployed from remote platforms should have the capability to conduct both intensive analyses as well as rapid, reconnaissance surveys while they function in the martian environment as surrogate geologists. In order to accommodate the reconnaissance mode of analysis and to compensate for analytical limitations imposed by the space-flight conditions, data analysis methods are being developed that will permit interpretation of data by recognition of signatures or "fingerprints". Specifically, we are developing a technique which will allow interpretation of diffraction patterns by recognition of characteristic signatures of different lithologic provences. This technique allows a remote vehicle to function in a rapid-scan mode using the lithologic signature to determine where a more thorough analysis is needed. An x-ray diffraction pattern is characterized by the angular positions of diffracted x-rays, x-ray intensity levels and background radiation levels. These elements may be used to identify a generalized x-ray signature. Lithologic signatures are being developed in two ways. A signature is composed using the ideal powder diffraction indices from the mineral assembledge common to a specific lithologic provence. This is then confirmed using a laboratory diffraction pattern of a whole rock powder. Preliminary results comparing the diffraction signatures of the major mineral assembledges common to basalt, carbonate, and evaporite basin deposits indicate that lithologies are differentiable as a "fingerprint". Statistical analyses are being performed to establish the confidence levels of this technique.

Marshall, J.↗

Atmospheric modeling related to Thematic Mapper scan geometry

A simulation study was carried out to characterize atmospheric effects in LANDSAT-D Thematic Mapper data. In particular, the objective was to determine if any differences would result from using a linear vs. a conical scanning geometry. Insight also was gained about the overall effect of the atmosphere on Thematic Mapper signals, together with the effects of time of day. An added analysis was made of the geometric potential for direct specular reflections (sun glint). The ERIM multispectral system simulation model was used to compute inband Thematic Mapper radiances, taking into account sensor, atmospheric, and surface characteristics. Separate analyses were carried out for the thermal band and seven bands defined in the reflective spectral region. Reflective-region radiances were computed for 40 deg N, 0 deg, and 40 deg S latitudes; June, Mar., and Dec. days; and 9:30 and 11:00 AM solar times for both linear and conical scan modes. Also, accurate simulations of solar and viewing geometries throughout Thematic Mapper orbits were made. It is shown that the atmosphere plays an important role in determining Thematic Mapper radiances, with atmospheric path radiance being the major component of total radiances for short wavelengths and decreasing in importance as wavelength increases. Path radiance is shown to depend heavily on the direct radiation scattering angle and on haze content. Scan-angle-dependent variations were shown to be substantial, especially for the short-wavelength bands.

Malila, W. A.↗

CCD scanning for asteroids and comets

A change coupled device (CCD) is used in a scanning mode to find new asteroids and recover known asteroids and comet nuclei. Current scientific programs include recovery of asteroids and comet nuclei requested by the Minor Planet Center (MPC), discovery of new asteroids in the main belt and of unusual orbital types, and follow-up astrometry of selected new asteroids discovered. The routine six sigma limiting visual magnitude is 19.6 and slightly more than a square degree is scanned three times every 90 minutes of observing time during the fortnight centered on New Moon. Semiautomatic software for detection of moving objects is in routine use; angular speeds as low as 11.0 arcseconds per hour were distinguished from the effects of the Earth's atmosphere on the field of view. A typical set of three 29-minute scans near the opposition point along the ecliptic typically nets at least 5 new main-belt asteroids down to magnitude 19.6. In 18 observing runs (months) 43 asteroids were recovered, astrometric and photometric data on 59 new asteroids were reported, 10 new asteroids with orbital elements were consolidated, and photometry and positions of 22 comets were reported.

Gehrels, T.↗

Use of a scanning CCD to discriminate asteroid images moving in a field of stars

In the presently revealed use of a CCD in scanning mode to recover asteroids and comet nuclei, discover new asteroids in the main belt, and follow up the astrometry of selected new asteroids, the routine limiting visual magnitude is 19.6. Semiautomatic software for detection of moving objects is in use, allowing angular speeds as low as 11.0 arcsec/hr to be distinguished from the effects of the earth's atmosphere on the field of view. A typical set of three 29-min scans near the opposition point along the ecliptic typically nets at least five new main belt asteroids down to magnitude 19.6. In 18 monthly observing runs, 59 new asteroids have been obtained and 22 comets have been located.

Mcmillan, R. S.↗

Direct prediction of saturated neoclassical tearing modes in slab using an equilibrium approach

We demonstrate for the first time that the nonlinear saturation of neoclassical tearing modes (NTMs) can be found directly using a variational principle based on Taylor relaxation, without needing to simulate the intermediate, resistivity-dependent dynamics. As in previous investigations of classical tearing mode saturation (Loizu et al 2020 Phys. Plasmas 27 070701; Loizu and Bonfiglio 2023 J. Plasma Phys. 89 905890507), we make use of Stepped Pressure Equilibrium Code (SPEC) (Hudson et al 2012 Phys. Plasmas 19 112502), an equilibrium solver based on the variational principle of the multi-region relaxed magnetohydrodynamics (MHDs), featuring stepped pressure profiles and arbitrary magnetic topology. We work in slab geometry and employ a simple bootstrap current model J bs = C$\boldsymbol{\nabla}$p to study the bootstrap-driven tearing modes, scanning over the asymptotic matching parameter Δ' and bootstrap current strength. Saturated island widths produced by SPEC agree well with the predictions of an initial value resistive MHDs code (Huang and Bhattacharjee 2016 Astrophys. J. 818 20) while being orders of magnitude faster to calculate. Additionally, we observe good agreement with a simple analytical modified Rutherford equation, without requiring any fitting coefficients. The match is obtained for both linearly unstable classical tearing modes in the presence of bootstrap current, and NTMs, which are linearly stable but nonlinear-unstable due to the effects of the bootstrap current.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Operation of the Prototype Holographic Atmospheric Scanner for Environmental Remote Sensing (PHASERS)

This study represents the first successful employment of the Holographic Optical Telescope and Scanner (HOTS) technology to make atmospheric backscattering measurements in a scanning mode. In several independent attempts the system successfully detected the return signal from atmospheric structures as they moved across the field-of-view (FOV) of the rotating Holographic Optical Element (HOE). Future plans include the addition of a narrow band filter and the necessary optics for day-time measurements, along with additional automation of the system and its data handling. In part, due to the success of this demonstration of the HOTS technology a new class of light weight scanning telescopes for lidar remote sensing from air and space craft platforms are under development and being tested for additional applications.

Guerra, David V.↗

Undercooling minimization in ultrasound coupled DTA measurements of molten salts

Molten salts are ionic liquids that are used for the electrolytic pyroprocessing of metals and as heat transfer fluids in very high temperature processes. Recently, halide-based molten salt reactors (MSR) have gained momentum for high density and environmentally responsible electricity generation. The function of these reactors and their fuel cycle depend on a knowledge of the halide salt’s thermodynamic properties [1]. Therefore, high accuracy phase equilibria of MSR relevant base halide and actinide containing salts are needed. Modern thermal analysis of the phase transitions of halide salts is usually done during heating at relatively high scan rates with commercial devices. Normally such measurements are adequate for pure or pseudo-binary salts. However, as the number of components in the mixture increases, accurately resolving the liquidus becomes increasingly difficult. Reversing the scanning mode greatly increases the sensitivity of phase transition measurements but can decrease accuracy due to undercooling [2] — a common occurrence in molten halide systems [3]. This work presents the development of a differential thermal analysis (DTA) cell intended for use in radiological gloveboxes. Non-contact ultrasonic agitation of the halide salt is implemented to limit kinetic limitations on crystallization during cooling to minimize undercooling [4]. Measurements on halide salts are also presented to elucidate the effect of non-contact mixing on undercooling. Reference [1] S. Boyd and C. Taylor, “3 - Chemical fundamentals and applications of molten salts,” in Molten Salt Reactors and Thorium Energy, T. J. Dolan, Ed., Woodhead Publishing, 2017, pp. 29–91. doi: 10.1016/B978-0-08-101126-3.00003-8. [2] K. Nitsch, A. Cihlár, and M. Rodová, “Molten state and supercooling of lead halides,” J. Cryst. Growth, vol. 264, no. 1, pp. 492–498, Mar. 2004, doi: 10.1016/j.jcrysgro.2004.01.011. [3] L. Rycerz, “Practical remarks concerning phase diagrams determination on the basis of differential scanning calorimetry measurements,” J. Therm. Anal. Calorim., vol. 113, no. 1, pp. 231–238, Jul. 2013, doi: 10.1007/s10973-013-3097-0. [4] Md. H. Zahir, S. A. Mohamed, R. Saidur, and F. A. Al-Sulaiman, “Supercooling of phase-change materials and the techniques used to mitigate the phenomenon,” Appl. Energy, vol. 240, pp. 793–817, Apr. 2019, doi: 10.1016/j.apenergy.2019.02.045.

11 - NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

MassIVE MSV000094084 - Data files for manuscript - Selected ion monitoring for orbitrap-based metabolomics: Please open README-data-for-SIM-paper-20240210.doc for details.

Orbitrap mass spectrometry in full scan mode enables the simultaneous detection of hundreds of metabolites and their isotope-labeled forms. Yet, sensitivity remains limiting for many metabolites, including low-concentration species, poor ionizers, and low-fractional-abundance isotope-labeled forms in isotope-tracing studies. Here, we explore selected ion monitoring (SIM) as a means of sensitivity enhancement. The analytes of interest are enriched in the orbitrap analyzer by using the quadrupole as a mass filter to select particular ions. In tissue extracts, SIM significantly enhances the detection of ions of low intensity, as indicated by improved signal-to-noise (S/N) ratios and measurement precision. In addition, SIM improves the accuracy of isotope-ratio measurements. SIM, however, must be deployed with care, as excessive accumulation in the orbitrap of similar m/z ions can lead, via space-charge effects, to decreased performance (signal loss, mass shift, and ion coalescence). Ion accumulation can be controlled by adjusting settings including injection time and target ion quantity. Overall, we suggest using a full scan to ensure broad metabolic coverage, in tandem with SIM, for the accurate quantitation of targeted low-intensity ions, and provide methods deploying this approach to enhance metabolome coverage. Please open README-data-for-SIM-paper-20240210.doc for details. [doi:10.25345/C5JH3DD3K] [dataset license: CC0 1.0 Universal (CC0 1.0)]

Rabinowitz, Joshua↗

Selected Ion Monitoring for Orbitrap-Based Metabolomics

Orbitrap mass spectrometry in full scan mode enables the simultaneous detection of hundreds of metabolites and their isotope-labeled forms. Yet, sensitivity remains limiting for many metabolites, including low-concentration species, poor ionizers, and low-fractional-abundance isotope-labeled forms in isotope-tracing studies. Here, we explore selected ion monitoring (SIM) as a means of sensitivity enhancement. The analytes of interest are enriched in the orbitrap analyzer by using the quadrupole as a mass filter to select particular ions. In tissue extracts, SIM significantly enhances the detection of ions of low intensity, as indicated by improved signal-to-noise (S/N) ratios and measurement precision. In addition, SIM improves the accuracy of isotope-ratio measurements. SIM, however, must be deployed with care, as excessive accumulation in the orbitrap of similar m/z ions can lead, via space-charge effects, to decreased performance (signal loss, mass shift, and ion coalescence). Ion accumulation can be controlled by adjusting settings including injection time and target ion quantity. Overall, we suggest using a full scan to ensure broad metabolic coverage, in tandem with SIM, for the accurate quantitation of targeted low-intensity ions, and provide methods deploying this approach to enhance metabolome coverage.

59 BASIC BIOLOGICAL SCIENCES↗

Helicopter Flight Test of a Compact, Real-Time 3-D Flash Lidar for Imaging Hazardous Terrain During Planetary Landing

A second generation, compact, real-time, air-cooled 3-D imaging Flash Lidar sensor system, developed from a number of cutting-edge components from industry and NASA, is lab characterized and helicopter flight tested under the Autonomous Precision Landing and Hazard Detection and Avoidance Technology (ALHAT) project. The ALHAT project is seeking to develop a guidance, navigation, and control (GN&C) and sensing system based on lidar technology capable of enabling safe, precise crewed or robotic landings in challenging terrain on planetary bodies under any ambient lighting conditions. The Flash Lidar incorporates a 3-D imaging video camera based on Indium-Gallium-Arsenide Avalanche Photo Diode and novel micro-electronic technology for a 128 x 128 pixel array operating at a video rate of 20 Hz, a high pulse-energy 1.06 μm Neodymium-doped: Yttrium Aluminum Garnet (Nd:YAG) laser, a remote laser safety termination system, high performance transmitter and receiver optics with one and five degrees field-of-view (FOV), enhanced onboard thermal control, as well as a compact and self-contained suite of support electronics housed in a single box and built around a PC-104 architecture to enable autonomous operations. The Flash Lidar was developed and then characterized at two NASA-Langley Research Center (LaRC) outdoor laser test range facilities both statically and dynamically, integrated with other ALHAT GN&C subsystems from partner organizations, and installed onto a Bell UH-1H Iroquois "Huey" helicopter at LaRC. The integrated system was flight tested at the NASA-Kennedy Space Center (KSC) on simulated lunar approach to a custom hazard field consisting of rocks, craters, hazardous slopes, and safe-sites near the Shuttle Landing Facility runway starting at slant ranges of 750 m. In order to evaluate different methods of achieving hazard detection, the lidar, in conjunction with the ALHAT hazard detection and GN&C system, operates in both a narrow 1deg FOV raster-scanning mode in which successive, gimbaled images of the hazard field are mosaicked together as well as in a wider, 4.85deg FOV staring mode in which digital magnification, via a novel 3-D superresolution technique, is used to effectively achieve the same spatial precision attained with the more narrow FOV optics. The lidar generates calibrated and corrected 3-D range images of the hazard field in real-time and passes them to the ALHAT Hazard Detection System (HDS) which stitches the images together to generate on-the-fly Digital Elevation Maps (DEM's) and identifies hazards and safe-landing sites which the ALHAT GN&C system can then use to guide the host vehicle to a safe landing on the selected site. Results indicate that, for the KSC hazard field, the lidar operational range extends from 100m to 1.35 km for a 30 degree line-of-sight angle and a range precision as low as 8 cm which permits hazards as small as 25 cm to be identified. Based on the Flash Lidar images, the HDS correctly found and reported safe sites in near-real-time during several of the flights. A follow-on field test, planned for 2013, seeks to complete the closing of the GN&C loop for fully-autonomous operations on-board the Morpheus robotic, rocket-powered, free-flyer test bed in which the ALHAT system would scan the KSC hazard field (which was vetted during the present testing) and command the vehicle to landing on one of the selected safe sites.

Roback, VIncent E.↗

An Analysis of Input Parameters for Film-Based Flash X-Ray Radiography

Flash X-ray radiography (flash) is a commonly used diagnostic technique in dynamic experiments. An analysis of the effects of input parameters on resulting metrics of image quality can aid the experimentalist in configuring the X-ray input parameters to produce the highest quality radiograph for a given experiment. Here, a flash X-ray test bed with HS800 film and a LANEX Medium F intensifier screen was used with an L3 450 kVp pulser and Scandiflash X-ray tube for this study. Input parameters including charge voltage, source filtering, and film-pack assembly were investigated for their impact on contrast-to-noise ratio (CNR), contrast, and contrast transfer function (CTF). Using VIDAR’s NDT Pro industrial film digitizer, scanner parameters such as optical density range, pixel spacing, scan mode, and digital bit-depth were also examined for their impact on image quality metrics. The highest CNR values were found with two LANEX intensifiers and no filtering. Charge voltage had no direct impact on CNR values. LANEX screen count and filtering resulted both in direct effects on CNR and interaction effects with each other and CNR value. Uncertainty bounds for CNR comparisons and repeatability of CTF evaluations are also discussed. Finally, the film results are compared with a previous study using other detector types, specifically Carestream INDUSTREX Flex GP, Flex HR, Flex XL Blue, and HPX-DR 3543.

dynamic radiography↗

Thermomechanical Degradation of Sintered Copper Under High-Temperature Thermal Shock

The need for reliable bonded interface materials is critical to realize the performance benefits of wide-bandgap devices in power electronics modules, especially in operating temperatures greater than 150 degrees C. In this paper, we investigate the thermomechanical performance of sintered copper (Cu) as a large-area attachment, bonded between Cu baseplates and active-metal-bonded substrates, under accelerated thermal shock (-40 degrees C to 200 degrees C) conditions. In the fabrication phase of the samples, we used different stencil patterns and found that the grid and stripe patterns resulted in a better outgassing of the residual organics during the sintering process, thereby ensuring a substantially improved bond quality compared to a full-area print. The paste consisted of Cu microflakes, and we performed sintering using a Budatec SP300 sintering press at 275 degrees C with 15 MPa of bonding pressure for 5 minutes in a nitrogen atmosphere. Under accelerated experiments, we monitored the degradation of the sintered Cu bond in the samples through C-mode scanning acoustic microscope (C-SAM) images. To quantify the defect percentage in C-SAM images, we investigated image denoising techniques to exclude the pattern prints. Finally, we cross-sectioned a sample and obtained scanning electron microscope images, which revealed adhesive fracture as the dominant failure mechanism.

ADVANCED PROPULSION SYSTEMS,INORGANIC, ORGANIC, PH↗

ARM FY2025 Radar Plan

The U.S. Department of Energy (DOE) Atmospheric Radiation Measurement (ARM) user facility is dedicated to delivering high-quality radar data that significantly advance our understanding of cloud and precipitation processes, improving climate models. With radars operating across diverse frequencies, scanning modes, and global climate conditions, extensive staffing is essential for effective management. Due to current staffing constraints, achieving the expected level of operational excellence requires a more strategic approach. To address this challenge, ARM has developed an operational radar plan for the upcoming Fiscal Year 2025 (FY25) based on budget and staffing considerations.

54 ENVIRONMENTAL SCIENCES↗