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NASA NTRS1980

Diffuse X-ray emission from the jets of SS 433

The detection of large-scale diffuse X-ray jets from the variable-emission-line object SS 433 is reported. Observations were made with the high resolution imager and imaging proportional counter on board the Einstein X-ray Observatory. The two diffuse X-ray features discovered are found to be aligned with both the central source of SS 433 and with the bulges of the shell of the huge supernova remnant W 50 associated with SS 433, thus confirming the detection of jets related to SS 433 and the link between SS 433 and W 50, establishing a minimum age of 1000 years for the jet phenomenon and offering an explanation of the size of W 50. Processes by which two oppositely directed beams of material from the SS 433 source region may emit the diffuse X-rays are then considered, including shock heating by interactions with the ambient medium and synchrotron radiation. Similarities between the morphologies of the diffuse X-ray emission and those of radio galaxies are also noted.

Seward, F.↗

NASA NTRS1983

X-ray observations of 20 3CR radio galaxies and their environs

X-ray observations of 20 3CR radio galaxies using the Imaging Proportional Counter on the Einstein Observatory are reported. Fourteen of the 18 galaxies, plus two sources without optical identification, are detected with soft X-ray luminosities (Lx) ranging from 10 to the 40.9th to 10 to the 44.4th ergs/s. In four of the galaxies there is evidence for extended X-ray structure. Lx is statistically correlated with the radio power of the core, the lobe radio power (especially below 1 GHz), and the steepness of the lobe radio spectrum at high frequencies. The complex interrelations between X-ray luminosities and radio core, radio lobe, optical nuclei, and galaxy clustering are examined; and it is found that a cluster origin of the X-rays provides the best explanation of these effects. Constraints on synchrotron and inverse Compton production of X-rays in radio lobes and on mechanisms of lobe confinement are also discussed.

Feigelson, E. D.↗

NASA NTRS2001

RXTE, VLBA, Optical, and Radio Monitoring of the Quasars 3C 279, PKS 1510--089, and 3C 273

We are continuing our combined RXTE X-ray, VLBA imaging (at 43 GHz), optical (several observatories), and radio (University of Michigan Radio Astronomy Observatory) monitoring of the quasars 3C 279 and PKS 1510-089, and have started similar monitoring of 3C 273. X-ray flares in 3C 279 and PKS 1510-089 are associated with ejections of superluminal components. In addition, there is a close connection between the optical and X-ray variability of 3C 279. There is a strong correlation between the 14.5 GHz and X-ray variability of PKS 1510-089 in 1997 and 1998 (with the radio leading the X-ray) that becomes weaker in subsequent years. X-ray fluctuations occur on a variety of timescales in 3C 273, with a major prolonged outburst in mid-2001. The lead author will discuss the correlations in terms of inverse Compton models for the X-ray emission coupled with synchrotron models for the lower-frequency radiation. Synchrotron self-Compton models can explain the "reverse" time lag in PKS 1510-089 is well as the variable correlation between the X-ray variations and those at lower frequencies in this object and in 3C 279.

Marscher, A. P.↗

NASA NTRS2000

A Comparison of the Extra Nuclear X-ray and Radio Features in M87

ROSAT High Resolution Imager (HRI) data from eight observations have been co-added to obtain an effective exposure of 230 ksec. We have identified a number of features and regions with excess X-ray brightness over that from a circularly symmetric model of the well known hot gas component. A prominent 'spur' extends 4feet from the vicinity of knot A towards the south-west. The brightness to the south and east of this spur is significantly higher than that to the north and west. Excess brightness is also found to the East of the nucleus, with a local maximum centered on the eastern radio lobe 3 feet from the core. There are two well known relationships between radio and X-ray emission for radio galaxies in clusters: coincidence of emissions because the X-rays come from inverse Compton or synchrotron processes; and anti-coincidence caused by exclusion of hot gas from radio entities. We present a radio/X-ray comparison to determine if either of these relationships can be isolated in M87. The greatest obstacle we face is the unknown projection which affects both bands.

Harris, D. E.↗

NASA NTRS2006

Comparison of Spitzer/IRAC Galactic Center Mid-IR Survey Results with X-ray and Radio Emission Due to High-Energy Processes in the Central 100 Parsecs

We compare the results of a small region from our 3.6 - 8.0 micron Spitzer/IRAC imaging survey of 2 x 1.5 deg around the Galactic Center with x-ray and radio emission due to high energy processes. The region we studied covers 100 x 100 parsecs, and was chosen to include a rich collection of sources, including Sgr A* and the bright Sgr AWest infrared/radio source complex, the non-thermal radio filaments and the thermal: radio arches. In a 40 x 40 parsec subset of that region we also make a preliminary analysis of the correlation between approx.2300 x-ray sources identified by Muno et al. (2003) and 20,000 infrared sources from our survey. We also investigate the correlation between infrared and radio emission in the large-scale structures including the thermal radio arches and non-thermal radio filaments. We set constrictions on the synchrotron spectrum observed at radio and millimeter wavelengths extrapolated to 8 micons, and set limits on the midinfrared variability of Sgr A* during and after the coordinated multi-wavelength observing campaign in September 2004.

Gezari, D. Y.↗

NASA NTRS1994

Supernova remnant candidates for the soft gamma-ray repeater 1900+14

Motivated by the association of two soft gamma-ray repeaters (SGRs) with supernova remnants (SNR) we have carried out radio, optical and X-ray studies of two cataloged SNRs in the large KONUS error box 11 deg x 8 min of SGR 1900+14. Our very large array (VLA) observations of SNR G43.9+1.6 do not reveal any obvious plerionic component. A radio flat-spectrum source, close to, but outside the error box was found. We suggest this to be a distant H II region foreground to the SNR. A sensitive VLA image at meter wavelengths show that the other SNR, G42.8+0.6, is an ordinary typical SNR with a shell morphology with no peculiarities such as a plerionic component. No ROSAT source with an apparent flux greater than or approximately 10(exp -13) ergs cm(exp -2) s(exp -1) is found within the two SNRs. Recently, Hurley et al. have reported a new very small error box close to G42.8+0.6. There is no radio feature within or close to the error box. However, a ROSAT source is found just outside this localization. We speculate that this is the quiescent X-ray counterpart of SGR 1900+14. We suggest that SGR 1900+14 is a neutron star that was born with high speed which has now overtaken the expanding shell of SNR G42.8+0.6. Owing to the low confining pressure, there has been no development of a synchrotron bubble which explains the absence of the radio plerion. In our picture, SGR 1900+14 is the oldest known SGR.

Vasisht, G.↗

NASA NTRS1998

Comparison of the X-Ray and Radio Light Curves of Quasar PKS 1510--089

We present results for the X-ray-bright superluminal AGN PKS 1510-089 (z=0.36) monitored weekly with the Rossi X-Ray Timing Explorer for the past four years in order to study the origin of X-ray emission from this extremely variable blazer. These RXTE data are compared with weekly cm-band flux and polarization observations from the Michigan Diameter telescope, to identify correlated activity and associated frequency-dependent time delays for constraining X-ray emission models; and bimonthly 7mm VLBA total and linearly polarized intensity imaging to identify temporal associations between X-ray events and the ejection of superluminal components and disturbances in the magnetic field, to test if the X-ray energy release is related to changes in the inner jet flow. Both the X-ray (2-20 keV) and radio flux are highly variable on timescales of weeks. The VLBA mas structure is dominated by a bright core with a weak jet; both the ejection of very fast superluminal knots and changes in the fractional polarization and EVPA of the core on timescales of one to four months are identified. Two outbursts in 1997 are well-resolved in both the centimeter and X-ray bands. Both the strong temporal association and the similar outburst shape support a causal relation, and a discrete cross-correlation analysis identifies that the X-ray lags the radio by 16 days during the bursts. Starting in 1998 the behavior changes: the correlation is weaker with the X-ray possibly leading the radio by six days. During the full time window there is a correlation between bands as expected if the radio photons are upscattered to X-ray energies. The time correlations and difference between the flat X-ray spectral index (0.0 <= alpha <= 0.5 where F(sub v) is proportional to v(exp -alpha)), and the mm-wave synchrotron spectrum (alpha = 0.8) are discussed within the framework of viable SSC models.

Aller, M. F.↗

NASA NTRS2005

High-Resolution Electron Energy-Loss Spectroscopy (HREELS) Using a Monochromated TEM/STEM

A 200 keV FEI TF20 XT monochromated (scanning) transmission electron microscope funded by NASA's SRLIDAP program is undergoing installation at Lawrence Livermore National Laboratory. Instrument specifications in STEM mode are Cs =1.0 mm, Cc =1.2 mm, image resolution =0.18 nm, and in TEM mode Cs =1.3 mm, Cc =1.3 mm, information limit =0.14 nm. Key features of the instrument are a voltage-stabilized high tension (HT) supply, a monochromator, a high-resolution electron energy-loss spectrometer/energy filter, a high-resolution annular darkfield detector, and a solid-state x-ray energy-dispersive spectrometer. The high-tension tank contains additional sections for 60Hz and high frequency filtering, resulting in an operating voltage of 200 kV plus or minus 0.005V, a greater than 10-fold improvement over earlier systems. The monochromator is a single Wien filter design. The energy filter is a Gatan model 866 Tridiem-ERS high resolution GIF spec d for less than or equal to 0.15 eV energy resolution with 29 pA of current in a 2 nm diameter probe. 0.13 eV has already been achieved during early installation. The x-ray detector (EDAX/Genesis 4000) has a take-off angle of 20 degrees, an active area of 30 square millimeters, and a solid angle of 0.3 steradians. The higher solid angle is possible because the objective pole-piece allows the detector to be positioned as close as 9.47 mm from the specimen. The voltage-stabilized HT supply, monochromator and GIF enable high-resolution electron energy-loss spectroscopy (HREELS) with energy resolution comparable to synchrotron XANES, but with approximately 100X better spatial resolution. The region between 0 and 100 eV is called the low-loss or valence electron energy-loss spectroscopy (VEELS) region where features due to collective plasma oscillations and single electron transitions of valence electrons are observed. Most of the low-loss VEELS features we are detecting are being observed for the first time in IDPs. A major focus of our research is to understand the origin and significance of these features and how they might be exploited to gain insight about IDPs and other meteoritic materials.

Sai, Z. R.↗

NASA NTRS1994

The nature of the compact X-ray source in the supernova remnant G27.4+0.0

High-resolution X-ray imaging data obtained with ROSAT is used to constrain the nature of the central compact source in the supernova remnant G27.4+0.0. Diffuse emission is seen from throughout the approximately 4 min diameter radio shell, while the central source remains unresolved at approximately 3 sec. We combine archival data from the Einstein HRI, IPC, and MPC with the ROSAT HRI data to define the X-ray spectra of the diffuse and point-like emission. The bulk of the shell radiation is consistent with that of a approximately 10(exp 7) K plasma, although a higher temperature component is also suggested by the data; coupled with the remnant's size and distance, we derive an age of between 500 and 2500 yr. The point source has a substantially harder spectrum, with a power-law photon index less than or approximately equal to 1. A search for periodic modulation from the point source yields upper limits ranging from 10%-35% for periods between 0.025 and 1000 s, depending on the assumed pulse shape. No aperiodic variability on timescales of from 10(exp 3) to 10(exp 8) s is required, although a factor of approximately 2 change between the Einstein and ROSAT eras is possible. We show that the point source cannot represent thermal emission from the surface of a young neutron star and is unlikely to be explained as nonthermal, Crab-like X-ray pulses or a small synchrotron nebula. The most likely models involve accretion-powered systems -- either a wind-fed neutron star with a massive companion or a low-mass X-ray binary. In all probability, this is the youngest X-ray binary in the Galaxy.

Helfand, David J.↗

NASA NTRS2006

Fluorescent Applications to Crystallization

By covalently modifying a subpopulation, less than or equal to 1%, of a macromolecule with a fluorescent probe, the labeled material will add to a growing crystal as a microheterogeneous growth unit. Labeling procedures can be readily incorporated into the final stages of purification, and tests with model proteins have shown that labeling u to 5 percent of the protein molecules does not affect the X-ray data quality obtained . The presence of the trace fluorescent label gives a number of advantages. Since the label is covalently attached to the protein molecules, it "tracks" the protein s response to the crystallization conditions. The covalently attached probe will concentrate in the crystal relative to the solution, and under fluorescent illumination crystals show up as bright objects against a darker background. Non-protein structures, such as salt crystals, do not show up under fluorescent illumination. Crystals have the highest protein concentration and are readily observed against less bright precipitated phases, which under white light illumination may obscure the crystals. Automated image analysis to find crystals should be greatly facilitated, without having to first define crystallization drop boundaries as the protein or protein structures is all that shows up. Fluorescence intensity is a faster search parameter, whether visually or by automated methods, than looking for crystalline features. Preliminary tests, using model proteins, indicates that we can use high fluorescence intensity regions, in the absence of clear crystalline features or "hits", as a means for determining potential lead conditions. A working hypothesis is that more rapid amorphous precipitation kinetics may overwhelm and trap more slowly formed ordered assemblies, which subsequently show up as regions of brighter fluorescence intensity. Experiments are now being carried out to test this approach using a wider range, of proteins. The trace fluorescently labeled crystals will also emit with sufficient intensity to aid in the automation of crystal alignment using relatively low cost optics, further increasing throughput at synchrotrons.

Pusey, Marc L.↗

NASA NTRS2006

Fluorescent Approaches to High Throughput Crystallography

We have shown that by covalently modifying a subpopulation, less than or equal to 1%, of a macromolecule with a fluorescent probe, the labeled material will add to a growing crystal as a microheterogeneous growth unit. Labeling procedures can be readily incorporated into the final stages of purification, and the presence of the probe at low concentrations does not affect the X-ray data quality or the crystallization behavior. The presence of the trace fluorescent label gives a number of advantages when used with high throughput crystallizations. The covalently attached probe will concentrate in the crystal relative to the solution, and under fluorescent illumination crystals show up as bright objects against a dark background. Non-protein structures, such as salt crystals, will not incorporate the probe and will not show up under fluorescent illumination. Brightly fluorescent crystals are readily found against less bright precipitated phases, which under white light illumination may obscure the crystals. Automated image analysis to find crystals should be greatly facilitated, without having to first define crystallization drop boundaries as the protein or protein structures is all that shows up. Fluorescence intensity is a faster search parameter, whether visually or by automated methods, than looking for crystalline features. We are now testing the use of high fluorescence intensity regions, in the absence of clear crystalline features or "hits", as a means for determining potential lead conditions. A working hypothesis is that kinetics leading to non-structured phases may overwhelm and trap more slowly formed ordered assemblies, which subsequently show up as regions of brighter fluorescence intensity. Preliminary experiments with test proteins have resulted in the extraction of a number of crystallization conditions from screening outcomes based solely on the presence of bright fluorescent regions. Subsequent experiments will test this approach using a wider range of proteins. The trace fluorescently labeled crystals will also emit with sufficient intensity to aid in the automation of crystal alignment using relatively low cost optics, further increasing throughput at synchrotrons.

Pusey, Marc L.↗

NASA NTRS2005

Fluorescent Approaches to High Throughput Crystallography

X-ray crystallography remains the primary method for determining the structure of macromolecules. The first requirement is to have crystals, and obtaining them is often the rate-limiting step. The numbers of crystallization trials that are set up for any one protein for structural genomics, and the rate at which they are being set up, now overwhelm the ability for strictly human analysis of the results. Automated analysis methods are now being implemented with varying degrees of success, but these typically cannot reliably extract intermediate results. By covalently modifying a subpopulation, 51%, of a macromolecule solution with a fluorescent probe, the labeled material will add to a growing crystal as a microheterogeneous growth unit. Labeling procedures can be readily incorporated into the final stages of purification. The covalently attached probe will concentrate in the crystal relative to the solution, and under fluorescent illumination the crystals show up as bright objects against a dark background. As crystalline packing is more dense than amorphous precipitate, the fluorescence intensity can be used as a guide in distinguishing different types of precipitated phases, even in the absence of obvious crystalline features, widening the available potential lead conditions in the absence of clear hits. Non-protein structures, such as salt crystals, will not incorporate the probe and will not show up under fluorescent illumination. Also, brightly fluorescent crystals are readily found against less fluorescent precipitated phases, which under white light illumination may serve to obscure the crystals. Automated image analysis to find crystals should be greatly facilitated, without having to first define crystallization drop boundaries and by having the protein or protein structures all that show up. The trace fluorescently labeled crystals will also emit with sufficient intensity to aid in the automation of crystal alignment using relatively low cost optics, further increasing throughput at synchrotrons. This presentation will focus on the methodology for fluorescent labeling, the crystallization results, and the effects of the trace labeling on the crystal quality.

Pusey, Marc L.↗

NASA NTRS2004

Fluorescent Approaches to High Throughput Crystallography

X-ray crystallography remains the primary method for determining the structure of macromolecules. The first requirement is to have crystals, and obtaining them is often the rate-limiting step. The numbers of crystallization trials that are set up for any one protein for structural genomics, and the rate at which they are being set up, now overwhelm the ability for strictly human analysis of the results. Automated analysis methods are now being implemented with varying degrees of success, but these typically can not reliably extract intermediate results. By covalently modifying a subpopulation, less than or = 1%, of a macromolecule solution with a fluorescent probe, the labeled material will add to a growing crystal as a microheterogeneous growth unit. Labeling procedures can be readily incorporated into the final stages of purification. The covalently attached probe will concentrate in the crystal relative to the solution, and under fluorescent illumination the crystals show up as bright objects against a dark background. As crystalline packing is more dense than amorphous precipitate, the fluorescence intensity can be used as a guide in distinguishing different types of precipitated phases, even in the absence of obvious crystalline features, widening the available potential lead conditions in the absence of clear "hits." Non-protein structures, such as salt crystals, will not incorporate the probe and will not show up under fluorescent illumination. Also, brightly fluorescent crystals are readily found against less fluorescent precipitated phases, which under white light illumination may serve to obscure the crystals. Automated image analysis to find crystals should be greatly facilitated, without having to first define crystallization drop boundaries and by having the protein or protein structures all that show up. The trace fluorescently labeled crystals will also emit with sufficient intensity to aid in the automation of crystal alignment using relatively low cost optics, further increasing throughput at synchrotrons. This presentation will focus on the methodology for fluorescent labeling, the crystallization results, and the effects of the trace labeling on the crystal quality.

Pusey, Marc L.↗

NASA NTRS2004

Fluorescent Approaches to High Throughput Crystallography

X-ray crystallography remains the primary method for determining the structure of macromolecules. The first requirement is to have crystals, and obtaining them is often the rate-limiting step. The numbers of crystallization trials that are set up for any one protein for structural genomics, and the rate at which they are being set up, now overwhelm the ability for strictly human analysis of the results. Automated analysis methods are now being implemented with varying degrees of success, but these typically cannot reliably extract intermediate results. By covalently modifying a subpopulation, less than or = 1%, of a macromolecule solution with a fluorescent probe, the labeled material will add to a growing crystal as a microheterogeneous growth unit. Labeling procedures can be readily incorporated into the final stages of a macromolecules purification. The covalently attached probe will concentrate in the crystal relative to the solution, and under fluorescent illumination the crystals will show up as bright objects against a dark background. As crystalline packing is more dense than amorphous precipitate, the fluorescence intensity can be used as a guide in distinguishing different types of precipitated phases, even in the absence of obvious crystalline features, widening the available potential lead conditions in the absence of clear "bits." Non-protein structures, such as salt crystals, will not incorporate the probe and will not show up under fluorescent illumination. Also, brightly fluorescent crystals are readily found against less fluorescent precipitated phases, which under white light illumination may serve to obscure the crystals. Automated image analysis to find crystals should be greatly facilitated, without having to first define crystallization drop boundaries and by having the protein or protein structures all that show up. The trace fluorescently labeled crystals will also emit with sufficient intensity to aid in the automation of crystal alignment using relatively low cost optics, further increasing throughput at synchrotrons. This presentation will focus on the methodology for fluorescent labeling, the crystallization results, and the effects of the trace labeling on the crystal quality.

Minamitani, Elizabeth Forsythe↗

NASA NTRS1985

Einstein observations of Vela X and the Vela pulsar

The imaging detectors of the Einstein X-ray observatory have been used to study the Vela pulsar and its surrounding region. Although the pulsar is a relatively strong source of X-rays, there are not detectable pulsations at the pulsar period; the pulsed X-ray luminosity is less than approximately 10 to the 31st ergs/s in the 0.1-4.5 keV band. Nor is there evidence for other types of variability in the pulsar's X-ray emission. The images reveal structure on four spatial scales: (1) a pointlike object coincident with the pulsar; (2) a relatively bright, approximately 4-arcmin nebula of diffuse emission about the pulsar; (3) an approximately 1-degree nebula of hard emission that lies between the pulsar and the radio feature Vela X; and (4) thermal emission from the entire approximately 5-degree Vela supernova remnant. Spectral data from the small nebula are well fitted by a synchrotron model. Under the assumption that emission from the pulsar itself is thermal blackbody radiation, the surface temperature of the neutron star is calculated to be 1 million K.

Harnden, F. R., Jr.↗

NASA NTRS1994

Radio and X-ray observations of the gamma-ray bright quasar PKS 0528+134

We present a study of the z = 2.07 quasar PKS 0528+134, which has been detected as an extraordinarily luminous gamma-ray source. Its radio properties are highly variable in both total and polarized flux density. Milliarcsecond-scale maps from global very long base interferometry (VLBI) experiments, an X-ray spectrum from ROSAT Position Sensitive Proportional Counter (PSPC) observations, and light curves in total flux density and polarization are used to investigate the geometry, radiation mechanism, and physical environment of the emission region in the source. The VLBI images reveal a bent jet extending toward the northeast on parsec scales, with less intense knots of emission appearing on the opposite side of the brightest spot. The position of the core usually found in such sources is unclear. The polarization angle is stable despite strong variability in polarized flux density and indicates that the magnetic field is aligned with the jet axis as defined by our 8.4 GHz image. The ROSAT X-ray flux density of PKS 0528+134 in 1991 March is measured to be 1.6 micro Jy at 1 keV, with a very steep spectral (`energy') index sigma(sub x) approximately equal to 2.2. The X-ray observations reveal the presence of cold gas along the line of sight significantly in excess of that present in the Galaxy. A strong radio flare began within two months of the first observation of a high flux of gamma-rays from PKS 0528+134 by Hunter et al. Using the geometry and spectral chacateristics determined by our VLBI observations, a synchrotron self-Compton calculation indicates that relativistic bulk motion is required in PKS 0528+134, with an estimated Doppler beaming factor delta approximately greater than 4.3, similar to the value delta approximately greater than 7 required to explain the low optical depth of the gamma-rays to photon-photon pair production. We suggest that the core activity of PKS 0528+134 is sporadic in nature, with the nonthermal outburst starting in 1991 representing a violent period involving ejection of relativistic plasma along a compact jet pointed almost directly toward us.

Zhang, Yun Fei↗

NASA NTRS2000

High-Frequency Observations of Blazars

We report on the results of high-frequency VLBA observations of 42 gamma-ray bright blazars monitored at 22 and 43 GHz between 1993.9 and 1997.6. In 1997 the observations included polarization-sensitive imaging. The cores of gamma-ray blazars are only weakly polarized, with EVPAs (electric-vector position angles) usually within 40 deg of the local direction of the jet. The EVPAs of the jet components are usually within 20 deg of the local jet direction. The apparent speeds of the gamma-ray bright blazars are considerably faster than in the general population of bright compact radio sources. Two X-ray flares (observed with RXTE) of the quasar PKS 1510-089 appear to be related to radio flares, but with the radio leading the X-ray variations by about 2 weeks. This can be explained either by synchrotron self-Compton emission in a component whose variations are limited by light travel time or by the Mirror Compton model.

Marscher, A. P.↗

NASA NTRS2000

High-Frequency Observations of Blazars

We report on the results of high-frequency VLBA observations of 42 gamma ray bright blazars monitored at 22 and 43 GHz between 1993.9 and 1997-6. In 1997 the observations included polarization-sensitive imaging. The cores of gamma ray blazars are only weakly polarized, with EVPAs (electric-vector position angles) usually within 40 degrees of the local direction of the jet. The EVPAs of the jet components are usually within 20 degrees of the local jet direction. The apparent speeds of the gamma ray bright blazars are considerably faster than in the general population of bright compact radio sources. Two X-ray flares (observed with RXTE) of the quasar PKS 1510-089 appear to be related to radio flares, but with the radio leading the X-ray variations by about 2 weeks. This can be explained either by synchrotron self-Compton emission in a component whose variations are limited by light travel time or by the Mirror Compton model.

Marscher, A. P.↗