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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 55 records · Page 3

Annealing effects in plated-wire memory elements. I - Interdiffusion of copper and Permalloy.

Results of investigations using X-ray diffraction and electron-beam microprobe techniques have shown that copper and Permalloy platings interdiffuse at low temperatures when plated-wire memory elements are annealed for times as short as 50 hr. Measurable interdiffusion between Permalloy platings and gold substrates does not occur in similar conditions. Both magnetic and compositional changes during aging are found to occur by a thermally activated process with activation energies around 38 kcal/mol. It is shown, however, that copper-diffusion and magnetic-dispersion changes during aging are merely concurrent processes, neither being the other's cause.

Knudson, C. I.↗

Noncontacting measuring device to indicate deflection of turbopump internal rotating parts

Noncontacting, nondestructive techniques to measure vibrations and deflections of parts in future LOX and LH2 multistage turbopump prototypes are reported. The measurements include shaft vibration, vibration of turbine wheel and blades, blade clearance, vibration of impellers, value component flutter, and vibration of face seal components. Three techniques were selected for development: ultrasonic Doppler devices, flash X-ray, and light-pipe reflectance.

Hamilton, D. B.↗

Incipient failure detection.

In connection with the preparation for long-range space missions it is highly important to be able to identify potentially failure prone equipment in advance of the launch commitment. Physical phenomena investigated for this purpose include X-ray and gamma radiation, electrical noise, IR and UV radiation, and vibration energy. The technique selected must be capable of detecting the onset and evaluating the progression of conditions that represent basic causes which could lead to failure. As a result of the investigation, techniques based on acoustic energy release were selected as the most promising for incipient failure detection.

Griswold, J. W.↗

New techniques in geochemical analysis

Thin layer and gas chromatography, Mossbauer and atomic absorption spectrometry, fission track analysis, X-ray fluorescence spectroscopy, and other methods employed in geochemistry

X-RAY FLUORESCENCE SPECTROSCOPY↗

Stress corrosion in titanium alloys and other metallic materials

Multiple physical and chemical techniques including mass spectroscopy, atomic absorption spectroscopy, gas chromatography, electron microscopy, optical microscopy, electronic spectroscopy for chemical analysis (ESCA), infrared spectroscopy, nuclear magnetic resonance (NMR), X-ray analysis, conductivity, and isotopic labeling were used in investigating the atomic interactions between organic environments and titanium and titanium oxide surfaces. Key anhydrous environments studied included alcohols, which contain hydrogen; carbon tetrachloride, which does not contain hydrogen; and mixtures of alcohols and halocarbons. Effects of dissolved salts in alcohols were also studied. This program emphasized experiments designed to delineate the conditions necessary rather than sufficient for initiation processes and for propagation processes in Ti SCC.

Harkins, C. G.↗

Apollo 6, Anomaly Report No. 6: Abnormal Structural Performance During Launch Phase

Approximately 2 minutes 13 seconds after lift-off of the Apollo 6 mission, abrupt changes of strain, vibration, and acceleration measurements were indicated in the S-IVB, instrument unit, adapter, lunar module, and command and service modules; photographs showed objects coming from the area of the adapter. The adapter, however, continued to sustain the required loads with no impairment of the mission. The investigation was first focused upon the understanding of the coupled vibration modes and characteristics of the launch vehicle and spacecraft.' Extensive test programs were conducted. It was eventually concluded that the adapter failure was not caused by vibration. Extensive study of the airborne photography and other evidence indicated that a large area of the adapter had lost inner facesheet from the honeycomb sandwich panels. Loads and stresses resulting from vibration were determined to be insufficient to initiate such a failure. The investigation was then directed toward determining the range of pressures that could have been trapped in the Apollo 6 adapter sandwich panels, and toward determining the tolerance of the panels to withstand pressure with various degrees of flaws such as adhesive voids and facesheet dents. The degradation effects of moisture and heat exposure on the adhesive strength were also studied and tested. These tests and analyses led to the conclusion that pressure internal to the sandwich panels could have caused the failure, if a large flaw existed. The pressure buildup would have been caused by aerodynamic heating effects on air and moisture trapped in the panel. The probable cause of the failure was found in the original ultrasonic inspection scan record of the affected adapter panel. In the center of the region where the adapter failed, horizontally along the station 709 panel splice, the record contained two thick anomalous lines extending several feet. Without an X-ray record of this region, the significance of this particular scan record cannot be fully understood. However, since all other evidence had indicated that the adhesive had to be weakened in a rather large area to initiate the failure, the investigation was focused intently upon the station 709 splices of other adapters. Sufficient information was developed to verify that deficient assembly techniques have consistently resulted in abnormalities in the structure at this station. These abnormalities were identified in adapters 12, 13, 14, 15, and 16. Before the splice abnormalities were pinpointed, corrective action was taken to reduce pressure "buildup in the honeycomb panels and to reduce heat degrading effects on the adhesive. This was done by drilling vent holes in the inner facesheet and covering the outer facesheet with cork. The adapters having identified abnormalities in the station 709 splice are being repaired, and the contractor is investigating ways of avoiding these -abnormalities in panels yet to be bonded.

Source record↗

Thermal Inspection for the Assessment of Adhesively Bonded Metal Adherends

Certification of adhesively bonded structures is currently a challenge for aircraft manufacturers. The ability to certify bonds in primary structure can reduce dependence on fasteners and this will enable more efficient manufacturing. For example, drilling holes and installing fasteners in bonded joints can be a potentially significant bottleneck in airframe manufacturing. In addition, fasteners increase the airframe weight and can add stress concentration areas. Reducing fastener count can accelerate manufacturing and improve aircraft performance. NASA is currently investigating nondestructive evaluation (NDE) techniques to assess bond integrity. For example, bond thickness influences bond strength and therefore NDE techniques are being investigated to determine bond thickness. For bonded metal structures, there is a large difference in the thermal diffusivity between the 7075 aluminum alloy metal adherends and aircraft grade adhesive. Multi-layered thermal models show a large variation in the thermal response for bondline adhesive thicknesses that vary from 100 to 300 microns for adherend thicknesses of 0.163 cm. Experimental through-transmission thermal measurements reveal promise to quantitatively characterize the bondline thickness. Results were validated with X-ray computed tomography and optical microscopy measurements, and influence of porosity on the thermal model and measurements are investigated.

X-ray computed tomography↗

Thermal Inspection for the Assessment of Adhesively Bonded Metal Adherents

Certification of adhesively bonded structures is currently a challenge for aircraft manufacturers. The ability to certify bonds in primary structure can reduce dependence on fasteners and this will enable more efficient manufacturing. For example, drilling holes and installing fasteners in bonded joints can be a potentially significant bottleneck in airframe manufacturing. In addition, fasteners increase the airframe weight and can add stress concentration areas. Reducing fastener count can accelerate manufacturing and improve aircraft performance. NASA is currently investigating nondestructive evaluation (NDE) techniques to assess bond integrity. For example, bond thickness influences bond strength and therefore NDE techniques are being investigated to determine bond thickness. For bonded metal structures, there is a large difference in the thermal diffusivity between the 7075 aluminum alloy metal adherends and aircraft grade adhesive. Multi-layered thermal models show a large variation in the thermal response for bondline adhesive thicknesses that vary from 100 to 300 microns for adherend thicknesses of 0.163 cm. Experimental through-transmission thermal measurements reveal promise to quantitatively characterize the bondline thickness. Results were validated with X-ray computed tomography and optical microscopy measurements, and influence of porosity on the thermal model and measurements are investigated.

bondline thickness↗

X-ray analysis of fatigue damage in copper

A Warren-Averbach x-ray line profile analysis was applied to, broadened x-ray diffraction peaks from copper deformed in fatigue. The copper specimens were fatigued by four point bending at various strain amplitudes, and measurements were made at various fractions of the total fatigue life. The analysis results in an estimation of 1) an average coherently diffracting domain size in a direction normal to the diffracting planes; and 2) a strain distribution function. The strain distribution function is in terms of the root mean square strain, <ϵ^(2)> where ϵ is averaged over a given distance at all points in the diffracting crystals. This rms strain is expressed as a function of averaging distance for a direction normal to the diffracting planes. The rms strains were found to be a function of the fatigue strain amplitude level, increasing with amplitude and reaching a maximum limiting value during the first 2% of the fatigue life. The strains were normally larger in the 4lO0 direction compared to the <111> direction and the absolute values were quite small. These results may be explained by assuming the dislocations are present in the form of dipoles because the lattice strain around a dipole is much less than around single dislocations. Conclusions arrived at in this analysis are in agreement with current theories of fatigue damage in metals. The result that maximum hardening is achieved during the initial few percent of the fatigue life is confirmed by many other investigators using entirely different analytical techniques. It is felt that the structure of the material is changing during this initial hardening stage to an eventual steady state characteristic of the testing conditions. A unique substructure is developed which thereafter persists, and the remainder of the fatigue test is taken up by crack propagation through this substructure until ultimate failure occurs by fracture. The formation of this steady state structure is dependent on the maximum fatigue strain amplitude and on the frequency and temperature of cycling for a particular material.

COPPER↗

Residual Stress Analysis of Overspeeded Disk with Central Hole by X-ray Diffraction

An X-ray - diffraction analysis of residual surface stresses after plastic strain was introduced in a parallel-sided 3S-O aluminum disk with a central hole by two types of centrifugal overspeed is reported. Both tangential and radial stresses were generally tensile with large local variations near the hole where surface stresses may have been partly superficial. These stresses were both tensile and compressive dependent on the distance from the disk center when mass compression was effected near the hole.

ALUMINUM↗

X-ray film holder permits single continuous picture of tubing joint

X ray technique produces a clear continuous picture of a welded brazed tubing joint on a single film with one exposure. A stationary X ray source located in the plane of the joint to be inspected, a means of rotating the tube, and a unique internal film holder and positioning fixture are used.

Diamond, J. W.↗