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At least 541 records · Page 30

Report of METL Mutual Inductance Level Sensor Development for Use in Liquid Metals – FY2023

A robust mutual inductance level sensor (MILS) for use in high temperature liquid metals has been developed at Argonne National Laboratory (ANL). The current design utilizes mineral insulated cables with a 300-series stainless steel sheath, magnesium oxide insulation, and a single copper conductor. Two coils are wrapped on a common core made of a 300-series stainless steel tube. One coil is energized with an alternating current (AC) source, and this electromagnetically couples with the second coil to generate an induced voltage. The voltage is measured to determine the mutual induction between the coils, and the mutual inductance measurement can be used to determine the level of a nearby liquid metal volume. The MILS can be located in an isolating thimble that is fully sealed to a vessel containing liquid metal for ease of maintenance and replacement. When the primary coil is energized with the AC source, the coil not only electromagnetic (EM) couples with the second coil, but also the surrounding liquid metal. The EM coupling with the surrounding liquid metal reduces the EM coupling with the second coil, producing an inverse-linear relationship between liquid metal level and secondary coil voltage. This has all been demonstrated at the Mechanisms Engineering Test Loop (METL) liquid sodium facility at ANL. The most current iteration of the MILS system is the MILS-MK-II. This sensor system has been commissioned in a non-sodium test stand where calibrations were performed using a sodium analog. The calibrations proved to be highly linear and repeatable. The MILS-MK-II has been installed in the METL expansion tank where high temperature sodium tests have been performed. The MILS-MK-II has been calibrated against a known standard at temperature of 300°C, and the calibrations have proved to be highly linear and repeatable. The calibrated MILS-MK-II has been in operation in the METL facility for several thousands of hours at temperatures around 300°C. The experimental data has been used to develop and validate electromagnetic finite element models in COMSOL Multiphysics, and now these models can be used to advance the development of the sensor system. Next steps will include temperature compensation to allow for operation at various temperatures. Additionally, efforts to incorporate a self-calibration methodology are underway.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Digital Signal Processing Techniques for the GIFTS SM EDU

The Geosynchronous Imaging Fourier Transform Spectrometer (GIFTS) Sensor Module (SM) Engineering Demonstration Unit (EDU) is a high resolution spectral imager designed to measure infrared (IR) radiance using a Fourier transform spectrometer (FTS). The GIFTS instrument employs three Focal Plane Arrays (FPAs), which gather measurements across the long-wave IR (LWIR), short/mid-wave IR (SMWIR), and visible spectral bands. The raw interferogram measurements are radiometrically and spectrally calibrated to produce radiance spectra, which are further processed to obtain atmospheric profiles via retrieval algorithms. This paper describes several digital signal processing (DSP) techniques involved in the development of the calibration model. In the first stage, the measured raw interferograms must undergo a series of processing steps that include filtering, decimation, and detector nonlinearity correction. The digital filtering is achieved by employing a linear-phase even-length FIR complex filter that is designed based on the optimum equiripple criteria. Next, the detector nonlinearity effect is compensated for using a set of pre-determined detector response characteristics. In the next stage, a phase correction algorithm is applied to the decimated interferograms. This is accomplished by first estimating the phase function from the spectral phase response of the windowed interferogram, and then correcting the entire interferogram based on the estimated phase function. In the calibration stage, we first compute the spectral responsivity based on the previous results and the ideal Planck blackbody spectra at the given temperatures, from which, the calibrated ambient blackbody (ABB), hot blackbody (HBB), and scene spectra can be obtained. In the post-calibration stage, we estimate the Noise Equivalent Spectral Radiance (NESR) from the calibrated ABB and HBB spectra. The NESR is generally considered as a measure of the instrument noise performance, and can be estimated as the standard deviation of calibrated radiance spectra from multiple scans. To obtain an estimate of the FPA performance, we developed an efficient method of generating pixel performance assessments. In addition, a random pixel selection scheme is developed based on the pixel performance evaluation. This would allow us to perform the calibration procedures on a random pixel population that is a good statistical representation of the entire FPA. The design and implementation of each individual component will be discussed in details.

Tian, Jialin↗

Langley Automated Sensor Inter-calibration System (LASICS): Open Access Tools for Satellite Imager Inter- Calibration

Satellite imager calibration teams are tasked with maintaining stable measurement records to facilitate reliable monitoring of geophysical parameters and ensure dependable input for forecast models. Satellite imagers are neither uniformly calibrated nor radiometrically scaled to a common reference standard. Consistent inter-calibration between various earth-orbiting satellite imager pairs is a critical step in the creation of seamless earth-scene reflectance data records over time for input to higher level algorithms that retrieve earth system climate-sensitive properties. Each imager inherently by virtue of its optics (and associated properties like spectral response etc.) and orbit will have a unique measurement of the same earth-scene reflected signal. A key part of this is the computationally efficient and optimal identification and prediction of science opportunities where the imager pairs from the irrespective earth-orbits near-simultaneously view the same stable terrestrial targets with nearly identical viewing and solar geometry.

Arun Gopalan↗

True coincidence summing corrections for an extended energy range HPGe detector

True coincidence summing (TCS) effect for natural radioactive families of U-238 and Th-232 represents a problem when an environmental sample with a close source-detector geometry measurement is performed. By using a certified multi-nuclide standard source to calibrate an energy extended range (XtRa) HPGe detector, it is possible to obtain an intensity spectrum slightly affected by the TCS effect with energies from 46 to 1836 keV. In this work, the equations and some other considerations required to calculate the TCS correction factor for isotopes of natural radioactive chains are described. It is projected a validation of the calibration, performed with the IAEA-CU-2006-03 samples (soil and water)

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

ARCSTONE: Calibration of Lunar Spectral Reflectance from Space

Detecting and improving the scientific understanding of global trends in complex Earth systems, such as climate, increasingly depends on assimilating datasets from multiple instruments and platforms over decadal timescales. Calibration accuracy, stability, and inter-consistency among different instruments are key to developing reliable composite data records from sensors in low Earth and geostationary orbits, but achieving sufficiently low uncertainties for these performance metrics poses a significant challenge. Space-borne instruments commonly carry on-board references for calibration at various wavelengths, but these increase mass and mission complexity, and are subject to degradation in the space environment. The Moon can be considered a natural solar diffuser which can be observed as a calibration target by most spaceborne Earth-observing instruments. Since the lunar surface reflectance is effectively time-invariant, establishing the Moon as a high-accuracy calibration reference enables broad inter-calibration opportunities even between temporally non-overlapping instruments and provides an exo-atmospheric absolute radiometric standard. The ARCSTONE mission goal is to establish the Moon as a reliable reference for high-accuracy on-orbit calibration in the visible and near-infrared spectral region. The ARCSTONE instrument is a compact spectrometer, which will be packaged on a CubeSat intended for low Earth orbit. It will measure the lunar spectral reflectance with accuracy < 0.5% (k=1), sufficient to establish an SI-traceable absolute lunar calibration standard when referenced to the spectral solar irradiance across the 350 to 2300 nm spectral range. This lunar reference will help to enable high-accuracy absolute calibration and inter-calibration of past, current, and future Earth-observing sensors, meteorological imagers, and long-term climate monitoring satellite systems. The ARCSTONE team will present the development status of a full-spectral-range (FSR) instrument, the intended approach to calibration and characterization, and the planned path toward mission implementation.

calibration↗

ARCSTONE: Calibration of Lunar Spectral Reflectance from Space

Detecting and improving the scientific understanding of global trends in complex Earth systems, such as climate, increasingly depends on assimilating datasets from multiple instruments and platforms over decadal timescales. Calibration accuracy, stability, and inter-consistency among different instruments are key to developing reliable composite data records from sensors in low Earth and geostationary orbits, but achieving sufficiently low uncertainties for these performance metrics poses a significant challenge. Space-borne instruments commonly carry on-board references for calibration at various wavelengths, but these increase mass and mission complexity, and are subject to degradation in the space environment. The Moon can be considered a natural solar diffuser which can be observed as a calibration target by most spaceborne Earth-observing instruments. Since the lunar surface reflectance is effectively time-invariant, establishing the Moon as a high-accuracy calibration reference enables broad inter-calibration opportunities even between temporally non-overlapping instruments and provides an exo-atmospheric absolute radiometric standard. The ARCSTONE mission goal is to establish the Moon as a reliable reference for high-accuracy on-orbit calibration in the visible and near-infrared spectral region. The ARCSTONE instrument is a compact spectrometer, which will be packaged on a CubeSat intended for low Earth orbit. It will measure the lunar spectral reflectance with accuracy < 0.5% (k=1), sufficient to establish an SI-traceable absolute lunar calibration standard when referenced to the spectral solar irradiance across the 350 to 2300 nm spectral range. This lunar reference will help to enable high-accuracy absolute calibration and inter-calibration of past, current, and future Earth-observing sensors, meteorological imagers, and long-term climate monitoring satellite systems. The ARCSTONE team will present the development status of a full-spectral-range (FSR) instrument, the intended approach to calibration and characterization, and the planned path toward mission implementation.

Moon↗

FTS maintenance and calibration at DSS 42/43

An FTS maintenance and calibration task was conducted at DSS 42/43 during August 1978. The objectives of this effort were (1) the routine maintenance and calibration of hydrogen masers, (2) installation and calibration of cesium standards, (3) installation of test equipment for frequency measurement, (4) CRG testing, (5) cabling inspection and repair, (6) check thermal and magnetic environment of H-maser/cesium room, and (7) calibration of frequency and timing subsystem.

Dachel, P. R.↗

WM-SVS-TP-003, Rev. 0, effective date 10/15/2015, WM-SVS Characterization Services User-Performed Calibration (UPC) Program

Los Alamos National Laboratory (LANL) Procedure P330-2, Control and Calibration of Measuring and Test Equipment (M&TE), requires the establishment of a Measurement Assurance Program and/or a User-Performed Calibration (UPC) Process, as applicable. This UPC has been developed in accordance with the authorization provided in QPA-VAR-2013. This program ensures that qualified individuals perform measurement control and develop measurement control and calibration procedures. Nondestructive analysis (NDA) instruments used for accountability, confirmation, and verification measurements are maintained by the Waste Management Services (WM-SVS) Characterization Services Team. NDA reference standards used for instrument control and calibration are certified for use by the Standards and Calibration Laboratory (S&CL) before use. The Characterization Services Team performs the measurements, develops procedures for performing instrument UPC, and ensures the measurement systems’ control before measurements are performed.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

SU-F-J-52: A Novel Approach to X-Ray Tube Quality Assurance for CBCT Systems in Order to Better Assess the Patient Imaging Dose in a Large, Multi-Unit Treatment Facility

Purpose: To standardize the tube calibration for Elekta XVI cone beam CT (CBCT) systems in order to provide a meaningful estimate of the daily imaging dose and reduce the variation between units in a large centre with multiple treatment units. Methods: Initial measurements of the output from the CBCT systems were made using a Farmer chamber and standard CTDI phantom. The correlation between the measured CTDI and the tube current was confirmed using an Unfors Xi detector which was then used to perform a tube current calibration on each unit. Results: Initial measurements showed measured tube current variations of up to 25% between units for scans with the same image settings. In order to reasonably estimate the imaging dose, a systematic approach to x-ray generator calibration was adopted to ensure that the imaging dose was consistent across all units at the centre and was adopted as part of the routine quality assurance program. Subsequent measurements show that the variation in measured dose across nine units is on the order of 5%. Conclusion: Increasingly, patients receiving radiation therapy have extended life expectancies and therefore the cumulative dose from daily imaging should not be ignored. In theory, an estimate of imaging dose can be made from the imaging parameters. However, measurements have shown that there are large differences in the x-ray generator calibration as installed at the clinic. Current protocols recommend routine checks of dose to ensure constancy. The present study suggests that in addition to constancy checks on a single machine, a tube current calibration should be performed on every unit to ensure agreement across multiple machines. This is crucial at a large centre with multiple units in order to provide physicians with a meaningful estimate of the daily imaging dose.

60 APPLIED LIFE SCIENCES↗

Spectral irradiance standard for the ultraviolet - The deuterium lamp

A set of deuterium lamps is calibrated as spectral irradiance standards in the 200-350-nm spectral region utilizing both a high accuracy tungsten spectral irradiance standard and a newly developed argon mini-arc spectral radiance standard. The method which enables a transfer from a spectral radiance to a spectral irradiance standard is described. The following characteristics of the deuterium lamp irradiance standard are determined: sensitivity to alignment; dependence on input power and solid angle; reproducibility; and stability. The absolute spectral radiance is also measured in the 167-330-nm region. Based upon these measurements, values of the spectral irradiance below 200 nm are obtained through extrapolation.

Saunders, R. D.↗

Satellite measurements of the backscattered ultraviolet to determine ozone trends, volcanic SO2, and nitric oxide

Measurements of the atmospheric backscattered UV albedo have been used from satellites for more than 20 years to measure ozone. The longest continuous record has been from the Solar Backscattered Ultraviolet instrument (SBUV) and TOMS on the Nimbus 7 satellite, which have been in operation since November of 1978. Because of degradation in space of the diffuser plate used to measure extraterrestrial solar flux, it has been necessary to develop new techniques to maintain the calibration of these instruments. Calibration is maintained by requiring that ozone measured by different wavelength pairs be consistent, and by requiring that ozone measured at different solar zenith angles be consistent. This technique of using a geophysical quantity, ozone, as a transfer standard for wavelength calibration is very powerful. The recalibrated data have been used to measure total ozone trends to an accuracy of +/- 1.3 percent 2(sigma) error over ten years. No significant trends are found near the equator, but significant trends larger than predicted by homogeneous chemistry are found at middle to high latitudes in both hemispheres. In addition, UV albedo data have been used to measure SO2 using band structure in the 300-310 nm range, and to measure nitric oxide in the upper stratosphere and mesosphere using the (10) and (02) NO gamma band fluorescence features.

Mcpeters, Richard↗

Satellite Instrument Calibration for Measuring Global Climate Change. Report of a Workshop at the University of Maryland Inn and Conference Center, College Park, MD. , November 12-14, 2002

Measuring the small changes associated with long-term global climate change from space is a daunting task. To address these problems and recommend directions for improvements in satellite instrument calibration some 75 scientists, including researchers who develop and analyze long-term data sets from satellites, experts in the field of satellite instrument calibration, and physicists working on state of the art calibration sources and standards met November 12 - 14, 2002 and discussed the issues. The workshop defined the absolute accuracies and long-term stabilities of global climate data sets that are needed to detect expected trends, translated these data set accuracies and stabilities to required satellite instrument accuracies and stabilities, and evaluated the ability of current observing systems to meet these requirements. The workshop's recommendations include a set of basic axioms or overarching principles that must guide high quality climate observations in general, and a roadmap for improving satellite instrument characterization, calibration, inter-calibration, and associated activities to meet the challenge of measuring global climate change. It is also recommended that a follow-up workshop be conducted to discuss implementation of the roadmap developed at this workshop.

NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY (NI↗

Bayesian Model Calibration for Extrapolative Prediction via Gibbs Posteriors

The current standard Bayesian approach to model calibration, which assigns a Gaussian process prior to the discrepancy term, often suffers from issues of unidentifiability and computational complexity and instability. When the goal is to quantify uncertainty in physical parameters for extrapolative prediction, then there is no need to perform inference on the discrepancy term. With this in mind, we introduce Gibbs posteriors as an alternative Bayesian method for model calibration, which updates the prior with a loss function connecting the data to the parameter. The target of inference is the physical parameter value which minimizes the expected loss. We propose to tune the loss scale of the Gibbs posterior to maintain nominal frequentist coverage under assumptions of the form of model discrepancy, and present a bootstrap implementation for approximating coverage rates. Our approach is highly modular, allowing an analyst to easily encode a wide variety of such assumptions. Furthermore, we provide a principled method of combining posteriors calculated from data subsets. We apply our methods to data from an experiment measuring the material properties of tantalum.

36 MATERIALS SCIENCE↗

Low Differential Pressure Generator

A method and apparatus for evaluating low differential pressure transducers includes a pressure generator in the form of a piston-cylinder assembly having a piston that may be manually positioned precisely within the cylinder to change the volume and thus the pressure at respective sides of the piston. At one side of the piston the cylinder communicates with a first chamber and at the other side of the piston the cylinder communicates with a second chamber, the first and second chambers being formed within a common tank by a partition wall. The chambers each communicate with the transducer to be evaluated and a standard pre-calibrated transducer the transducers being connected fluidly in parallel so that a pressure differential between air in the two chambers resulting from movement of the piston within the cylinder is communicated to both the transducer to be evaluated and the standard transducer, and the outputs of the transducers is observed and recorded.

Stout, Stephen J.↗

Theory of wide-angle photometry from standard stars

Wide angle celestial structures, such as bright comet tails and nearby galaxies and clusters of galaxies, rely on photographic methods for quantified morphology and photometry, primarily because electronic devices with comparable resolution and sky coverage are beyond current technological capability. The problem of the photometry of extended structures and of how this problem may be overcome through calibration by photometric standard stars is examined. The perfect properties of the ideal field of view are stated in the guise of a radiometric paraxial approximation, in the hope that fields of view of actual telescopes will conform. Fundamental radiometric concepts are worked through before the issue of atmospheric attenuation is addressed. The independence of observed atmospheric extinction and surface brightness leads off the quest for formal solutions to the problem of surface photometry. Methods and problems of solution are discussed. The spectre is confronted in the spirit of standard stars and shown to be chimerical in that light, provided certain rituals are adopted. After a brief discussion of Baker-Sampson polynomials and the vexing issue of saturation, a pursuit is made of actual numbers to be expected in real cases. While the numbers crunched are gathered ex nihilo, they demonstrate the feasibility of Newton's method in the solution of this overdetermined, nonlinear, least square, multiparametric, photometric problem.

Usher, Peter D.↗