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NASA NTRS2008

Smaller, Lower-Power Fast-Neutron Scintillation Detectors

Scintillation-based fast-neutron detectors that are smaller and less power-hungry than mainstream scintillation-based fast-neutron detectors are undergoing development. There are numerous applications for such detectors in monitoring fast-neutron fluxes from nuclear reactors, nuclear materials, and natural sources, both on Earth and in outer space. A particularly important terrestrial application for small, low-power, portable fast-neutron detectors lies in the requirement to scan for nuclear materials in cargo and baggage arriving at international transportation facilities. The present development of miniature, low-power scintillation-based fast-neutron detectors exploits recent advances in the fabrication of avalanche photodiodes (APDs). Basically, such a detector includes a plastic scintillator, typically between 300 and 400 m thick with very thin silver mirror coating on all its faces except the one bonded to an APD. All photons generated from scintillation are thus internally reflected and eventually directed to the APD. This design affords not only compactness but also tight optical coupling for utilization of a relatively large proportion of the scintillation light. The combination of this tight coupling and the avalanche-multiplication gain (typically between 750 and 1,000) of the APD is expected to have enough sensitivity to enable monitoring of a fast-neutron flux as small as 1,000 cm(exp -2)s(exp -1). Moreover, pulse-height analysis can be expected to provide information on the kinetic energies of incident neutrons. It has been estimated that a complete, fully developed fast-neutron detector of this type, would be characterized by linear dimensions of the order of 10 cm or less, a mass of no more than about 0.5 kg, and a power demand of no more than a few watts.

Patel, Jagdish↗

NASA NTRS2013

Advanced Materials and Manufacturing for Low-Cost, High-Performance Liquid Rocket Combustion Chambers

A document describes the low-cost manufacturing of C103 niobium alloy combustion chambers, and the use of a high-temperature, oxidation-resistant coating that is superior to the standard silicide coating. The manufacturing process involved low-temperature spray deposition of C103 on removable plastic mandrels produced by rapid prototyping. Thin, vapor-deposited platinum-indium coatings were shown to substantially improve oxidation resistance relative to the standard silicide coating. Development of different low-cost plastic thrust chamber mandrel materials and prototyping processes (selective laser sintering and stereolithography) yielded mandrels with good dimensional accuracy (within a couple of mils) for this stage of development. The feasibility of using the kinetic metallization cold-spray process for fabrication of free-standing C1O3 thrusters on removable plastic mandrels was also demonstrated. The ambient and elevated temperature mechanical properties of the material were shown to be reasonably good relative to conventionally processed C103, but the greatest potential benefit is that coldsprayed chambers require minimal post-process machining, resulting in substantially lower machining and material costs. The platinum-iridium coating was shown to provide greatly increased oxidation resistance over the silicide when evaluated through oxyacetylene torch testing to as high as 300 F (= 150 C). The iridium component minimizes reaction with the niobium alloy chamber at high temperatures, and provides the high-temperature oxidation resistance needed at the throat.

Williams, Brian E.↗

NASA NTRS2019

Heat Transfer Enhancement in Cryogenic Quenching Process

This paper reports a heat transfer advancement in the cryogenic quenching process. An experiment was performed to evaluate the enhancement of quenching heat transfer by the use of metal tubes with low thermal conductivity coating layers. Four coating thicknesses with various coolant mass flow rates of liquid nitrogen were investigated. The results indicated that the tube inner surface coating greatly enhanced the quenching efficiency. The quenching efficiency was found to increase with increasing number of coating layers, and the efficiency also increased with decreasing mass flow rates. In general, the efficiencies cover a range between 40.6% and 80%. Comparing to the bare surface case, the percentage increase in the quenching efficiency was the minimum at 4.2% for a single coated layer at the highest flow rate and the maximum of 109.1% for four coated layers at the lowest flow rate. The coated tubes could save up to 53% in the amount of cryogen consumption.

Surface coating↗

NASA NTRS2016

ASTM Committee C28: International Standards for Properties and Performance of Advanced Ceramics, Three Decades of High-quality, Technically-rigorous Normalization

Physical and mechanical properties and performance of advanced ceramics and glasses are difficult to measure correctly without the proper techniques. For over three decades, ASTM Committee C28 on Advanced Ceramics, has developed high quality, rigorous, full-consensus standards (e.g., test methods, practices, guides, terminology) to measure properties and performance of monolithic and composite ceramics that may be applied to glasses in some cases. These standards testing particulars for many mechanical, physical, thermal, properties and performance of these materials. As a result these standards provide accurate, reliable, repeatable and complete data. Within Committee C28 users, producers, researchers, designers, academicians, etc. have written, continually updated, and validated through round-robin test programs, nearly 50 standards since the Committees founding in 1986. This paper provides a retrospective review of the 30 years of ASTM Committee C28 including a graphical pictogram listing of C28 standards along with examples of the tangible benefits of advanced ceramics standards to demonstrate their practical applications.

properties↗

NASA NTRS1984

Advanced thin film thermocouples

The fabrication, materials characterization, and performance of thin film platinum rhodium thermocouples on gas turbine alloys was investigated. The materials chosen for the study were the turbine blade alloy systems MAR M200+Hf with NiCoCrAlY and FeCrAlY coatings, and vane alloy systems MAR M509 with FeCrAlY. Research was focussed on making improvements in the problem areas of coating substrate stability, adhesion, and insulation reliability and durability. Diffusion profiles between the substrate and coating with and without barrier coatings of Al2O3 are reported. The relationships between fabrication parameters of thermal oxidation and sputtering of the insulator and its characterization and performance are described. The best thin film thermocouples were fabricated with the NiCoCrAlY coatings which were thermally oxidized and sputter coated with Al2O3.

Kreider, K. G.↗

NASA NTRS1979

Space optics: Imaging X-ray optics workshop; Proceedings of the Seminar, Huntsville, Ala., May 22-24, 1979

The papers in this volume are broadly based and represent a comprehensive summary of past achievements, new designs, techniques and future plans in space optics. The design, construction, testing and use of grazing incidence optics have played an integral role in the advance of X-ray astronomy. Topics of interest include a cosmic X-ray telescope for ARIES rocket observations, quest for ultrahigh resolution in X-ray optics, optical coating techniques for Wolter-type substrates, astronomical applications of grazing incidence telescopes with polynomial surfaces, and a paraboloidal X-ray telescope mirror for solar coronal spectroscopy.

Weisskopf, M.↗

NASA NTRS1986

Research relative to high resolution camera on the advanced X-ray astrophysics facility

The HRC (High Resolution Camera) is a photon counting instrument to be flown on the Advanced X-Ray Astrophysics Facility (AXAF). It is a large field of view, high angular resolution, detector for the x-ray telescope. The HRC consists of a CsI coated microchannel plate (MCP) acting as a soft x-ray photocathode, followed by a second MCP for high electronic gain. The MCPs are readout by a crossed grid of resistively coupled wires to provide high spatial resolution along with timing and pulse height data. The instrument will be used in two modes, as a direct imaging detector with a limiting sensitivity of 10 to the -15 ergs sq cm sec in a 10 to the 5th second exposure, and as a readout for an objective transmission grating providing spectral resolution of several hundreds to thousands.

Source record↗

NASA NTRS1986

The Advanced X-ray Astrophysics Facility high resolution camera

The HRC (High Resolution Camera) is a photon counting instrument to be flown on the Advanced X-Ray Astrophysics Facility (AXAF). It is a large field of view, high angular resolution, detector for the X-ray telescope. The HRC consists of a CsI coated microchannel plate (MCP) acting as a soft X-ray photocathode, followed by a second MCP for high electronic gain. The MCPs are readout by a crossed grid of resistively coupled wires to provide high spatial resolution along with timing and pulse height data. The instrument will be used in two modes, as a direct imaging detector with a limiting sensitivity of 10 to the -15th ergs/sq cm sec in a 10 to the 5th second exposure, and as a readout for an objective transmission grating providing spectral resolution of several hundreds to thousands.

Murray, Stephen S.↗

NASA NTRS2004

LiCoO2 and SnO2 Thin Film Electrodes for Lithium-Ion Battery Applications

There is an increasing need for small dimension, ultra-lightweight, portable power supplies due to the miniaturization of consumer electronic devices. Rechargeable thin film lithium-ion batteries have the potential to fulfill the growing demands for micro-energy storage devices. However, rechargeable battery technology and fabrication processes have not kept paced with the advances made in device technology. Economical fabrication methods lending excellent microstructural and compositional control in the thin film battery electrodes have yet to be fully developed. In this study, spin coating has been used to demonstrate the flexibility of the approach to produce both anode (SnO2) and cathode (LiCoO2) thin films. Results on the microstructure crystal structure and electrochemical properties of the thin film electrodes are described and discussed.

Maranchi, Jeffrey P.↗

NASA NTRS2013

Evaluation of Ceramic Matrix Composite Technology for Aircraft Turbine Engine Applications

The goals of the NASA Environmentally Responsible Aviation (ERA) Project are to reduce the NO(x) emissions, fuel burn, and noise from turbine engines. In order to help meet these goals, commercially-produced ceramic matrix composite (CMC) components and environmental barrier coatings (EBCs) are being evaluated as parts and panels. The components include a CMC combustor liner, a CMC high pressure turbine vane, and a CMC exhaust nozzle as well as advanced EBCs that are tailored to the operating conditions of the CMC combustor and vane. The CMC combustor (w/EBC) could provide 2700 F temperature capability with less component cooling requirements to allow for more efficient combustion and reductions in NOx emissions. The CMC vane (w/EBC) will also have temperature capability up to 2700 F and allow for reduced fuel burn. The CMC mixer nozzle will offer reduced weight and improved mixing efficiency to provide reduced fuel burn. The main objectives are to evaluate the manufacturability of the complex-shaped components and to evaluate their performance under simulated engine operating conditions. Progress in CMC component fabrication, evaluation, and testing is presented in which the goal is to advance from the proof of concept validation (TRL 3) to a system/subsystem or prototype demonstration in a relevant environment (TRL 6).

Halbig, Michael C.↗

NASA NTRS1990

High-temperature polymer matrix composites

Polymers research at the NASA Lewis Research Center has produced high-temperature, easily processable resin systems, such as PMR-15. In addition, the Polymers Branch has investigated ways to improve the mechanical properties of polymers and the microcracking resistance of polymer matrix composites in response to industry need for new and improved aeropropulsion materials. Current and future research in the Polymers Branch is aimed at advancing the upper use temperature of polymer matrix composites to 700 F and beyond by developing new resins, by examining the use of fiber reinforcements other than graphite, and by developing coatings for polymer matrix composites to increase their oxidation resistance.

Meador, Michael A.↗

NASA NTRS1992

Feasibility study of the use of synchrotron radiation in the calibration of AXAF - Initial reflectivity results

The 1-percent calibration accuracy goal of the Advanced X-ray Astrophysics Facility is being approached by way of an experiment at the National Synchrotron Light Source that will demonstrate the accuracy achievable in reflectance measurements conducted on coated flat mirrors in the 50 eV-12 keV energy range. The coatings will be of commercially produced Au, Ni, and Ir, deposited either by sputtering or by e-beam deposition. Optical constants will be estimated via the reflectance vs. angle-of-incidence method.

Graessle, D. E.↗

NASA NTRS1997

Low Cost Large Space Antennas

The mobile communication community could significantly benefit from the availability of low-cost, large space-deployable antennas. A new class of space structures, called inflatable deployable structures, will become an option for this industry in the near future. This new technology recently made significant progress with respect to reducing the risk of flying large inflatable structures in space. This progress can be attributed to the successful space flight of the Inflatable Antenna Experiment in May of 1996, which prompted the initiation of the NASA portion of the joint NASA/DOD coordinated Space Inflatables Program, which will develop the technology to be used in future mobile communications antennas along with other users. The NASA/DOD coordinated Space Inflatables Program was initiated in 1997 as a direct result of the Inflatable Antenna Experiment. The program adds a new NASA initiative to a substantial DOD program that involves developing a series of ground test hardware, starting with 3 meter diameter units and advancing the manufacturing techniques to fabricate a 25 meter ground demonstrator unit with surface accuracy exceeding the requirements for mobile communication applications. Simultaneously, the program will be advancing the state of the art in several important inflatable technology areas, such as developing rigidizable materials for struts and tori and investigating thin film technology issues, such as application of coatings, property measurement and materials processing and assembly techniques. A very important technology area being addressed by the program is deployment control techniques. The program will sponsor activities that will lead to understanding the effects of material strain energy release, residual air in the stowed structure, and the design of the launch restraint and release system needed to control deployment dynamics. Other technology areas directly applicable to developing inflatable mobile communication antennas in the near future are analytical performance prediction tools, configuration studies and miniaturizing the inflation systems.

Chmielewski, Artur B.↗

NASA NTRS2013

Luminescence-Based Diagnostics of Thermal Barrier Coating Health and Performance

Thermal barrier coatings (TBCs) are typically composed of translucent ceramic oxides that provide thermal protection for metallic components exposed to high-temperature environments in both air- and land-based turbine engines. For advanced turbine engines designed for higher temperature operation, a diagnostic capability for the health and performance of TBCs will be essential to indicate when a mitigating action needs to be taken before premature TBC failure threatens engine performance or safety. In particular, it is shown that rare-earth-doped luminescent sublayers can be integrated into the TBC structure to produce luminescence emission that can be monitored to assess TBC erosion and delamination progression, and to map surface and subsurface temperatures as a measure of TBC performance. The design and implementation of these TBCs with integrated luminescent sublayers are presented.

Eldridge, Jeffrey I.↗

NASA NTRS2019

Further Development Of Aperture: A Precise Extremely Large Reflective Telescope Using Re-Configurable Elements: NASA Innovative Advanced Concepts (NIAC) - Phase II

One of the pressing needs for space ultraviolet-visible astronomy is a design to allow larger mirrors than the James Webb Space Telescope primary. The diameter of the rocket fairing limits the mirror diameter such that all future missions calling for mirrors up to 16 meters in diameter or larger will require a mirror that is deployed post-launch. In response to the deployment requirement, we address the issues of this concept called "A Precise Extremely Large Reflective Telescope Using Reconfigurable Elements (APERTURE) with both hardware experiments and software simulations... We designed and built several fixtures with O-rings to hold a membrane. We established a coating process to make a membrane that was coated on one side with Cr and the other side with Cr-Terfenol-D-NiCo. The Terfenol-D (T-D hereafter) is the MSM (Magnetic Smart Memory) we use. We bought and established a procedure for measuring a deformation over time and purchased a Shack Hartmann system from Imagine Optic (https://www.imagine-optic.com). The first substrate we used was DuPont (TM) Kapton® polyimide film. Due to material creep, we found the stability over a 48-hour period with a Kapton substrate was not as good as desired (greater than 1 micron). We then switched to CP1 Polyimide. We found the CP1 much more stable to creep, being stable from about 3 hours to 48 hours to within a measurement error to below approximately 0.1 micron. We produced a 13 micron maximum deviation on a 50-millimeter-diameter piece of CP1 (25 microns thick). The T-D coating was about 2 microns, and the other layers, about 10 nanometers. The magnetic field at the base was about 0.1 teslas. We can make the T-D film at least 5 times thicker and the magnetic field at least 5 times stronger, and hence make deformations as much as 25 times larger. We have a formed a collaboration produced at the NIAC (NASA Innovative Advanced Concepts) mid-term review with Dr. Ron Shiri of Goddard Space Flight Center (GSFC) to explore making controlled deviations on lambda/14-lambda/20 scales which are required to bring a surface to the diffraction limit. We carried out only preliminary work on Si using a Coordinate Measuring Machine (CMM), which produced deviations on the 1 micron level. We are still working on a program to bring to GSFC a flat enough (radius of curvature greater than 10 microns) -coated a Si piece with Cr, T-D, NiCo. Then we plan to carry out tests with an interferometer. Further, we formed a new collaboration with Prof. Rajan Vaidyanathan of the University of Central Florida to replace the CP1 with a shape memory alloy (SMA). With his collaboration, we acquired new Federal funding outside of NASA to explore the use of SMAs (we use NiTi). Our preliminary results indicate that we can produce deformations greater than 1 micron on approximately 100 microns thick. Furthermore we have shown that the NiTi can deploy to better than 1 micron of its set original and then trained shape.

Re-Configurable Elements↗

NASA NTRS2006

Evaluation of Coatings and Materials for Future Radiators

Radiators are used to reject energy from space vehicles through radiant heat transfer. They are typically the largest component in a vehicle's thermal control system and can have a large impact on the vehicle design and operation. NASA s current vision for exploration dictates that radiators for a Crew Exploration Vehicle (CEV), a Lunar Surface Access Module (LSAM), and a lunar base will need to be developed. These applications present new challenges when compared to previous radiators on the Space Shuttle and International Space Station (ISS). In addition, many technological advances have been made that could positively impact future radiator design. This paper outlines new requirements for future radiators and documents a trade study performed to select the some promising technologies for further evaluation. The technologies include K1100 based carbon composites for the radiator surface as well as Optical Solar Reflectors (OSRs), a lithium based white paint, and electrochromic thin films for optical coatings. Coupons were made using these materials and tests were performed to characterize their performance. Testing included evaluating structural and thermal properties of the carbon composites, thermal cycling, launch pad weather simulation, and exposure to solar wind, and Ultraviolet (UV) radiation.

Tuan, George C.↗

NASA NTRS2009

Mid-Infrared Reflectance Imaging of Thermal-Barrier Coatings

An apparatus for mid-infrared reflectance imaging has been developed as means of inspecting for subsurface damage in thermal-barrier coatings (TBCs). The apparatus is designed, more specifically, for imaging the progression of buried delamination cracks in plasma-sprayed yttria-stabilized zirconia coatings on turbine-engine components. Progression of TBC delamination occurs by the formation of buried cracks that grow and then link together to produce eventual TBC spallation. The mid-infrared reflectance imaging system described here makes it possible to see delamination progression that is invisible to the unaided eye, and therefore give sufficiently advanced warning before delamination progression adversely affects engine performance and safety. The apparatus (see figure) includes a commercial mid-infrared camera that contains a liquid-nitrogen-cooled focal plane indium antimonide photodetector array, and imaging is restricted by a narrow bandpass centered at wavelength of 4 microns. This narrow wavelength range centered at 4 microns was chosen because (1) it enables avoidance of interfering absorptions by atmospheric OH and CO2 at 3 and 4.25 microns, respectively; and (2) the coating material exhibits maximum transparency in this wavelength range. Delamination contrast is produced in the midinfrared reflectance images because the introduction of cracks into the TBC creates an internal TBC/air-gap interface with a high diffuse reflectivity of 0.81, resulting in substantially higher reflectance of mid-infrared radiation in regions that contain buried delamination cracks. The camera is positioned a short distance (.12 cm) from the specimen. The mid-infrared illumination is generated by a 50-watt silicon carbide source positioned to the side of the mid-infrared camera, and the illumination is collimated and reflected onto the specimen by a 6.35-cm-diameter off-axis paraboloidal mirror. Because the collected images are of a steady-state reflected intensity (in contrast to the transient thermal response observed in infrared thermography), collection times can be lengthened to whatever extent needed to achieve desired signal-to-noise ratios. Each image is digitized, and the resulting data are processed in several steps to obtain a true mid-infrared reflectance image. The raw image includes thermal radiation emitted by the specimen in addition to the desired reflected radiation. The thermal-radiation contribution is eliminated by subtracting the image obtained with the illumination off from the image obtained with the illumination on. A flat-field correction is then made to remove the effects of non-uniformities in the illumination level and pixel-to-pixel variations in sensitivity. This correction is performed by normalizing to an image of a standard object that has a known reflectance at a wavelength of 4 microns. After correction, each pixel value is proportional to the reflectance (at a wavelength of 4-microns) at the corresponding location on the specimen. Mid-infrared reflectance imaging of specimens that were thermally cyc led for different numbers of cycles was performed and demonstrated t hat mid-infrared reflectance imaging was able to monitor the gradual delamination progression that occurs with continued thermal cycling . Reproducible values were obtained for the reflectance associated w ith an attached and fully delaminated TBC, so that intermediate refle ctance values could be interpreted to successfully predict the numbe r of thermal cycles to failure.

Edlridge, Jeffrey I.↗

NASA NTRS1993

Polymer Infiltration Studies

Significant progress has been made on the preparation of carbon fiber composites using advanced polymer resins during the past three months. Current and ongoing research activities reported herein include: (1) Prepregger Hot Sled Operation; (2) Ribbonizing Powder-Impregnated Towpreg; (3) Textile Composites from Powder-Coated Towpreg: Role of Bulk Factor; and (4) Powder Curtain Prepreg Process. During the coming months research will be directed toward further development of the new powder curtain prepregging method and on ways to customize dry powder towpreg for textile and robotic applications in aircraft part fabrication. Studies of multi-tow powder prepregging and ribbon preparation will be conducted in conjunction with continued development of prepegging technology and the various aspects of composite part fabrication using customized towpreg. Also, work will continue on the analysis of the new solution prepegger.

Marchello, Joseph M.↗