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DOE OSTI2019

Effect of deuterium irradiation on graphite boronized in the NSTX-U tokamak

Boronization has been used in the National Spherical Torus-Upgrade (NSTX-U) as first wall conditioning technique. The technique decreased the oxygen impurities in the plasma and the O% on the Plasma Facing Components (PFC) as measured with an in-vacuo probe. Samples were extracted from tiles removed from the tokamak for post-mortem and controlled studies. Ex-vessel low energy and fluence D2+ and Ar+ irradiations were characterized in-situ to elucidate surface evolution of a cored graphite sample with an intrinsic concentration of boron from a tokamak environment. In addition, quadrupole mass spectrometer measurements of emitted D-containing species during irradiation, indicate potential retention of D by the boronized graphite interface and correlated back to the surface chemistry evolution. Classical Molecular Dynamics (CMD) simulations were used to investigate the chemistry of the B-C-O-D system. The results suggest that boron coatings retain oxygen by forming oxidized boron states in the presence of deuterium plasmas and corroborate empirical findings. A four times increase in the O% of the boron coatings was observed following in-situ deuterium exposures, in contrast with a reduction of equal magnitude observed after Ar irradiations. These results illustrate the complex chemistry driven by energetic ions at the edge of tokamaks plasmas on the PFCs.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2015

Validation Results for Core-Scale Oil Shale Pyrolysis

This report summarizes a study of oil shale pyrolysis at various scales and the subsequent development a model for in situ production of oil from oil shale. Oil shale from the Mahogany zone of the Green River formation was used in all experiments. Pyrolysis experiments were conducted at four scales, powdered samples (100 mesh) and core samples of 0.75”, 1” and 2.5” diameters. The batch, semibatch and continuous flow pyrolysis experiments were designed to study the effect of temperature (300°C to 500°C), heating rate (1°C/min to 10°C/min), pressure (ambient and 500 psig) and size of the sample on product formation. Comprehensive analyses were performed on reactants and products - liquid, gas and spent shale. These experimental studies were designed to understand the relevant coupled phenomena (reaction kinetics, heat transfer, mass transfer, thermodynamics) at multiple scales. A model for oil shale pyrolysis was developed in the COMSOL multiphysics platform. A general kinetic model was integrated with important physical and chemical phenomena that occur during pyrolysis. The secondary reactions of coking and cracking in the product phase were addressed. The multiscale experimental data generated and the models developed provide an understanding of the simultaneous effects of chemical kinetics, and heat and mass transfer on oil quality and yield. The comprehensive data collected in this study will help advance the move to large-scale in situ oil production from the pyrolysis of oil shale.

Staten, Josh↗

NASA NTRSDate not supplied

Pneumatic Sampler (P-Sampler) for the Martian Moons Exploration (MMX)

The Martian Moons eXploration (MMX) mission, led by the Japanese Aerospace Exploration Agency (JAXA), will focus on the exploration of the two Martian moons – Phobos and Deimos (Figure 1). The spacecraft will perform close-up remote sensing and observations of both moons and collect a sample from Phobos for Earth sample return. MMX has set the two mission goals: (1) determining the origin of the Martian moons and (2) observing processes in the circumplanetary environment of Mars, based on remote sensing, in-situ observations, and laboratory analyses of returned samples of Phobos regolith [1-2]. To fulfill the mission goals, MMX employs a double sampling approach: Coring and Pneumatic Samplers (Figure 2).The Coring Sampler (C-Sampler), a core soil tube deployed by a robotic arm, providing access to the building blocks of Phobos beneath the surface (>2 cm), and also collect a mixture of near surface material. The P-Sampler, on the other hand, would selectively sample the surface veneer and provides reference of surface component with the C-Sampler. The double sampling system not only enhances the scientific merits of MMX but also reduces risks associated with the sampling of Phobos. Without enough knowledge of the physical and chemical properties, and the geotechnical conditions of the surface of Phobos (e.g., compositions, temperature gradient/variation, porosity, grain size distribution), having two sampling systems that utilize entirely different sampling approaches is prudent.

Dylan Van Dyne↗

DOE OSTI2025

Roughrider Carbon Storage Hub (Final Report)

The Roughrider Carbon Storage Hub was a 2-year project (October 2023 – September 2025) conducted by the Energy & Environmental Research Center (EERC) focused on advancing the feasibility of a commercial-scale carbon dioxide (CO 2 ) geologic storage hub in McKenzie County, North Dakota. The project’s objective was to investigate the potential that stacked storage complexes (multiple deep saline formations) can safely and economically store at least 50 million tonnes of CO 2 within 30 years. The captured CO 2 would be sourced from industrial emitters including project partner ONEOK, Inc.’s gas-processing plants and a planned gas-to-liquids facility. Drilling of the Roughrider 1 stratigraphic test well (14,979-ft total depth) was completed in November 2024. The wellbore intersected four candidate storage formations: Inyan Kara, Broom Creek, Mission Canyon, and Black Island–Deadwood. Operational challenges, including a stuck drill string, were resolved without long-term impact. A comprehensive logging and coring program was conducted, followed by successful well abandonment and site reclamation. Over 660 ft of 4-in. whole core was retrieved. Core plug samples were processed and analyzed for petrophysical and geochemical properties. Results confirmed promising porosity and permeability in the Inyan Kara and Broom Creek Formations and removal of the Mission Canyon and Black Island–Deadwood horizons from further investigation. Data derived from the logging and coring program were used to improve initial geologic models built from legacy data. CO 2 injection simulations showed that the Inyan Kara alone can feasibly store the target mass of CO 2 . Because of subtle differences in geologic structure and porosity trends between the formations, a stacked storage scenario using the Broom Creek and Inyan Kara Formations resulted in a larger overall plume area than using the Inyan Kara alone. Preliminary CO 2 pipeline routes from the industrial sources were mapped utilizing existing rights of way and evaluated for capacity and cost using U.S. Department of Energy Office of Fossil Energy and Carbon Management/National Energy Technology Laboratory models and U.S. Environmental Protection Agency emissions data. Integrating capture, transport, and storage cost estimates with policy incentives (e.g., 45Q credits) provided a total cost-per-ton analysis. Results indicate that the small scale of the volumes to be transported over the cumulative large distances does not support the project’s financial viability. However, the groundwork laid during this project from geological, regulatory, and social perspectives positions the Roughrider hub site as a promising candidate for commercial carbon storage in North Dakota, especially if the economy of scale is introduced for CO 2 transportation to the hub site.

01 COAL, LIGNITE, AND PEAT↗

DOE OSTI2016

SPRUCE Deep Peat Heating (DPH) Peat Water Content and Temperature for Experimental Plot Cores, June 2014 through June 2015

This data set provides the peat water content and peat temperature at time of sampling for peat cores collected before and during the SPRUCE Deep Peat Heating (DPH) study. Cores were collected during three sampling events: 03 June 2014, 09 September 2014, and 16 June 2015. Two cores were extracted from hollow locations in each of the 10 experimental plots (4, 6, 8, 10, 11, 13, 16, 17, 19, and 20). The five ambient plots (5, 7, 14, and 21) were not included in the DPH sampling efforts. See Table 1. Cores were partitioned into samples at 11 depth increments: 0-10, 10-20, 20-30, 30-40, 40-50, 50-75, 75-100, 100-125, 125-150, 150-175, and 175-200 cm below surface of the hollow. The DPH study was undertaken to evaluate possible rapid responses of deep peat carbon (C) stocks, microbial communities, and biogeochemical cycling processes to unprecedented temperatures. In June 2014, deep soil heating was initiated at 5 warming levels (+0, +2.25, +4.5, +6.75 and +9 °C) with 2 replicate plots per level. Warming levels at depth were achieved over a 25 (+ 2.25 °C) to 60-day (+9 °C) period depending on the target treatment temperatures. Data file – There is one comma-separated (*.csv) file with peat core water content and temperature at time of sampling, plus the amount of dried archived material retained after analyses. User Note: In this third release, four variables related to extrapolations of peat core temperature were removed. See the Data Set History table for additional details. 25-150, 150-175, and 175-200 cm below surface of the hollow.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2015

Magnetic behavior of La-doped Fe{sub 3}O{sub 4} studied by perturbed angular correlation spectroscopy with {sup 111}Cd and {sup 140}Ce

In this paper, the local magnetic properties of La-doped Fe{sub 3}O{sub 4} (5% and 10%) bulk and Nanoparticles (NPs) samples were studied by measuring hyperfine interactions in a wide range of temperature from 10 to 900 K with perturbed γ-γ angular correlation spectroscopy using {sup 111}In({sup 111}Cd) and {sup 140}La({sup 140}Ce) as probe nuclei. Results for the temperature dependence of the magnetic hyperfine field (B{sub hf}) for bulk and NP samples, pure and doped with La show that its behavior follows a second order Brillouin-like transition from which the Curie temperature (T{sub C}) was determined (T{sub C} ∼ 855 K). Results also show two different regions in NP samples: the core where a minor fraction of probe nuclei with well defined magnetic dipole frequency was observed and the shell where a major fraction with broad distributed electric quadrupolar frequency (surface effect in NP) was observed. The Verwey transition T{sub V} ∼ 120 K, due the order disorder phase, was also observed in all samples. The results are discussed in terms of the magnetic exchange interaction between Fe{sup 2+} and Fe{sup 3+} ions in the two regions of NP.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

NASA NTRS1993

Natural thermoluminescence profiles in lunar cores and implications for meteorites

Meteorites and lunar samples have been irradiated by high energy cosmic rays, typically for millions of years. In addition to producing isotopic changes, the irradiation creates ionization which may be recorded in the form of stored thermoluminescence (TL) in certain minerals, the most important of which is feldspar. One aspect of interpreting the TL of these samples is the effect of 'shielding' or depth control, which is particularly important for meteorites, since they have lost an unknown amount of mass during atmospheric entry. Here we report theoretical calculations which we compare with samples from lunar cores for which we have excellent stratigraphic control. We then discuss the implications for these results for the TL of meteorites, which have a different irradiation geometry. We find that, in general, calculated profiles are similar to those observed in lunar samples and meteorites. Additional effects, such as orbital (thermal) history and terrestrial age must also be considered in the case of meteorites.

Benoit, P. H.↗

DOE OSTI2015

A Bayesian, multivariate calibration for Globigerinoides ruberMg/Ca

The use of Mg/Ca in marine carbonates as a paleothermometer has been challenged by observations that implicate salinity as a contributing influence on Mg incorporation into biotic calcite and that dissolution at the sea-floor alters the original Mg/Ca. Yet, these factors have not yet been incorporated into a single calibration model. In this paper, we introduce a new Bayesian calibration for Globigerinoides ruber Mg/Ca based on 186 globally distributed core top samples, which explicitly takes into account the effect of temperature, salinity, and dissolution on this proxy. Our reported temperature, salinity, and dissolution (here expressed as deep-water ΔCO 2- 3 ) sensitivities are (±2σ) 8.7±0.9%/°C, 3.9±1.2%/psu, and 3.3±1.3%/μmol.kg -1 below a critical threshold of 21 μmol/kg in good agreement with previous culturing and core-top studies. We then perform a sensitivity experiment on a published record from the western tropical Pacific to investigate the bias introduced by these secondary influences on the interpretation of past temperature variability. This experiment highlights the potential for misinterpretations of past oceanographic changes when the secondary influences of salinity and dissolution are not accounted for. Finally, multiproxy approaches could potentially help deconvolve the contributing influences but this awaits better characterization of the spatio-temporal relationship between salinity and δ 18 O sw over millennial and orbital timescales.

58 GEOSCIENCES↗

NASA NTRSDate not supplied

Stratigraphy of the Apollo 17 Landslide Core 73002 From FMR Maturity and VNIR and Mössbauer Spectroscopy

A suite of samples from the Apollo missions to the Moon (1969-1973) were set aside and stored under controlled conditions to have unexamined lunar samples available decades later for analyses that take advantage of evolved sample handling techniques, maturation of then existing instrumentation, and development of new analytical techniques and instrumentation [e.g., 1]. One preserved sample is the Apollo 17 double drive tube core (73001/2) that was driven into the lunar surface on the landslide deposit at Station 3 on the South Massif in the Taurus-Littrow valley [2]. The deeper section (73001) was stored frozen in a Core Sample Vacuum Container (CSVC) to maximize preservation of lunar volatiles. We report here, as a part of the Apollo Next Generation Sample Analysis (ANGSA) Initiative [1,3], stratigraphy for the upper core section (73002) with respect to maturity (ferromagnetic resonance (FMR) maturity index Is/FeO [4-6]), visible-near-IR (VNIR) spectroscopy, and, for representative samples, grain-size analysis and Mössbauer spectroscopy. Stratigraphy provides data to model the dynamics of lunar landslide deposits and their post-emplacement evolution in comparison to impact-driven mixing on an airless body and stratigraphic context for volatile and (if any) organic behavior. Reported by [7] are preliminary results for multispectral imaging and hyperspectral scanning of the first dissection pass of 73002.

R. V. Morris↗

DOE OSTI2015

Fe 2 O 3 –TiO 2 core–shell nanorod arrays for visible light photocatalytic applications

By using the glancing angle deposition technique and post-deposition annealing, Fe 2 O 3 –TiO 2 core-shell nanorod arrays with specific crystalline states can be designed and fabricated. The Fe 2 O 3 –TiO 2 core-shell samples annealed at temperatures greater than 450°C formed α-Fe 2 O 3 and anatase TiO 2 , and showed higher catalytic efficiency for the degradation of methylene blue (MB) under visible light illumination when compared with pure anatase TiO 2 or α-Fe 2 O 3 nanorod arrays. Solar conversion of carbon dioxide and water vapor in the presence of Fe 2 O 3 –TiO 2 core-shell nanorod arrays was also investigated. Carbon monoxide, hydrogen, methane, and methanol along with other hydrocarbons were produced after only several hours’ exposure under ambient sunlight. It was determined that the core-shell structure showed greater efficiency for solar CO 2 conversion than the pure TiO 2 nanorod arrays.

Glancing angle deposition↗

NASA NTRS2020

STIG: A Two-Speed Transmission Aboard the Mars2020 Coring Drill

The coring drill, part of the Sampling & Caching Subsystem (SCS) aboard the Mars2020 rover, demands a wide range of drill bit torque and speed capabilities during sample acquisition operations. The two driving operating points are high speed, low torque for rotary-percussive coring, as well as low speed, high torque for separating the rock core sample from its parent rock. The spindle twin-input transmission (STIG) allows these and other operating points to be reached with an actuator of substantially less peak power and maximum current draw than that of a single-speed actuator. Rather than containing gearing of its own, the transmission interfaces to an actuator with two outputs of different gear ratios, allowing the transmission to select one of the two of the outputs to be coupled to the drill bit. This paper describes the design, capabilities, and challenges associated with the transmission and the dual-output actuator.

Szwarc, Timothy↗

NASA NTRS2006

Concept for coring from a low-mass rover

Future Mars missions, such as the Mars Sample Return (MSR) mission, may benefit from core sample acquisition from a low-mass rover where the rover cannot be assumed to be stationary during a coring operation. Manipulation from Mars rovers is currently done under the assumption that the rover acts as a stationary, stable platform for the arm. An MSR mission scenario with a low-mass rover has been developed and the technology needs have been investigated. Models for alternative types of coring tools and tool-environment interaction have been developed and input along with wheel-soil interaction models into the Stanford Simulation & Active Interfaces (SAI) simulation environment to enable simulation of coring operations from a rover. Coring tests using commercial coring tools indicate that the quality of the core is a critical criterion in the system design. Current results of the models, simulation, and coring tests are provided.

rovers↗

DOE OSTI2019

Wabash CarbonSAFE Subtask 7.1 – Pre-drilling Site Assessment Topical Report: DOE-FE0031626-1

The Wabash CarbonSAFE project will drill a stratigraphic test well at the Wabash Valley Resources facility near Terre Haute, Indiana. Lithologic, geomechanical, and geophysical data collected from samples testing and an extensive geophysical logging suite will be used to determine the feasibility for the geologic sequestration of 50 million metric tons or more of injected carbon dioxide. The primary target reservoir and caprock to be investigated for the Wabash CarbonSAFE project are the Mt. Simon Sandstone and Eau Claire Shale, respectively. The project team has assessed the planned Wabash #1 drilling site using subsurface geologic data and analyses from both Illinois and Indiana. These data were used to generate geologic structure and isopach thickness maps for target reservoir and caprock layers which were incorporated into a detailed discussion of the nature of the Illinois Basin’s Cambro-Ordovician carbon dioxide storage complex at the drilling site. Formation tops were prognosed for 19 lithologic units to aid drilling and coring procedures. Additional GIS analysis indicates that no known structural features will negatively impact the target storage reservoir or caprock, nor will protected and sensitive areas, groundwater resources, or existing resource development be negatively affected by Wabash #1 drilling activities. The Wabash #1 Geologic/Structure Test well drilling permit was awarded by Indiana Department of Natural Resources (IN-DNR) – Division of Oil and Gas on November 12th, 2019, and the well is expected to be drilled to a total depth of approximately 8,350 feet. Potential impacts on drilling progress include abandoned underground coal mines which mined the Springfield and Survant coals until 1964 and 1954, respectively, and a lost circulation zone in the Potosi Dolomite, which has been demonstrated to have intermittent cavernous porosity from karstification. This document also details the coring and sampling program, proposed logging suite, and well testing program, all of which will be dynamically reviewed as drilling progresses.

29 ENERGY PLANNING, POLICY, AND ECONOMY↗

DOE OSTI2016

Results and analysis of saltstone cores taken from saltstone disposal unit cell 2A

As part of an ongoing Performance Assessment (PA) Maintenance Plan, Savannah River Remediation (SRR) has developed a sampling and analyses strategy to facilitate the comparison of field-emplaced samples (i.e., saltstone placed and cured in a Saltstone Disposal Unit (SDU)) with samples prepared and cured in the laboratory. The primary objectives of the Sampling and Analyses Plan (SAP) are; (1) to demonstrate a correlation between the measured properties of laboratory-prepared, simulant samples (termed Sample Set 3), and the field-emplaced saltstone samples (termed Sample Set 9), and (2) to validate property values assumed for the Saltstone Disposal Facility (SDF) PA modeling. The analysis and property data for Sample Set 9 (i.e. six core samples extracted from SDU Cell 2A (SDU2A)) are documented in this report, and where applicable, the results are compared to the results for Sample Set 3. Relevant properties to demonstrate the aforementioned objectives include bulk density, porosity, saturated hydraulic conductivity (SHC), and radionuclide leaching behavior.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2017

Spinel Ferrite Core–Shell Nanostructures by a Versatile Solvothermal Seed-Mediated Growth Approach and Study of Their Nanointerfaces

An easy, low-cost, repeatable seed-mediated growth approach in solvothermal condition has been proposed to synthesize bimagnetic spinel ferrite core–shell heterostructures in the 10–20 nm particle size range. Cobalt ferrite and manganese ferrite nanoparticles (CoFe 2 O 4 and MnFe 2 O 4 ) have been coated with isostructural spinel ferrites like maghemite/magnetite, MnFe 2 O 4 , and CoFe 2 O 4 with similar cell parameters to create different heterostructures. The conventional study of the structure, morphology, and composition has been combined with advanced techniques in order to achieve details on the interface at the nanoscale level. Clear evidence of the heterostructure formation have been obtained (i) indirectly by comparing the 57 Fe Mössbauer spectra of the core–shell samples and an ad hoc mechanical mixture and (ii) directly by mapping the nanoparticles’ chemical composition by electron energy loss spectroscopy (EELS) and energy-dispersive X-ray spectroscopy (EDX) in the scanning transmission electron microscopy mode (STEM). Additionally, chemical-sensitive electron tomography in STEM-EDX mode has been applied in order to obtain detailed 3D images with a sub-nanometer spatial resolution.

36 MATERIALS SCIENCE↗

DOE OSTI2021

Reactivity of CO 2 with Utica, Marcellus, Barnett, and Eagle Ford Shales and Impact on Permeability

We report that in order to reduce greenhouse gas emissions while recovering hydrocarbons from unconventional shale formations, processes that make use of carbon dioxide to enhance oil recovery while storing carbon dioxide (CO 2 ) should be considered. Here, we examine samples from three shale basins across the United States (Utica and Marcellus Shales in the Appalachian Basin, Barnett Shale in the Bend Arch-Ft. Worth Basin, and Eagle Ford in the Western Gulf Basin) to address the following questions: (1) do changes from reaction with CO 2 and fluids at the micrometer and nanometer scale alter flow pathways and, in turn, impact hydrocarbon production, CO 2 storage, and seal integrity and (2) can CO 2 or fluid reactivity be predicted based on physical or chemical properties of shale formations? Experiments were conducted at 40 °C and 10.3 MPa to characterize the interaction between CO 2 and shale using X-ray diffraction (XRD), carbon and sulfur analysis, in situ Fourier transform infrared spectroscopy (FT-IR), feature relocation scanning electron microscopy coupled with energy-dispersive spectroscopy (SEM-EDS), mercury (Hg) intrusion porosimetry, and Brunauer-Emmett-Teller (BET) surface area and pore size analysis coupled with density functional theory (DFT) methods. Changes in mechanical, physical, and flow properties of shale cores due to CO 2 exposure were addressed using a New England Research Autolab 1500 and Xenon X-ray computed tomography (CT) scanning. Results showed that CO 2 did not promote significant reactivity with the shale if water was not present; only shales with swelling clays or residual interstitial pore water reacted with dry CO 2 to promote reactivity in shale. When water was added as a reactant, CO 2 formed carbonic acid and reacted with the shale to dissolve carbonate pockets, etched and pitted the shale matrix surfaces, and increased the microporosity and decreased nanoporosity. Porosity and permeability increased appreciably in core shale samples after exposure to CO 2 saturated fluid due to dissolution of carbonate. Shale mechanical properties were not altered. Trends were not observed that could tie CO 2 or fluid reactivity to physical or chemical properties of the shale formations at the basin scale from the samples we examined. However, if the shale contained significant amounts of carbonate and water was available to react with the CO 2 , pore sizes were altered in the matrix and permeability and porosity increased.

04 OIL SHALES AND TAR SANDS↗

DOE OSTI2014

Three-dimensional NDE of VHTR core components via simulation-based testing. Final report

A next generation, simulation-driven-and-enabled testing platform is developed for the 3D detection and characterization of defects and damage in nuclear graphite and composite structures in Very High Temperature Reactors (VHTRs). The proposed work addresses the critical need for the development of high-fidelity Non-Destructive Examination (NDE) technologies for as-manufactured and replaceable in-service VHTR components. Centered around the novel use of elastic (sonic and ultrasonic) waves, this project deploys a robust, non-iterative inverse solution for the 3D defect reconstruction together with a non-contact, laser-based approach to the measurement of experimental waveforms in VHTR core components. In particular, this research (1) deploys three-dimensional Scanning Laser Doppler Vibrometry (3D SLDV) as a means to accurately and remotely measure 3D displacement waveforms over the accessible surface of a VHTR core component excited by mechanical vibratory source; (2) implements a powerful new inverse technique, based on the concept of Topological Sensitivity (TS), for non-iterative elastic waveform tomography of internal defects - that permits robust 3D detection, reconstruction and characterization of discrete damage (e.g. holes and fractures) in nuclear graphite from limited-aperture NDE measurements; (3) implements state-of-the art computational (finite element) model that caters for accurately simulating elastic wave propagation in 3D blocks of nuclear graphite; (4) integrates the SLDV testing methodology with the TS imaging algorithm into a non-contact, high-fidelity NDE platform for the 3D reconstruction and characterization of defects and damage in VHTR core components; and (5) applies the proposed methodology to VHTR core component samples (both two- and three-dimensional) with a priori induced, discrete damage in the form of holes and fractures. Overall, the newly established SLDV-TS testing platform represents a next-generation NDE tool that surpasses all existing techniques for the 3D ultrasonic imaging of material damage from non-contact, limited-aperture waveform measurements. Outlook. The next stage in the development of this technology includes items such as (a) non-contact generation of mechanical vibrations in VHTR components via thermal expansion created by high-intensity laser; (b) development and incorporation of Synthetic Aperture Focusing Technique (SAFT) for elevating the accuracy of 3D imaging in highly noisy environments with minimal accessible surface; (c) further analytical and computational developments to facilitate the reconstruction of diffuse damage (e.g. microcracks) in nuclear graphite as they lead to the dispersion of elastic waves, (d) concept of model updating for accurate tracking of the evolution of material damage via periodic inspections; (d) adoption of the Bayesian framework to obtain information on the certainty of obtained images; and (e) optimization of the computational scheme toward real-time, model-based imaging of damage in VHTR core components.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

DOE OSTI2016

Reduced snow cover alters root‐microbe interactions and decreases nitrification rates in a northern hardwood forest

Abstract Snow cover is projected to decline during the next century in many ecosystems that currently experience a seasonal snowpack. Because snow insulates soils from frigid winter air temperatures, soils are expected to become colder and experience more winter soil freeze‐thaw cycles as snow cover continues to decline. Tree roots are adversely affected by snowpack reduction, but whether loss of snow will affect root‐microbe interactions remains largely unknown. The objective of this study was to distinguish and attribute direct (e.g., winter snow‐ and/or soil frost‐mediated) vs. indirect (e.g., root‐mediated) effects of winter climate change on microbial biomass, the potential activity of microbial exoenzymes, and net N mineralization and nitrification rates. Soil cores were incubated in situ in nylon mesh that either allowed roots to grow into the soil core (2 mm pore size) or excluded root ingrowth (50 μm pore size) for up to 29 months along a natural winter climate gradient at Hubbard Brook Experimental Forest, NH ( USA ). Microbial biomass did not differ among ingrowth or exclusion cores. Across sampling dates, the potential activities of cellobiohydrolase, phenol oxidase, and peroxidase, and net N mineralization rates were more strongly related to soil volumetric water content ( P < 0.05; R 2 = 0.25–0.46) than to root biomass, snow or soil frost, or winter soil temperature ( R 2 < 0.10). Root ingrowth was positively related to soil frost ( P < 0.01; R 2 = 0.28), suggesting that trees compensate for overwinter root mortality caused by soil freezing by re‐allocating resources towards root production. At the sites with the deepest snow cover, root ingrowth reduced nitrification rates by 30% ( P < 0.01), showing that tree roots exert significant influence over nitrification, which declines with reduced snow cover. If soil freezing intensifies over time, then greater compensatory root growth may reduce nitrification rates directly via plant‐microbe N competition and indirectly through a negative feedback on soil moisture, resulting in lower N availability to trees in northern hardwood forests.

Sorensen, Patrick O.↗