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NASA NTRS1986

Compression failure mechanisms of composite structures

An experimental and analytical study was conducted to delineate the compression failure mechanisms of composite structures. The present report summarizes further results on kink band formation in unidirectional composites. In order to assess the compressive strengths and failure modes of fibers them selves, a fiber bundle was embedded in epoxy casting and tested in compression. A total of six different fibers were used together with two resins of different stiffnesses. The failure of highly anisotropic fibers such as Kevlar 49 and P-75 graphite was due to kinking of fibrils. However, the remaining fibers--T300 and T700 graphite, E-glass, and alumina--failed by localized microbuckling. Compressive strengths of the latter group of fibers were not fully utilized in their respective composite. In addition, acoustic emission monitoring revealed that fiber-matrix debonding did not occur gradually but suddenly at final failure. The kink band formation in unidirectional composites under compression was studied analytically and through microscopy. The material combinations selected include seven graphite/epoxy composites, two graphite/thermoplastic resin composites, one Kevlar 49/epoxy composite and one S-glass/epoxy composite.

Hahn, H. T.↗

NASA NTRS1986

A study of the stress wave factor technique for nondestructive evaluation of composite materials

The acousto-ultrasonic method of nondestructive evaluation is an extremely sensitive means of assessing material response. Efforts continue to complete the understanding of this method. In order to achieve the full sensitivity of the technique, extreme care must be taken in its performance. This report provides an update of the efforts to advance the understanding of this method and to increase its application to the nondestructive evaluation of composite materials. Included are descriptions of a novel optical system that is capable of measuring in-plane and out-of-plane displacements, an IBM PC-based data acquisition system, an extensive data analysis software package, the azimuthal variation of acousto-ultrasonic behavior in graphite/epoxy laminates, and preliminary examination of processing variation in graphite-aluminum tubes.

Sarrafzadeh-Khoee, A.↗

NASA NTRS1986

Development of composite tube protective coatings

Protective coatings for graphite/epoxy (Gr/Ep) tubular structures proposed for the Space Station are evaluated. The program was divided into four parts; System Definition, Coating Concept Selection and Evaluation, Scale-up and Assembly, and Reporting. System Definition involved defining the structural and environmental properties required of the Gr/Ep tubes. The prepreg and ply sequence selected was a P75S/934 (O2, + or - 20, O2)sub s layup which meets the various structural requirements of the Space Station. Coating Concept and Selection comprised the main emphasis of the effort. Concepts for protectively coating the Gr/Ep tubes included the use of metal foil and electroplating. The program results demonstrated that both phosphoric and chromic acid anodized Al foil provided adequate adhesion to the Gr/Ep tubes and stability of optical properties when subjected to atomic oxygen and thermal cycling representative of the LEO environment. SiO2/Al coatings sputtered onto Al foils also resulted in an excellent protective coating. The electroplated Ni possessed unacceptable adhesion loss to the Gr/Ep tubes during atomic oxygen testing. Scale-Up and Assembly involved fabricating and wrapping 8-ft-long by 2-in-diameter Gr/EP tubes with chromic acid anodized foil and delivering these tubes, along with representative Space Station erectable end fittings, to NASA LaRC.

Dursch, H.↗

NASA NTRS1985

Prediction of impact force and duration due to low-velocity impact on circular composite laminates

Two simple and improved models - energy-balance and spring-mass - were developed to calculate impact force and duration during low velocity impact of circular composite plates. Both models include the contact deformation of the plate and the impactor as well as bending, transverse shear, and membrane deformations of the plate. The plate was transversely isotropic graphite/epoxy composite laminate and the impactor was a steel sphere. Calculated impact forces from the two analyses agreed with each other. The analyses were verified by comparing the results with reported test data.

Shivakumar, K. N.↗

NASA NTRS1984

The effect of cyclic loading on the stiffness degradation of angle-ply composite laminates

An experimental investigation has been conducted to determine the effect of cyclic loading on the stiffness degradation of composite laminates. Specimens were tested in tension-tension fatigue at a frequency of 10 Hz and a stress ratio of 0.1, over a wide range of stress levels. The laminate employed for this investigation was made of graphite/epoxy in an angle-ply (+ or - 35)2s orientation. During this investigation both static and dynamic stiffness reduction data were recorded during constant amplitude fatigue testing, and the results are presented in tabular and graphical form.

Jones, D. L.↗

NASA NTRS1985

Delamination and debonding of materials

The general topics consist of stress analysis, mechanical behavior, and fractography/NDI of composite laminates. Papers are presented on a dynamic hybrid finite-element analysis for interfacial cracks in composites, energy release rate during delamination crack growth in composite laminates, matrix deformation and fracture in graphite-reinforced epoxies, and the role of delamination and damage development on the strength of thick notched laminates. In addition, consideration is given to a new ply model for interlaminar stress analysis, a fracture mechanics approach for designing adhesively bonded joints, the analysis of local delaminations and their influence on composite laminate behavior, and moisture and temperature effects on the mixed-mode delamination fracture of unidirectional graphite/epoxy.

Johnson, W. S.↗

NASA NTRS1985

A fracture mechanics approach for designing adhesively bonded joints

An analytical and experimental investigation was undertaken to determine if the adhesive debond initiation stress could be predicted for arbitrary joint geometries. The analysis was based upon a threshold total strain-energy-release rate (Gth) concept. Two bonded systems were tested: T300/5208 graphite/epoxy adherends bonded with either EC-3445 or FM-300 adhesive. The Gth for each adhesive was determined from cracked-lap-shear (CLS) specimens by initiation tests. Finite-element analyses of various tapered CLS specimen geometries predicted the specimen stress at which the total strain-energy-release rate (GT) equaled Gth at the joint tip. Experiments verified the predictions. The approach described herein predicts the maximum stress at which an adhesive joint can be cycled yet not debond. Furthermore, total strain-energy-release rate appeared to be the driving parameter for cyclic debonding and debond initiation in structural adhesives. In addition, debond initiation and growth were found to occur with virtually no peel stress present.

Johnson, W. S.↗

NASA NTRS1986

Fracture of thick laminated composites

The fracture of thick laminated graphite/epoxy composites has been the subject of an extensive research program. The program was divided into three major areas of investigation which included laminate thickness, laminate stacking sequence, and part-through surface flaws. The results from this program are reviewed with emphasis placed on their applicability to the design of thick laminated composite structures.

Harris, C. E.↗

NASA NTRS1986

Prediction of the long-term creep compliance of general composite laminates

An accelerated viscoelastic characterization procedure for use with polymer-based composite materials is presented which employs short term test data obtained using unidirectional specimens to predict the long term viscoelastic behavior of general composite laminates. This procedure is here illustrated using the Schapery (1966, 1969) nonlinear theory as the required viscoelastic constitutive model, as well as classical lamination theory for the lamination scheme. The technique is applied to T300/5208 graphite/epoxy.

Tuttle, M. E.↗

NASA NTRS1986

Influence of interface ply orientation on fatigue damage of adhesively bonded composite joints

An experimental study of cracked-lap-shear specimens was conducted to determine the influence of adherend stacking sequence on debond initiation and damage growth in a composite-to-composite bonded joint. Specimens consisted of quasi-isotropic graphite/epoxy adherends bonded together with either FM-300 or EC 3445 adhesives. The stacking sequence of the adherends was varied such that 0 deg, 45 deg, or 90 deg plies were present at the adherend-adhesive interfaces. Fatigue damage initiated in the adhesive layer in those specimens with 0 deg and 45 deg interface plies. Damaage initiated in the form of ply cracking in the strap adherend for the specimens with 90 deg interface plies. The fatigue-damage growth was in the form of delamination within the composite adherends for specimens with the 90 deg and 45 deg plies next to the adhesive, while debonding in the adhesive resulted for the specimens with 0 deg plies next to the adhesive. Those joints with the 0 deg and 45 deg plies next to either adhesive has essentially the same fatigue-damage-initiation stress levels. These stress levels were 13 and 71 percent higher, respectively, than those for specimens with 90 deg plies next to the EC 3445 and FM-300 adhesives.

Johnson, W. S.↗

NASA NTRS1985

Deformation and failure of transversely loaded composite plates

Quasi-isotropic graphite/epoxy clamped circular plates were loaded under control point loading. Deflections and strains at various locations were monitored up to failure. Various damage mechanisms, such as intralaminar matrix cracking, delaminations and fiber breaks, are correlated with the strain records. The damage at various stages of deformation was characterized by means of X-radiography. Results are compared with an approximate isotropic plate theory.

Daniel, I. M.↗

NASA NTRS1985

Interaction of mixed mode loading on cyclic debonding in adhesively bonded composite joints

A combined experimental and analytical investigation of an adhesively-bonded composite joint was conducted to characterize the fracture mode dependence of cyclic debonding. The system studied consisted of graphite/epoxy adherends bonded with EC 3445 adhesive. Several types of specimens are tested which provide the cyclic debond growth rate measurements under various load conditions: mode 1, mixed mode 1 to 2, and mostly mode 2. This study shows that the total strain-energy-release rate is the governing factor for cyclic debonding.

Mall, S.↗

NASA NTRS1986

Hybrid deployable/erectable solar dynamic box truss system

The design of a hybrid deployable/erectable solar dynamic box truss power generation system for the initial operation capability (IOC) of the Space Shuttle is examined. An organic Rankine cycle heat engine for IOC solar power generation is studied. The design configuration is a simple parabolic concentration where the receiver is located in the focal plane with its aperture at the focal point. The relationship between concentrator size and collection efficiency is analyzed. The geometry of the deployable graphite/epoxy box truss ring and the reflective panels of the system are described. Mass properties and dynamic analyses are performed to evaluate the center of gravity location and moments of inertia characteristics of the energy conversion subsystem (ECS). The deployable/erectable truss is applicable for large IR space telescopes and center and offset fed ECSs.

Coyner, J. V., Jr.↗

NASA NTRS1986

Postbuckling behavior of longitudinally compressed orthotropic plates with three-dimensional flexibility

Postbuckling results for the average longitudinal compressive stress vs applied displacement are obtained for aluminum (isotropic), aluminum/epoxy (quasi-isotropic), and 45-deg graphite/epoxy (orthotropic) plates using classical (Kirchhoff) and conventional transverse shearing theories. An analysis of the results obtained shows that, in the postbuckling range, the classical theory cannot provide reasonably accurate results even for thin plates.

Stein, M.↗

NASA NTRS1986

Effect of laminate thickness and specimen configuration on the fracture of laminated composites

Attention is given to the effect of laminate thickness on graphite/epoxy laminates in the present measurements of fracture toughness in center cracked tension specimens, compact tension specimens, and three-point bend specimens. Crack tip damage development prior to fracture is also studied. The results obtained show fracture toughness to be a function of laminate thickness, being in all cases independent of crack size. The fracture surface of all thick laminates was uniform in the interior and self-similar with the starter notch. With only one exception, the fracture toughness of the thicker laminates was relatively independent of specimen configuration.

Harris, C. E.↗

NASA NTRS1986

Characterization of mode I and mixed-mode failure of adhesive bonds between composite adherends

A combined experimental and analytical investigation of an adhesively bonded composite joint was conducted to characterize both the static and fatigue beyond growth mechanism under mode 1 and mixed-mode 1 and 2 loadings. Two bonded systems were studied: graphite/epoxy adherends bonded with EC 3445 and FM-300 adhesives. For each bonded system, two specimen types were tested: a double-cantilever-beam specimen for mode 1 loading and a cracked-lapshear specimen for mixed-mode 1 and 2 loading. In all specimens tested, failure occurred in the form of debond growth. Debonding always occurred in a cohesive manner with EC 3445 adhesive. The FM-300 adhesive debonded in a cohesive manner under mixed-mode 1 and 2 loading, but in a cohesive, adhesive, or combined cohesive and adhesive manner under mode 1 loading. Total strain-energy release rate appeared to be the driving parameter for debond growth under static and fatigue loadings.

Mall, S.↗

NASA NTRS1986

A comparison of the fracture behavior of thick laminated composites utilizing compact tension, three-point bend, and center-cracked tension specimens

An experimental study of the effects of specimen configuration and laminate thickness on the fracture behavior of notched laminated composites is presented. The behavior of (0/+, 45/90)ns, (0/90)ns and (0/+, - 45)ns graphite/epoxy T300/5208 laminates was studied. When fracture toughness was computed at the failing load of the center-cracked tension specimen, laminate thickness significantly influenced fracture toughness. If fracture toughness was computed at the interception of the 5 percent secant line with the load-COD record, fracture toughness was found to be independent of both laminate thickness and specimen configuration. Defined in this manner, fracture toughness can be physically interpreted as an indicator of the onset of significant notch-tip damage.

Harris, C. E.↗

NASA NTRS1986

Deformation and damage of composite plates under impact loading

Transient deformation and damage were studied in impacted graphite/epoxy plates. The plates were 8-ply and 16-ply quasi-isotropic laminates clamped around a 12.7 cm diameter circumference. They were instrumented with surface and embedded strain gages and loaded by a 202 gr mass dropped from a height of 1.8 m. The load history and imparted energy were obtained by means of an accelerometer attached to the impactor. Transient strains at various locations through the thickness and at various distances from the loading point were obtained. The characteristic features of the strain records are associated with specific failure modes in the laminate. The deformation history was also correlated with the induced damage as detected by X-radiography and ultrasonics. Impact damage is more extensive in the thicker laminate. Damage takes the form of delaminated strips parallel to the fiber direction in each ply and increasing in length from top to bottom.

Daniel, I. M.↗