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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 577 records · Page 32
All sourcesNASA NTRSDOE OSTI
DOE OSTI2021

X-ray free electron laser heating of water and gold at high static pressure

Probing of reactive materials such as H 2 O ices and fluids at the high pressures and temperatures of planetary interiors is limited by unwanted chemical reactions and confinement failure. Faster experiments can mitigate such issues, but the common approach of adiabatic compression limits the conditions achieved. This study demonstrates a fast experimental strategy for the creation and probing of selected extreme states using static compression coupled with ultrafast X-ray laser heating. Indirect X-ray heating of H 2 O through the use of a gold absorber is evidenced by sample melting inferred from textural changes in the H 2 O diffraction lines and inter-dispersion of gold and H 2 O melts. Coupled with numerical analysis of femtosecond energy absorption, thermal equilibration, and heat transfer, all evidence indicates that temperatures in excess of an electron volt have been reached in the H 2 O at high pressure. Even after repeated heating, samples stayed chemically unchanged from the starting material.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
NASA NTRS1973

The X-ray structure of the Vela X region observed from Uhuru.

The X-ray source 2U 0832-45 in the Vela X region is centered on the pulsar PSR 0833-45 and is less than 1.2 deg in extent. Weak X-ray emission is seen from two other localized regions within the radio complex, but the diffuse emission of the Vela X-ray nebula seen below 2 keV is not detected in the Uhuru energy range. We consider it likely that the X-ray source at the pulsar is being excited by the rotational energy loss of the pulsar.

Kellogg, E.↗
NASA NTRS1995

A search for an X-ray scattering halo around Scorpius X-1

Results are presented of an experiment to detect the presence of X-ray scattering by interstellar dust grains in the form of a halo around Sco X-1. We utilize te principle that X-ray scattering off an optical is reduced by 1/sin theta for reflections out of the plane of incidence, thus reducing instrumental scattering off our moderate quality (1 arcminute) X-ray optic. We find an upper limit X-ray flux from Sco X-1 in the form of a halo at a mean energy of 0.69 keV of 7.6% of the point source flux at the 1 sigma confidence level. From this we derive an upper limit of E(B-V) = 0.12 towards Sco X-1. This is about half the value (E(B-V) approximately 0.3) derived toward Sco X-1 using the 2200 A interstellar absorption feature, indicating probable circumstellar origin to the 2200 A feature.

Gallagher, Dennis↗
NASA NTRS1979

A high-sensitivity X-ray survey using the Einstein Observatory and the discrete source contribution to the extragalactic X-ray background

Surveys of two fields have been carried out utilizing the X-ray imaging instruments of the Einstein Observatory to a limiting flux of 1.3 x 10 to the -14th ergs/sq cm s in the 1-3 keV band, a several hundred-fold increase in sensitivity with respect to previous surveys. Forty-three objects are observed with positional accuracies varying from 5 to 60 arcsec. Optical and radio studies of candidate counterparts are described. The number-intensity relationship for extragalactic sources is evaluated, and the consequences of the findings are discussed with particular emphasis on the discrete source contribution to the extragalactic X-ray background. It is concluded that a large fraction of the background is due to previously unresolved discrete sources.

Giacconi, R.↗
NASA NTRS1978

Observation of X-ray eclipses from LMC X-4

Observations made with the Rotation Modulation Collimator system (RMC) have revealed that X-ray source X-4 in the Large Magellanic Cloud (LMC X-4) is most likely part of a binary system. An analysis of the star's coordinates is presented, with attention given to orbital period and flux intensity variations. Stellar mass and orbital inclination angle are estimated for both X-4 and its companion star.

Li, F.↗
NASA NTRS2003

X-Ray Diffraction and Imaging Study of Imperfections of Crystallized Lysozyme with Coherent X-Rays

Phase-sensitive x-ray diffraction imaging and high angular-resolution diffraction combined with phase contrast radiographic imaging are employed to characterize defects and perfection of a uniformly grown tetragonal lysozyme crystal in symmetric Laue case. The fill width at half-maximum (FWHM) of a 4 4 0 rocking curve measured from the original crystal is approximately 16.7 arcseconds, and defects, which include point defects, line defects, and microscopic domains, have been clearly observed in the diffraction images of the crystal. The observed line defects carry distinct dislocation features running approximately along the <110> growth front, and they have been found to originate mostly at a central growth area and occasionally at outer growth regions. Individual point defects trapped at a crystal nucleus are resolved in the images of high sensitivity to defects. Slow dehydration has led to the broadening of the 4 4 0 rocking curve by a factor of approximately 2.4. A significant change of the defect structure and configuration with drying has been revealed, which suggests the dehydration induced migration and evolution of dislocations and lattice rearrangements to reduce overall strain energy. The sufficient details of the observed defects shed light upon perfection, nucleation and growth, and properties of protein crystals.

Hu, Zheng-Wei↗
DOE OSTI2024

Theoretical and experimental analysis of the modulated phase grating X-ray interferometer

X-ray grating interferometry allows for the simultaneous acquisition of attenuation, differential-phase contrast, and dark-field images, resulting from X-ray attenuation, refraction, and small-angle scattering, respectively. The modulated phase grating (MPG) interferometer is a recently developed grating interferometry system capable of generating a directly resolvable interference pattern using a relatively large period grating envelope function that is sampled at a pitch that is small enough that X-ray spatial coherence can be achieved by using a microfocus X-ray source or G0 grating. We present the theory of the MPG interferometry system for a 2-dimensional staggered grating, derived using Fourier optics, and we compare the theoretical predictions with experiments we have performed with a microfocus X-ray system at Pennington Biomedical Research Center, LSU. The theoretical and experimental fringe visibility is evaluated as a function of grating-to-detector distance. Additionally, quantitative experiments are performed with porous carbon and alumina compounds, and the mean normalized dark-field signal is compared with independent porosimetry measurements. Qualitative analysis of attenuation and dark-field images of a dried anchovy are shown.

47 OTHER INSTRUMENTATION↗
NASA NTRS1985

Energy dispersive X-ray diffraction in the diamond anvil, high-pressure apparatus - Comparison of synchrotron and conventional X-ray sources

The use of both conventional fixed-anode X-ray sources and synchrotron radiation to carry out energy-dispersive X-ray diffraction experiments at high pressure in a diamond anvil cell, is discussed. The photon flux at the sample and at the detector for the two cases are compared and the results are presented in graphs. It is shown that synchrotron radiation experiments can be performed with nearly two orders of magnitude increase in data rate if superior detectors and detector electronics are available.

Spain, I. L.↗
NASA NTRS1980

Implications of cyclotron features in the X-ray spectrum of Hercules X-1

The modification of physical processes due to an intense magnetic field is investigated in order to uncover implications for X-ray spectra from binary pulsars. It is found that for large enough fields, the quantum nature of electron orbits must be taken into account, and for densities typical of binary X-ray pulsars it is found that electrons spend most of their time in the ground state. For this case, the production of cyclotron line photons following collisional excitation is estimated and the effects of the transfer of line photons through the hot plasma are considered. A line feature as narrow as reported by Truemper et al. appears unlikely. However, more recent observations allow a much broader line; in addition, a consistent absorption feature due to knock-on electrons may explain the spectral steepening at about 20 keV.

Bussard, R. W.↗
DOE OSTI2021

Robotic sample changers for macromolecular X-ray crystallography and biological small-angle X-ray scattering at the National Synchrotron Light Source II

In this work, we present two robotic sample changers integrated into the experimental stations for the macromolecular crystallography (MX) beamlines AMX and FMX, and the biological small-angle scattering (bioSAXS) beamline LiX. They enable fully automated unattended data collection and remote access to the beamlines. The system designs incorporate high-throughput, versatility, high-capacity, resource sharing and robustness. All systems are centered around a six-axis industrial robotic arm coupled with a force torque sensor and in-house end effectors (grippers). They have the same software architecture and the facility standard EPICS-based BEAST alarm system. The MX system is compatible with SPINE bases and Unipucks. It comprises a liquid nitrogen dewar holding 384 samples (24 Unipucks) and a stay-cold gripper, and utilizes machine vision software to track the sample during operations and to calculate the final mount position on the goniometer. The bioSAXS system has an in-house engineered sample storage unit that can hold up to 360 samples (20 sample holders) which keeps samples at a user-set temperature (277 K to 300 K). The MX systems were deployed in early 2017 and the bioSAXS system in early 2019.

36 MATERIALS SCIENCE↗
DOE OSTI2022

Atomic-Site-Specific Surface Valence-Band Structure from X-Ray Standing-Wave Excited Photoemission

X-ray standing-wave (XSW) excited photoelectron emission was used to measure the site-specific valence band (VB) for ½ monolayer (ML) Pt grown on a SrTiO 3 (001) surface. The XSW induced modulations in the core level (CL), and VB photoemission from the surface and substrate atoms were monitored for three ℎ⁡kl substrate Bragg reflections. The XSW CL analysis shows the Pt to have a face-centered-cubic-like cube-on-cube epitaxy with the substrate. The XSW VB information compares well to a density functional theory calculated projected density of states from the surface and substrate atoms. Altogether, this Letter represents a novel method for determining the contribution to the density of states by valence electrons from specific atomic surface sites.

74 ATOMIC AND MOLECULAR PHYSICS↗
NASA NTRS1966

X-ray emission from Sco x-1.

X-ray emission from Scorpio X-1, discussing origin of extar and possible role in stellar evolution

SCORPIO CONSTELLATION↗
NASA NTRS1983

The detection of X rays from Jupiter

X rays in the energy band 0.2-3.0 keV have been detected coming from both polar regions of Jupiter. The observations were made in 1979 and 1981 by using the imaging proportional counter and high resolution imaging detectors on the Einstein X-ray astronomy satellite. The measured flux density of approximately 0.0006/sq cm-sec at earth corresponds to an X ray luminosity of approximately 4 x 10 to the 9th W in the 0.2- to 3.0-keV energy band. The energy spectrum of the X rays is extremely soft and can be characterized by a power law with an exponent of approximately 2.3. Detector energy resolution is insufficient to distinguish a soft line spectrum from a continuum. However, the shape of the response and the observed X ray power indicate that the source of this auroral emission is not electron bremsstrahlung as on the earth, but is most probably line emission from O and S ions with energies between 0.03 and 4.0 MeV/nucleon precipitating from the outer boundary of the Io plasma torus at L approximately 8.

Metzger, A. E.↗
NASA NTRS1973

Long-term X-ray observations of Scorpius X-1 by OSO-III.

Review of the observations of Scorpius X-1 in the energy range 7.7-22 keV provided by the X-ray telescope on the OSO-III satellite over the period from May 19 to June 13, 1967. Optical observations representative of the full range of temporal behavior of the source are available on 10 nights during this period. Sco X-1, in spite of being the most extensively observed X-ray source, remains one of the least understood. Coordinated observations in various wavelength bands, although inconclusive so far, represent potentially the most fruitful approach.

Pelling, R. M.↗
NASA NTRS1992

The structure of the coronal soft X-ray source associated with the dark filament disappearance of 1991 September 28 using the Yohkoh Soft X-ray Telescope

The structure of the coronal soft X-ray source associated with the dark filament disappearance on September 28, 1991, observed with the Soft X-ray Telescope, is examined as a possible example of the 'eruption-reconnection' model of filament disappearance. The results suggest, however, that this model may not fit. There is a strong possibility that much of the dark filament mass remains in the heated unwinding axial field.

Mcallister, Alan↗
NASA NTRS1995

The average X-ray/gamma-ray spectra of Seyfert galaxies from Ginga and OSSE and the origin of the cosmic X-ray background

We have obtained the first average 2-500 keV spectra of Seyfert galaxies, using the data from Ginga and Compton Gamma-Ray Observatory's (CGRO) Oriented Scintillation Spectrometer Experiment (OSSE). Our sample contains three classes of objects with markedly different spectra: radio-quiet Seyfert 1's and 2's, and radio-loud Seyfert 1's. The average radio-quiet Seyfert 1 spectrum is well-fitted by a power law continuum with the energy spectral index alpha approximately equals 0.9, a Compton reflection component corresponding to a approximately 2 pi covering solid angle, and ionized absorption. There is a high-energy cutoff in the incident power law continuum: the e-folding energy is E(sub c) approximately equals 0.6(sup +0.8 sub -0.3) MeV. The simplest model that describes this spectrum is Comptonization in a relativistic optically-thin thermal corona above the surface of an accretion disk. Radio-quiet Seyfert 2's show strong netural absorption, and there is an indication that their X-ray power laws are intrinsically harder. Finally, the radio-loud Seyfert spectrum has alpha approximately equals 0.7, moderate neutral absorption E(sub C) = 0.4(sup +0.7 sub -0.2) MeV, and no or little Compton reflection. This is incompatible with the radio-quiet Seyfert 1 spectrum, and probably indicating that the X-rays are beamed away from the accretion disk in these objects. The average spectra of Seyferts integrated over redshift with a power-law evolution can explain the hard X-ray spectrum of the cosmic background.

Zdziarski, Andrzej A.↗
NASA NTRS1979

Extended-bandwidth X-ray observations of Cygnus X-1

An energy- and time-resolved observation of Cyg X-1, sensitive from 0.15 to 20 keV, is reported which was performed to investigate the spectrum and time variability of the flux at low X-ray energies. Data in the band from 1.5 to 42 keV, obtained in two previous rocket flights, are reanalyzed to search for any energy dependence of the time signature. No such energy dependence is found, so the explanation of the observed low-energy excess of Cyg X-1 as emission from an extended region separate from the high-energy source is rendered untenable. The evident stability of the power-law spectrum of Cyg X-1 through the observed shot-noise variation is shown to suggest that the spectrum has a Comptonization origin. It is concluded that there is no obvious analogy to be made between Cyg X-1 and X-ray bursters.

Priedhorsky, W.↗