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At least 577 records · Page 32

Machine finishes balls to high degree of roundness

Machine was developed to finish ball to roundness within 12.5 nm (half a microinch) from any types of hard material. Grinding and polishing to this tolerance is accomplished by lapping elements on four to six motor-driven spindles. Spindles are adjustably spring-loaded to ensure constant contact pressure on ball and are driven by variable speed electric motors.

Angele, W.↗

Experiment S010: Agena micrometeorite collection

A study was made of the micrometeoroid content of the upper atmosphere and the near-earth space environment. Highly polished collection surfaces attached to the target docking adapter (TDA) were exposed to micrometeorite impact and debris collection during the Gemini 8, 9, and 10 missions. Also, the device was attached to the Gemini Agena target vehicle (GATV) during the Gemini 12 mission. The effects of space environment exposure on viable microorganisms were recorded. No substantive data regarding space environment micrometeorite content were derived from the Gemini 9 or 12 missions. However, some substantive data were obtained from the experiment package that was retrieved from the Gemini 10 mission. The micrometeorite-flux values obtained were in general agreement with values obtained from previous experiments by the use of other experimental equipment. The microorganisms that were retrieved from the Gemini 10 experiment package did not survive. However, the same kinds of specimens inside the package had good survival rates. Upon initial analysis, it appeared that the closed-cover shielding was a contributing factor in the protection and survival of the microorganisms.

Hemenway, C. L.↗

Experiment S012: Micrometeorite collection

The micrometeorite activity in a near-earth environment and the effect of the environment on microorganisms were studied by exposure of polished metal and plastic surfaces to the environment outside the Gemini spacecraft. Preliminary results are summarized as follows: (1) The cumulative influx rate in the size ranges from 10 to the minus 15th power to 10 to the minus 14th power gram was approximately 2 particles/ sq m/sec, as determined on the Gemini 12 mission; (2) The cumulative influx rate in the same mass range, as determined by the data from the Gemini 9 mission was almost 200 particles/ sq m/sec; and (3) The large particle cumulative influx rate was about 3 x 0.00001 particle/ sq m/sec, with a mass of the order of 10 to the minus 7th power gram. No living organisms could be found on the sterile collecting surfaces after recovery and handling.

Hemenway, C. L.↗

Distribution of Apollo 15 lunar samples: News release

More than 2200 Apollo 15 samples and polished thin sections weighing a total of about three kilograms will be distributed to 201 principal investigators for study during the next year. The scientific investigations will provide detailed information on the samples' mineralogy, petrology, chemistry, age, and history and on the effects of micrometeorite impacts, solar radiation, and cosmic ray bombardment. Preliminary examination of samples show the Apollo 15 material to be of three types: dark colored iron-rich basalts associated with mare and rille formation; a few basalts enriched in feldspar collected near the Apennine front; and light colored fragmental rocks or breccias consisting of soil-like materials which were cemented together or of rock fragments which were welded together by partial remelting.

Dick, L.↗

Meteoroid activity on the lunar surface from the Surveyor 3 sample examination

The Surveyor 3 television camera shroud and polished aluminum tube, retrieved as a result of the Apollo 12 mission after 2-1/2 years on the lunar surface, were examined at the NASA Manned Spacecraft Center for evidence of meteoroid impact. The results of this examination were compared with other estimates of the meteoroid flux in the lunar vicinity and are shown to be in good agreement with the Lunar Orbiter penetration rates. In addition, the relationship between a derived lunar surface meteoroid cumulative-flux model and the comparable near-earth model is discussed in the light of theoretical predictions. It is shown that the effect of the gravitational field of the earth on the near-earth environment was greater than previously predicted. The implication is that the average meteoroid velocity relative to the earth is probably 17 km/s. The many low velocity impacts on the Surveyor 3 camera and tube are shown to be of lunar surface origin and to be primarily the result of rocket exhaust interaction.

Cour-Palais, B. G.↗

Ion microprobe mass analysis of lunar samples. Lunar sample program

Mass analyses of selected minerals, glasses and soil particles of lunar, meteoritic and terrestrial rocks have been made with the ion microprobe mass analyzer. Major, minor and trace element concentrations have been determined in situ in major and accessory mineral phases in polished rock thin sections. The Pb isotope ratios have been measured in U and Th bearing accessory minerals to yield radiometric age dates and heavy volatile elements have been sought on the surfaces of free particles from Apollo soil samples.

Anderson, C. A.↗

Infrared and Raman spectroscopic studies of structural variations in minerals from Apollo 11, 12, 14 and 15 samples, volume 3

Infrared and Raman vibrational spectroscopic data, yielding direct information on molecular structure, were obtained for single grains ( 150 microns) of minerals, basalts, and glasses isolated from Apollo 11, 12, 14, and 15 rock and dust samples, and for grains in Apollo 14 polished butt samples. From the vibrational data, specification substitutions were determined for the predominant silicate minerals of plagioclase, pyroxene, and olivine. Unique spectral variations for grains of K-feldspar, orthopyroxene, pyroxenoid, and ilmenite were observed to exceed the ranges of terrestrial samples, and these variations may be correlatable with formation histories. Alpha-quartz was isolated as pure single grains, in granitic grains composited with sanidine, and in unique grains that were intimately mixed with varying amounts of glass. Accessory minerals of chromite and ulvospinel were isolated as pure grains and structurally characterized from their distinctive infrared spectra. Fundamental vibrations of the SiO4 tetrahedra in silicate minerals were used to classify bulk compositions in dust sieved fractions, basalt grains and glass particles, and to compare modal characteristics for maria, highland and rille samples. No hydrated minerals were found in any of the samples studied, indicating anhydrous formation conditions.

Estep, P. A.↗

Surface studies on Surveyor 3 tubing sections

Sections C and E of the unpainted, polished aluminum tubing from the strut of the radar altimeter and Doppler velocity sensor were examined in a transmission electron microscope for micrometeorite damage and ion bombardment. Both sections were contaminated and eroded on one side; it is suggested that these conditions were caused by sandblasting by lunar dust and retrorocket plume contamination during Surveyor 3 landing. Microcraters of different configurations were found on the bright sides of the tubes. Several degrees of violence were involved in the formation of the craters, and the particle size could be responsible for some differences. All micropits found were on the bright areas and data indicate 0.2 hypervelocity impact/sq cm and 2/sq cm for other types of craters. The greatest degree of damage resulted from particle impact and was limited to a maximum depth of 2 microns.

Buvinger, E. A.↗

Results of examination of the returned Surveyor 3 samples for particulate impacts

The television housing and a section of the strut of the radar altimeter and Doppler velocity sensor were examined optically and with a scanning electron microscope for particulate impacts. The white surface of the camera was discolored during the months the Surveyor 3 was on the moon; however, most of the craters must have occurred as a result of lunar dust sandblasted by the LM exhaust. The polished section of the strut exhibits contamination which appears brown and seems to be partially composed of crystals. Electron microscopic analysis of the strut section indicated no craters of hypervelocity impact origin, confirmed pitting density results of the optical scans, and indicated that material in the craters is of lunar origin. No meteorite impacts larger than 25 microns were detected on the tubing section.

Cour-Palais, B. G.↗

Lubrication with sputtered MoS2 films.

Sputtered MoS2 films (2000-6500 A) were deposited on highly polished metal surfaces. These films have a low coefficient of friction (0.03-0.04) at speeds of 40-80 rpm and loads of 250-1000 grams. At loads of 250 grams the wear lives are over 0.5 million cycles, but at 1000 gram loads, it decreases to 38,000 cycles. Friction experiments and tensile tests have indicated that sputtered films have a strong adherence to metal surfaces. Electron transmission, diffraction and scanning electron microscopy show that these films have an extremely small particle size, less than 30 A in diameter, and are very dense and free from observable pinholes. The high kinetic energy of these sputtered species, the submicroscopic particle size and the sputter-etched substrate surface is responsible for strong adhesion and cohesion of the sputtered film.

Spalvins, T.↗

Mechanism of the oxidation of titanium disilicide.

Study of the oxidation of TiSi2 at temperatures of 300 to 1300 C. Wafers prepared using the techniques of powder metallurgy had densities of 95 to 98% of the theoretical value. On oxidation at temperatures up to 600 C, the polished wafers formed a protective, titania-silica glass. The rate data indicate a complex surface and diffusion-limited mechanism. Above 600 deg C, the oxide consisted of an amorphous SiO2 film with crystalline islands of TiO2 (rutile). From 1000 to 1300 C, parabolic kinetics with an activation energy of 21.3 kcal/mole were observed. These data are consistent with a model in which the rate-determining step is the diffusion of oxygen through the silica film with the simultaneous diffusion of titanium from the substrate to the islands of rutile growing on top of the amorphous silica.

Schwettmann, F. N.↗

Lubrication with sputtered MoS2 films.

Sputtered MoS2 films (2000-6500 A) were deposited on highly polished metal surfaces. These films have a low coefficient of friction (0.03-0.04) at speeds of 40-80 rpm and loads of 250-1000 grams. At loads of 250 grams, the wear lives are over 0.5 million cycles, but at 1000 gram loads, it decreases to 38,000 cycles. Friction experiments and tensile tests have indicated that sputtered films have a strong adherence to metal surfaces. Electron transmission, diffraction, and scanning electron microscopy show that these films have an extremely small particle size less than 30 A in diameter and are very dense and free from observable pinholes.

Spalvins, T.↗

Detection of fiber cracking by acoustic emission.

A theoretical model is presented that relates acoustic emission to fiber cracking which occurs during a rising load tension test on a fiber reinforced composite. The percentage of broken fibers in an Al3Ni fiber reinforced aluminum was measured as a function of tensile strain by optical inspection of the polished surface of strained specimens. This information was used in conjunction with the proposed model to predict the acoustic emission response of the composite material. These predictions were compared with experimental observations, and a good agreement was obtained between the two sets of results. These results indicate that it is possible to relate acoustic emission quantitatively to the micromechanics of the deformation processes occurring within fiber reinforced composites, thereby demonstrating the applicability of acoustic emission to materials studies and also to nondestructive evaluation of the integrity of composite materials.

Harris, D. O.↗