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DOE OSTI2024

Advanced Instrumentation for Metal Additive Manufacturing

Laser powder bed fusion (LPBF) is the most widely used process for metal additive manufacturing (AM), particularly where complex geometries provide performance advantages unattainable with traditional manufacturing techniques. However, LPBF is highly sensitive to innate variability in both the powder spreading and fusion steps, often leading to defects such as pores that are difficult to detect yet significantly impair component mechanical properties and fatigue life. This thesis presents a range of novel instruments enabling both precise assessment of powder layer characteristics and in-situ thermal metrology of metal AM to advance the quality control of LPBF. First, leveraging a custom X-ray microscope and a radiation-transport model developed through this work, transmission X-ray imaging is used to study spreading of thin metal powder layers. Effective layer depth is directly mapped at a process-relevant size scale, surpassing optical techniques that can only estimate local deposition from layer surface topography. Layer packing density and quality are shown to be influenced by powder flowability and particle size relative to nominal powder layer thickness. Layer quality is additionally connected to the geometry of the spreading implement and its velocity. This technique and its presented findings enable pairing feedstocks with spreading strategies that create layers with consistent packing density and uniformity. Second, a twofold approach is employed to optically interrogate the laser fusion step of LPBF for observing signatures of defect formation. Aperture division multiplexing is conceptualized, providing for simultaneous laser delivery and high-fidelity infrared (IR) process monitoring through a common optic. In-situ microscopy at 50 μm spatial resolution and at mid-wave IR wavelengths is proven readily achievable with the first purpose-built optic of this type. Next, a bespoke imaging spectrometer, along with a temperature-emissivity separation technique, is used to retrieve accurate process temperatures over a 1000 K range. Data from these instruments are correlated to porosity as fine as 4.3 μm in two LPBF test artifacts, as verified using computed tomography (CT), establishing the viability of robust optically-based component qualification.

Penny, Ryan↗

NASA NTRSDate not supplied

Calibration and Validation of the SHERLOC Instrument Operating in Jezero Crater, Mars

The Scanning Habitable Environments with Raman and Luminescence for Organics and Chemistry (SHERLOC) is an instrument onboard the Mars 2020 Perseverance rover. It consists of a spectrometer that measures deep ultraviolet (DUV) resonance Raman and native fluorescence photons generated through surface interactions with a 248.6 nm pulsed laser. Two microscopic imagers, the Autofocus Context Imager (ACI) and the Wide-Angle Topographic Sensor for Operations and eNgineering (WATSON), provide high-resolution context images of SHERLOC targets. The ACI is co-boresighted with the spectrometer. To ensure proper calibration, the SHERLOC calibration target (SCT) is mounted on the front of the rover and consists of ten different materials. The SCT was designed, fabricated, assembled, and tested by Jacobs Technology, Inc., and NASA Johnson Space Center. The dimensions of the calibration target housing are 150 x 89 x 33 mm and it weighs ~437 g. The ten targets are arranged in two rows; the first six are hard targets (AlGaN for Raman and fluorescence, diffuse transmission target, a slice of the SaU008 Mars meteorite, an intensity maze, and polycarbonate over geocache coin) and the remaining four are soft-goods targets (Vectran, Ortho-Fabric, Teflon, and nGimat-coated Teflon). The hard targets calibrate the spectrometer’s Raman and fluorescence spectral accuracy, ambient light reflection, and Raman response curve, while the soft-goods targets are spacesuit materials that function as human exploration targets, some of which are also used for spectral calibration. SHERLOC also has an internal calibration target consisting of AlGaN on sapphire (275 nm) located inside the ACI opaque dust cover to ensure proper instrument functioning between calibration target analyses. Initial SHERLOC, ACI, and WATSON calibration and validation on Mars was performed using the internal calibration target on sols 59, 83, 98, and 141; WATSON imaging of the SCT on sols 26 and 62, and SHERLOC spectroscopy and ACI imaging of the SCT on sol 59. These early data provide initial insights into instrument performance and the stability and degradation of the calibration target materials relative to the Martian surface and dust environment. Early observations also have implications for future astronaut spacesuit materials.

Trevor G Graff↗

DOE OSTI2020

A Replacement Cold Neutron Guide System for HFIR (Conceptual Design Report)

The design of a replacement cold neutron guide system for the High Flux Isotope Reactor (HFIR) is presented. The proposed six-channel design uses the latest technologies and is optimally designed to account for operational and site constraints. These include the design of the cold source and the beam tube, the size and shape of the penetrations in the reactor confinement boundary, and the shape and orientation of the guide hall. The existing user instruments are a macromolecular diffractometer (IMAGINE), an IMAGING station, two small-angle neutron scattering (SANS) instruments (Bio-SANS and GP-SANS), and a cold triple-axis spectrometer (C-TAX). These instruments will all be reinstalled at end-of-guide positions with improved performance, and a position for a new high-performance neutron spin echo instrument will be created. The proposed guide design requires an extension to the guide hall toward the south. The calculated flux gain for a typical experiment is between a factor of 1.3 and 3 for all instruments, with the exception of the C-TAX instrument, which stands to gain a factor of >30 in flux at the sample. The new guide system will also offer additional performance gains, such as an increase in Q-range on Bio-SANS. The stated performance gains do not take into account any potential performance gains resulting from renewal and realignment of the guide system. The design of the guide system in the common sections up to about 25 m from the source is considered to be complete and ready for engineering design, while the designs of the instrument-specific guides are in some cases still a work in progress. The present report describes the current status of those designs.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

NASA NTRS1985

Quantitative analysis of hard X-ray 'footpoint' flares observed by the solar maximum mission

Amplifier gain and collimator hole size variations across the field of view, amplifier/filter efficiency, variations in effective collimator hole size and angular response with photon energy, dead-time, and hard X-ray plate transmission, are among the factors for which instrumental corrections have to be incorporated to effect reliable correction and deconvolution of images from the SMM satellite's Hard X-ray Imaging Spectrometer (HXIS). Attention is given to the substantial Poisson noise in these energy bands. The maximum entropy deconvolution/correction routine developed for establishing the spatial structure reliably inferrable from HXIS data is presented, together with the results of the application of this routine to the three impulsive flares reported by Duijemian et al. (1982) from April 10, May 21, and November 5, 1980.

Mackinnon, A. L.↗

NASA NTRS1988

Mars Observer - Science

The scientific objectives and experiments planned for the Mars Observer mission are discussed. Scientific instruments for the mission are described and illustrated, including a gamma-ray spectrometer, a visual and IR mapping spectrometer, a thermal emission spectrometer, an imaging camera, a radar altimeter and radiometer, a magnetometer, and a pressure modulate IR radiometer. Mission objectives include studying the global elemental and mineralogical character of the Martian surface, defining the topography and gravitational field, studying the atmospheric circulation, and determining the time and space distribution, abundance sources, and sinks of volatile material and dust over a seasonal cycle.

Albee, Arden L.↗

NASA NTRS1991

Moderate Resolution Imaging Spectrometer (MODIS) design evolution and associated development and verification of data product efforts

The Moderate Resolution Imaging Spectrometer (MODIS) is a key observing facility to be flown on the Earth Observing System (EOS). The facility is composed of two instruments called MODIS-N (nadir) and MODIS-T (tilt). The MODIS-N is being built under contract to NASA by the Santa Barbara Research Center. The MODIS-T is being fabricated by the Engineering Directorate at the Goddard Space Flight Center. The MODIS Science Team has defined nearly 40 biogeophysical data products for studies of the ocean and land surface and properties of the atmosphere including clouds that can be expected to be produced from the MODIS instruments shortly after the launch of EOS. The ocean, land, atmosphere, and calibration groups of the MODIS Science Team are now proceeding to plan and implement the operations and facilities involving the analysis of data from existing spaceborne, airborne, and in-situ sensors required to develop and validate the algorithms that will produce the geophysical data products. These algorithm development and validation efforts will be accomplished wherever possible within the context of existing or planned national and international experiments or programs such as those in the World Climate Research Program.

Salomonson, Vincent V.↗

NASA NTRS1991

Recovery of reflectance from imaging spectrometer measured radiance using a radiative transfer code

Radiance data were acquired over part of the Clark Mountain Range, California in 1990 by the Airborne Visible Infrared Imaging Spectrometer (AVIRIS). From these calibrated radiance data, the lateral distribution of water vapor in precipitable mm was recovered through analysis of the 940 nm water absorption. Surface pressure height was calculated from the 760 nm oxygen absorption band in the AVIRIS data. Surface slopes are estimated from relative elevations derived from the equivalent water vapor elevation for a standard atmosphere. Atmospheric optical depths measured at the Mountain Pass site in these data are extended to the entire region and varied based on the calculated surface pressure elevation. These parameters, derived from every AVIRIS spatial element, are used to constrain the LOWTRAN 7 radiative transfer code for the recovery of surface reflectance. Once transformed to reflectance, the imaging spectrometer data may be analyzed quantitatively for determination of surface composition, and compared with reflectance measurements acquired from different locations, times, and instruments.

Green, Robert O.↗

NASA NTRS1997

GRIS detection of Al-26 1809 keV line emission from the Galactic center region as a broad line

The gamma ray imaging spectrometer (GRIS) was used to observe the 1809 keV emission from the Galactic center region. The observed line is broader than the instrument resolution. The measured intrinsic width is 5.4 +/- 1.4 keV full width half medium, which is more than three times the maximum Doppler broadening expected due to Galactic rotation. The detection of such a wide feature, suggesting a high dispersion velocity has implications for the origin of Galactic Al-26. It suggests a supernova explosion origin or a Wolf-Rayet stellar wind origin of Al-26. The fact that the Al-26 has not come to rest after 10(exp 6) years presents a challenge to the current understanding of the Al-26 production and propagation in the Galaxy.

Naya, Juan E.↗

NASA NTRS2012

Instrumentation and First Results of the Reflected Solar Demonstration System for the Climate Absolute Radiance and Refractivity Observatory

The Climate Absolute Radiance and Refractivity Observatory (CLARREO) mission key goals include enabling observation of high accuracy long-term climate change trends, use of these observations to test and improve climate forecasts, and calibration of operational and research sensors. The spaceborne instrument suites include a reflected solar spectroradiometer, emitted infrared spectroradiometer, and radio occultation receivers. The requirement for the RS instrument is that derived reflectance must be traceable to Sl standards with an absolute uncertainty of <0.3% and the error budget that achieves this requirement is described in previo1L5 work. This work describes the Solar/Lunar Absolute Reflectance Imaging Spectroradiometer (SOLARIS), a calibration demonstration system for RS instrument, and presents initial calibration and characterization methods and results. SOLARIS is an Offner spectrometer with two separate focal planes each with its own entrance aperture and grating covering spectral ranges of 320-640, 600-2300 nm over a full field-of-view of 10 degrees with 0.27 milliradian sampling. Results from laboratory measurements including use of integrating spheres, transfer radiometers and spectral standards combined with field-based solar and lunar acquisitions are presented. These results will be used to assess the accuracy and repeatability of the radiometric and spectral characteristics of SOLARIS, which will be presented against the sensor-level requirements addressed in the CLARREO RS instrument error budget.

McCorkel, Joel↗

NASA NTRS1994

Ultraviolet imaging and spectroscopy of planetary atmospheres

The main scientific results of the participation of the Institute of Astrophysics (Belgium) in the NASA's Pioneer Venus mission are reported on. The data were obtained with the Pioneer Orbiter's Ultraviolet Spectrometer (POUVS). The instrument provided a morphological study of the nitric oxide ultraviolet night glow. Information concerning the altitude of the airglow emitting layer was also collected and used to constrain models of turbulent transport on the night side of the planet. Models of the odd nitrogen thermospheric chemistry and transport were developed to analyze the observations and derive the properties of the global circulation of Venus' upper atmosphere. Images of the Jovian ultraviolet aurora were obtained. The morphology and the time variations of the HI Ly-alpha and H2 Lyman and Werner bands were acquired at different longitudes. The observed distribution was compared with the results of the spectrometric observations made with the Voyager and the International Ultraviolet Explorer missions. Images concerning the Io surface albedo and Saturn's disk and ring's reflectivity were also obtained.

Gerard, Jean-Claude↗

NASA NTRS2004

Upcoming and Future Missions in the Area of Infrared Astronomy: Spacecraft and Ground-based Observations

The IRIS instrument on the Voyager spacecrafts made major discoveries with regard to the giant planets, their moons and rings and paved the way for future infrared observations for planetary missions within our solar system. The CIRS instrument of Cassini with much greater spectral-spatial resolution and sensitivity than that provided by IRIS is now rapidly approaching the Saturnian system with orbit insertion on July 1, 2004, for which CIRS is expected to provide an order of magnitude advance beyond that provided by IRIS. The Mars program is also presently dominated by infrared observations in the near to mid-infrared spectral bands for missions such as Mars Global Surveyor and its TES instrument and Odyssey with its THEMIS instrument. In the case of Earth science we have such missions as TIMED, which makes infrared observations of the thermosphere using the SABER instrument. With the newly formed New Frontiers Program we have the opportunity for $650M missions such as Kuiper Belt-Pluto Explorer and Jupiter Polar Orbiter with Probes. Under the Flagship line, once per decade, we have the opportunity for $1B missions for which Europa is presently being considered; for this mission infrared measurements could look for hot spots within the maze of cracks and faults on Europa s surface. On Kuiper Belt- Pluto there is an imaging near-IR spectrometer called LEISA. Another mission on the horizon is Titan Orbiter Aerorover Mission (TOAM) for which there is planned a state-of-art version of CIRS called TIRS on the orbiter that will map out the atmospheric composition with unprecedented wavelength coverage and spectral-spatial resolution. This instrument will also provide temperature maps of the surface of Titan to look for hot spots where life may form. On the same mission there will be a descent imager on the Aerorover (i.e., balloon) similar to that provided by LEISA on the Pluto mission to provide compositional-topographical maps of Titan s surface. Other future mission will also be discussed. Improved thermal detectors could have important applications in solar physics, specifically in the detection of far-IR synchrotron emission from energetic electrons in solar flares. For infrared astronomy we have missions like SIRTF and JWST, which will cover the spectral range from near-IR to far-IR in the search and probing of both new and old planetary systems in our galaxy and the measurement of the most distant galaxies of our universe. SIRTF is scheduled to be launched in August 2003, while JWST will be launched next decade. Another mission is TPF, which will use interferometer techniques at infrared wavelengths to search for planetary systems beyond 2010. With regard to ground based telescopes we have, for example, the twin 10 meter Keck telescopes and the IRTF telescope at Mauna Kea. The Keck telescopes are presently using interferometer techniques. Over the next several decades there are plans for 50 meter to 200 meter telescopes providing near-IR to far-IR measurements with the eventual plan to combine all telescopes using interferometer techniques to provide unprecedented spectral-spatial resolution and sensitivity.

Sittler, E. C., Jr.↗

NASA NTRS2017

Ultra-Stable Spectrometer for Sky-Scanning, Sun-Tracking Atmospheric Research (5STAR)

The Spectrometer for Sky-Scanning, Sun-Tracking Atmospheric Research (4STAR) combines airborne sun tracking and sky scanning with diffraction spectroscopy to improve knowledge of atmospheric constituents and their links to airpollution and climate. Direct beam hyperspectral measurement of optical depth improves retrievals of gas constituentsand determination of aerosol properties. Sky scanning enhances retrievals of aerosol type and size distribution.Hyperspectral cloud-transmitted radiance measurements enable the retrieval of cloud properties from below clouds.These measurements tighten the closure between satellite and ground-based measurements. 4STAR incorporates amodular sun-tracking sky-scanning optical head with optical fiber signal transmission to rack mounted spectrometers,permitting miniaturization of the external optical tracking head, and future detector evolution.4STAR has supported a broad range of flight experiments since it was first flown in 2010. This experience provides thebasis for a series of improvements directed toward reducing measurement uncertainty and calibration complexity, andexpanding future measurement capabilities, to be incorporated into a new 5STAR instrument. A 9-channel photodioderadiometer with AERONET-matched bandpass filters will be incorporated to improve calibration stability. A wide dynamic range tracking camera will provide a high precision solar position tracking signal as well as an image of sky conditions around the solar axis. An ultrasonic window cleaning system design will be tested. A UV spectrometer tailored for formaldehyde and SO2 gas retrievals will be added to the spectrometer enclosure. Finally, expansion capability for a 4 channel polarized radiometer to measure the Stokes polarization vector of sky light will be incorporated. This paper presents initial progress on this next-generation 5STAR instrument.

atmosphere↗

NASA NTRS1993

Ultraviolet Imaging Spectrometer

Wide-field imaging systems equipped with objective prisms or gratings have had a long history of utility in groundbased observations of meteors and comets. Deployment of similar instruments from low Earth orbit would allow the first UV observations of meteors. This instrument can be used for comets and Lyman alpha coronae of Earth-orbit-crossing asteroids. A CaF2 prism imaging spectrograph designed for stellar observations was used aboard Skylab to observe Comet Kohoutek (1973f), but its 1300-A cut-off precluded Lyman alpha images and it was not used for observation of meteors. Because the observation of the UV spectrum of a meteor has never been attempted, researchers are denied the opportunity to obtain composition information from spectra at those wavelengths. We propose construction of a flight instrument functioning in the 1100-3200 A spectral range that is suitable for a dedicated satellite ('Quick Star') or as a space-station-attached payload. It can also be an autonomous package in the space shuttle cargo bay.

Wdowiak, T. J.↗

NASA NTRS2019

Machine Learning Approaches to Data Reduction from the MapX X-ray Fluorescence Instrument for Detection of Biosignatures and Habitable Planetary Environments

The search for evidence of life or its processes involves the detection of biosignatures suggestive of extinct or extant life, or the determination that an environment either has or once had the potential to harbor life. In situ elemental imaging is useful in either case, since features on the mm to μm scale reveal geological processes which may indicate past or present habitability. The Mapping X-ray Fluorescence Spectrometer (MapX) is an in-situ instrument designed to identify these features on planetary surfaces. Here we present progress on instrument development, data analysis methods, and element quantification.

Walroth, Richard C.↗

NASA NTRS1994

High-spatial-resolution passive microwave sounding systems

The principal contributions of this combined theoretical and experimental effort were to advance and demonstrate new and more accurate techniques for sounding atmospheric temperature, humidity, and precipitation profiles at millimeter wavelengths, and to improve the scientific basis for such soundings. Some of these techniques are being incorporated in both research and operational systems. Specific results include: (1) development of the MIT Microwave Temperature Sounder (MTS), a 118-GHz eight-channel imaging spectrometer plus a switched-frequency spectrometer near 53 GHz, for use on the NASA ER-2 high-altitude aircraft, (2) conduct of ER-2 MTS missions in multiple seasons and locations in combination with other instruments, mapping with unprecedented approximately 2-km lateral resolution atmospheric temperature and precipitation profiles, atmospheric transmittances (at both zenith and nadir), frontal systems, and hurricanes, (3) ground based 118-GHz 3-D spectral images of wavelike structure within clouds passing overhead, (4) development and analysis of approaches to ground- and space-based 5-mm wavelength sounding of the upper stratosphere and mesosphere, which supported the planning of improvements to operational weather satellites, (5) development of improved multidimensional and adaptive retrieval methods for atmospheric temperature and humidity profiles, (6) development of combined nonlinear and statistical retrieval techniques for 183-GHz humidity profile retrievals, (7) development of nonlinear statistical retrieval techniques for precipitation cell-top altitudes, and (8) numerical analyses of the impact of remote sensing data on the accuracy of numerical weather predictions; a 68-km gridded model was used to study the spectral properties of error growth.

Staelin, D. H.↗

NASA NTRS1987

Remote mineralogical and vegetation mapping using imaging spectrometry

Two airborne flight systems were developed for geological studies: the airborne imaging spectrometer (AIS) and the advanced visible and infrared imaging spectrometer. A satellite imaging spectrometer system, the high resolution imaging spectrometer, is currently being developed and is planned for flight on the proposed NASA Earth Orbiting System. Examples of the application of these instruments in mineral and vegetation studies are described. Experiments conducted with AIS over the Cuprite Mining District (Nevada) and the Owens Valley (California) demonstrate the power of this new approach to remote sensing.

King, James, Jr.↗

NASA NTRS1992

Exploration of Pluto

Two NASA-sponsored cost-constrained mission implementations for the exploration of Pluto are described. One is the Pluto Fast Flyby (PFF) mission, which utilizes an 83 kg spacecraft to be launched in 1998 aboard a Titan IV (Solid Rocket Motor Upgrade)/Centaur) for an about 7-year-long direct trajectory to Pluto, which will carry an integrated CCD-imaging/UV spectrometer, with a possible integrated IR spectrometer. The other is the Pluto-350 spacecraft, weighing about 316 kg, which will carry a broader instrument set, greater redundancy, and which will require greater than 11 year flight time. Pluto-350 will be launched in 2001 aboard a Delta or Atlas, toward earth and Jupiter swingbys to provide the energy to reach Pluto.

Staehle, Robert L.↗

NASA NTRS1995

Two-Diffraction-Order, Beam-Splitting, Imaging Spectrometer

Two-octave imaging spectrometer utilizes light of two harmonically related wavelengths diffracted to harmonically related orders at same angles, followed by separation via dichroic beam splitter before final imaging. Conceptual design of spectrometer calls for minimum number of optical elements to achieve coverage of required visible and near-infrared wavelengths in instrument of reduced size, weight, and cost.

Labaw, Clayton C.↗