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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 613 records · Page 34
All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

Magnetoelectronic phenomena due to quantum magnetization fluctuations

The goal of the project was to identify techniques to study magnetoelectronic phenomena such as spin transfer (ST) that stem from the quantum-mechanical nature of magnetization, and utilize them to characterize these quantum phenomena. The first such technique, electronic measurements based on the dependence of resistance on the population of spin-wave quanta (magnons) in a magnetic nanostructure, was shown by detailed measurements to be significantly influenced by the current-driven generation of a highly nonequilibrium phonon distribution by electrical current. This previously unrecognized phenomenon adds to the understanding of current-induced heating phenomena, qualitatively changes the methodology of analysis of current-induced heating common in scientific studies and engineering of current-carrying nanostructures. It benefits the public by providing a new direction for mitigation of Joule heating effects in electronic devices. The project also included quantum simulations of current-induced effects in magnetic nanostructures, which revealed that linear momentum and energy conservation are important for ST. Only angular momentum conservation was previously believed to be important. This finding is important for the fundamental understanding of ST, and for the design of efficient magnetoelectronic devices taking advantage of these conservation laws. Simulations also showed that non-classical ST is dominant in antiferromagnets, which will transform the understanding of ST in these systems. Finally, experimental studies of spin-transfer in ultrathin transition metal films revealed very large non-classical effects which were traced to the quantum origins of magnetism associated in the studied systems with the formation of an orbital liquid state. These findings i) transform the understanding of "conventional" transition-metal magnetism, ii) open a new field of studies in magnetism and a new method for the electronic control of magnetic properties and magnetism itself, and iii) provide a new approach to the development of efficient magnetoelectronic devices.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
NASA NTRS1982

Magnetic changes accompanying the thermal decomposition of nontronite /in air/ and its relevance to Martian mineralogy

It is found that the thermal treatment of nontronite in air, for long periods at 700 C or short periods at 900 C, results in the destruction of the nontronite structure, a distinct reddening in color, and a large increase in magnetic susceptibility and saturation magnetization. Measurements and calculations of the magnetic properties suggest that the magnetism is due to the presence of ultrafine particles of alpha or gamma Fe2O3. The highly magnetic thermally treated nontronite is amorphous to X-rays consistent with an ultrafine grain size. Prolonged heating results in the growth of alpha Fe2O3, while reflectivity spectra of a sample heated for 1 hr at 900 C indicate the presence of an opaque, magnetite-like phase in addition to alpha Fe2O3. It is found that the thermally treated nontronite has chemical, color, and magnetic properties similar to those found by Viking on Mars. It is concluded that these results indicate an origin for the fine grained Martian surface material by repeated impacts into an Fe-rich smectite-charged regolith (Weldon et al., 1980).

Moskowitz, B. M.↗
NASA NTRS1984

Downstream properties of magnetic flux transfer events

Attention is given to the downstream evolution of the field line tubes known as 'flux transfer events' (FTEs), whose magnetic field and plasma properties are distinct from those of the nearby unmerged magnetosheath and magnetosphere field lines. After the FTE has moved 200 earth radii down the tail, its drained portion reaches 25 earth radii radially outward from the tail boundary. It is suggested that most multiple crossings of the tail boundary observed by spacecraft are encounters with tailward-moving FTEs, thereby explaining both the behavior of boundary normals during multiple crossings and how the sign of the IMF causes the observed dawn-dusk asymmetries in the thickness of the magnetotail boundary layer.

Sibeck, D. G.↗
NASA NTRS1989

Functional Microspheres

Tiny beads develop from aqueous solution. Process forms beads of polyglutaraldehyde directly from solution. Beads of 0.5-to-1.0-micron diameter with fluorescent or magnetic properties made. Fluorescent or magnetic properties allow marked cells to be traced and identified. Useful in biology, clinical chemistry, and biochemistry.

Rembaum, Alan↗
DOE OSTI2019

Preparation and Characterization of NdFeB/PrCo{sub 5} Nanocomposite Magnetic Materials

We first developed NdFeB/PrCo{sub 5} nanocomposite magnetic material by high-energy ball milling, and the influence of the different contents of PrCo{sub 5} on the magnetic properties of NdFeB was studied by means of XRD, DSC, and VSM. The results showed that compared with single-phase NdFeB permanent-magnet material, NdFeB/PrCo{sub 5} nanocomposite magnetic material has superior magnetic properties. When the content of PrCo{sub 5} is 10% and the time of ball milling is 10 h, the magnetic properties for NdFeB/PrCo{sub 5} nanocomposite magnetic material is best: coercivity is 13.2 kOe, which increased by 14.8% over pure NdFeB phase. Remanent magnetization is 96.31 emu/g and the saturation magnetization is 132.29 emu/g. The remanence ratio is 0.728.

36 MATERIALS SCIENCE↗
NASA NTRS2004

Developing Glassy Magnets from Simulated Composition of Martian Soil for Exploration Applications

The long-term exploration goals of NASA include developing human habitation on Mars and conducting scientific investigations on Mars and other planetary bodies. In situ resource processing is a key objective in this area. We focus on the possibility of making magnetic glasses in situ for potential applications development. The paper will focus on ongoing work at NASA Marshall Space Flight Center on making magnetic glass from Mars soil simulants and its characterization. Analysis of the glass morphology, strength, chemistry and resulting magnetic properties will provide a fundamental understanding of the synthesized material that can be used for potential applications development. in an effort to characterize the magnetic properties of the Mars glasses, a series of tests were performed at NASA MSFC. Preliminary tests indicated that the glasses were attracted to a magnet and also had a small amount of residual magnetism. They were opaque (almost black in color). As the first step, a sample of Mars 1 glass (approx.1 mm x 1 mm x 5 mm length) was machined, weighed and its hysteresis curve was measured using a Vibration Sample Magnetometer (VSM). Next, a small furnace was designed and built and the sample was baked in a graphite (reducing agent) crucible at 800 C in an Argon atmosphere for 3 hours in the presence of a uniform, transverse (transverse to the 5mm length of the sample) magnetic field of 0.37 Tesla. The treated sample showed reddening on the outside and showed substantially increased residual magnetism. This sample was again analyzed in the VSM. The data clearly showed that some chemical change occurred during the heat treatment (color change) and that both the glasses have useful magnetic properties. Although no orientation effects of the magnetic field were considered, the data showed the following: 1. Both glass samples are primarily soft magnets and display ferromagnetic behavior (hysteresis, saturation, etc.) 2. The treated glass has improved saturation magnetism (order of magnitude increase), retentivity (factor of 6 increase) and susceptibility (order of magnitude increase) compared to the untreated glass 3. The untreated sample has higher coercivity (approx.50% that of Nickel) than the treated sample 4. Both samples have similar energy density. Results from a systematic study to quantify the effects of processing conditions such as heat treatment, atmosphere, containerless processing (by electrostatic levitation), and applications of external magnetic fields of different strengths will be discussed. Efforts on optimizing the magnetic properties of the product and the feasibility of using it for a couple of specific magnetic applications such as heat generation using an ac field and for electro forming will also be covered. The latter is an in situ manufacturing technique being studied for in-space fabrication applications at MSFC.

Ramachandran, N.↗
NASA NTRS1975

Magnetochemistry of the Apollo landing sites

A coherent magnetochemical picture of lunar samples is presented which was determined from a synthesis of available magnetic-property data and corresponding chemical and petrographic data for soils and rock samples collected at the Apollo landing sites. The magnetic properties of the samples are correlated with Al/Si ratio as well as with telescope spectral reflectivity curves, and magnetochemical diagrams based on composition-sensitive magnetic parameters describing the Fe metal and Fe(2+) contents are used to classify the samples. It is shown that the relative metal-fraction size distribution and magnetic stability for different rock types and soils of varying Al/Si values are reflected in a plot of the ratio of saturation isothermal remanence to saturation magnetization vs the ratio of remanent coercive force to coercive force. It is concluded that all the Apollo landing sites have distinct telescope curves correlated with petrology, chemistry, Al/Si values, and magnetic properties. The established correlations suggest the possibility of estimating the magnetic properties of the regolith from remote-sensing observations.

Wasilewski, P. J.↗
DOE OSTI2025

Discovery of a Ferromagnetic Nickel Chalcogenide Nanocluster Ni 3 S 3 H(PEt 3 ) 5

Atomically precise ligated nanoclusters (NC) are promising cluster-based materials with novel molecular architectures and tunable magnetic properties. Herein, the synthesis and characterization of a nickel sulfide NC Ni 3 S 3 H(PEt 3 ) 5 (PEt 3 = triethylphosphine) with distinct magnetic properties are reported. Magnetization measurements reveal its magnetic moment of 1.5 µ B in the solid phase, consistent with the existence of one unpaired electron predicted by density functional theory (DFT) calculations. Additionally, experimental measurements indicate the presence of ferromagnetic ordering within each Ni 3 S 3 H(PEt 3 ) 5 NC and strong coercivity at temperatures below 20 K. Ion mobility-mass spectrometry is employed in conjunction with DFT calculations and collision cross-section simulations to investigate the structure of the isolated Ni 3 S 3 H(PEt 3 ) 5 . Theoretical studies show that [Ni 3 S 3 H(PEt 3 ) 5 ] + has a planar Ni 3 S 3 core where three Ni atoms are arranged in a triangle with three bridging S atoms residing in the same plane. This structure is preserved in both solution and solid phases, which is confirmed by spectroscopic studies of Ni 3 S 3 H(PEt 3 ) 5 . Additionally, DFT calculations indicate that all spins at the Ni sites are aligned parallel, confirming the presence of ferromagnetic coupling. Overall, this study provides key insights into the structure and magnetic properties of Ni 3 S 3 H(PEt 3 ) 5 , which will facilitate the design of new NC-based magnetic materials.

Nickel sulfide nanocluster↗
DOE OSTI2018

Structural and Magnetic Characteristics of Ferroxplana Co{sub 2}Y Nanoferrites Synthesized via Two Chemical Routes

Barium Y-type hexaferrite Ba{sub 2}Co{sub 2}Fe{sub 12}O{sub 22} nanopowders have been purposefully tailored using two different chemical wet methods, namely sol-gel auto-combustion (SGA) and co-precipitation (CP) routes. The impact of the pre-annealing and the annealing temperature of the formed precursors synthesized using two strategies on the structural, microstructure, and magnetic properties was investigated using x-ray diffraction (XRD), scanning electron microscopic (SEM), Fourier transform infrared spectroscopy (FT-IR), and vibrating sample magnetometer (VSM). For instance, well-defined Ba{sub 2}Co{sub 2}Fe{sub 12}O{sub 22} hexagonal plate-like particles was observed using SGA and CP routes for the precursors pre-annealed at 600 {sup ∘}C for 4 h and then annealed at low temperature 1000 {sup ∘}C for 2 h. The magnetic properties measured at room temperature evinced that hexaferrite Co{sub 2}Y particles have ferromagnetic characteristics. Good magnetic properties involving saturation magnetization (M{sub s}) of 23.64 and 24.37 emu/g and the coercivity (H{sub c}) of 417.76 and 280.92 Oe were accomplished for the samples pre-annealed at 600 {sup ∘}C for 4 h and then annealed at 1000 {sup ∘}C for 2 h for SGA and CP methods, respectively.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2022

Phase stability and magnetic and electronic properties of a spark plasma sintered CoFe – P soft magnetic alloy

More efficient power conversion devices are able to transmit greater electrical power across larger distances to satisfy growing global electrical needs. A critical requirement to achieve more efficient power conversion are the soft magnetic materials used as core materials in transformers, inductors, and motors. To that effect it is well known that the use of non-equilibrium microstructures, which are, for example, nanocrystalline or consist of single phase solid solutions, can yield high saturation magnetic polarization and high electrical resistivity necessary for more efficient soft magnetic materials. In this work, we synthesized CoFe – P soft magnetic alloys containing nanocrystalline, single phase solid solution microstructures and studied the effect of a secondary intermetallic phase on the saturation magnetic polarization and electrical resistivity of the consolidated alloy. Single phase solid solution CoFe – P alloys were prepared through mechanically alloying metal powders and phase decomposition was observed after subsequent consolidation via spark plasma sintering (SPS) at various temperatures. The secondary intermetallic phase was identified as the orthorhombic (Co x Fe 1-x ) 2 P phase and the magnetic properties of the (Co x Fe 1-x ) 2 P intermetallic phase were found to be detrimental to the soft magnetic properties of the targeted CoFe – P alloy.

36 MATERIALS SCIENCE↗
DOE OSTI2024

Large-scale Linear Magnetic Holes with Magnetic Mirror Properties in Hybrid Simulations of Solar Wind Turbulence

Magnetic holes (MHs) are coherent magnetic field dips whose size ranges from fluid to kinetic scale, ubiquitously observed in the heliosphere and in planetary environments. Despite the long-standing effort in interpreting the abundance of observations, the origin and properties of MHs are still debated. In this Letter, we investigate the interplay between plasma turbulence and MHs, using a 2D hybrid simulation initialized with solar wind parameters. We show that fully developed turbulence exhibits localized elongated magnetic depressions, whose properties are consistent with linear MHs frequently encountered in space. The observed MHs develop self-consistently from the initial magnetic field perturbations by trapping hot ions with large pitch angles. Ion trapping produces an enhanced perpendicular temperature anisotropy that makes MHs stable for hundreds of ion gyroperiods, despite the surrounding turbulence. We introduce a new quantity, based on local magnetic field and ion temperature values, to measure the efficiency of ion trapping, with potential applications to the detection of MHs in satellite measurements. We complement this method by analyzing the ion velocity distribution functions inside MHs. Our diagnostics reveal the presence of trapped gyrotropic ion populations, whose velocity distribution is consistent with a loss cone, as expected for the motion of particles inside a magnetic mirror. Our results have potential implications for the theoretical and numerical modeling of MHs.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2021

Structure-property correlations and scaling in the magnetic and magnetocaloric properties of GdCrO 3 particles

The structure, magnetic, and magnetocaloric (MC) properties of orthorhombic nanocrystalline GdCrO 3 with six particle sizes: < d > = 87, 103, 145, 224, 318, and 352 nm are reported. The particle size was tailored by annealing under different temperatures and estimated by scanning electron microscopy. With increase in < d >, Goldschmidt tolerance factor t, orthorhombic strain s, and out-of-plane Cr–O 1 –Cr bond angle first decrease, reaching minimum values for < d > = 224 nm, and then increase for sample with < d > = 318 nm and 352 nm, thus showing a V-shaped variation. Temperature dependence of the magnetization (M) reveals an antiferromagnetic transition at ${T}_{\text{N}}^{\text{Cr}}\sim 168$ K for < d > ≥ 224 nm and ${T}_{\text{N}}^{\text{Cr}}\sim 167$ K for < d > < 224 nm and an essentially d-independent spin-reorientation at T SR = 9 K. M measured at 5 K and 7 T first increases with increase in < d >, reaching maximum value for sample with < d > = 224 nm, and then decreases for samples with < d > = 318 nm and 352 nm, showing an inverted-V variation with < d >. Similar < d >-dependence is observed for the magnetic entropy change (MEC) and relative cooling power (RCP) showing a close relationship between the structural and magnetic properties of GdCrO 3 nanoparticles investigated here. The 224 nm sample with the minimum values of t, s, and Cr–O 1 –Cr bond angle exhibits the maximum value of MEC (–ΔS) = 37.8 J kg –1 K –1 at 5 K under a field variation (ΔH) of 7 T and its large estimated RCP of 623.6 J Kg –1 is comparable with those of typical MC materials. Both (–ΔS) and RCP are shown to scale with the saturation magnetization MS, suggesting that MS is the crucial factor controlling their magnitudes. Assuming (–ΔS) ~ (ΔH) n , the temperature dependence of n for the six samples are determined, n varying between 1.3 at 5 K to n = 2.2 at 130 K in line with its expected magnitudes based on mean-field theory. Furthermore, these results on structure-property correlations and scaling in GdCrO 3 suggest that its MC properties are tunable for potential low-temperature magnetic refrigeration applications.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
NASA NTRS1998

The Parsec-Scale Magnetic Field Properties of Low-Optical Polarization Blazars

Past variability studies of flat-spectrum, compact extra-galactic radio sources have suggested that low- and high-optically polarized quasars (LPQ/HPQ) are the same type of object, differing only in the angle their relativistic jets make to the line of sight. This view has been challenged, however, by recent millimeter-wave polarization observations which indicate intrinsic differences in the inner magnetic field properties of the two classes. The inner jets of LPQs tend to have lower fractional polarizations than HPQs, and inferred magnetic field directions that are mostly parallel to the jet. The magnetic fields of HPQs, on the other hand, lie mainly in a transverse direction. The latter configuration is a prediction of the standard shock-in-jet model, in which a portion of a jet undergoes a strong transverse compression, thereby enhancing the perpendicular components of an originally tangled magnetic field. The main goal of this study is to establish a connection between the optical polarization and magnetic field properties of the inner jets of blazars. The magnetic field orientations of several HPQs have been shown to be stable over many years, which may be due to standing shock(s) located close to the base of the jet. Since these shocks are able to produce large amounts of optically polarized synchrotron radiation, their presence may very well determine whether an object is classified as an HPQ or LPQ. We have imaged the parsec-scale jet regions and magnetic fields of 11 LPQs with the Very Long Baseline Array (VLBA) at 43 and 22 GHz, and have obtained near- simultaneous optical polarization data for the sample. We discuss correlations between the optical and radio polarization data, and compare the LPQ properties to those of a sample of HPQs presently being monitored with the VLBA and JCMT at mm and sub-mm wavelengths, respectively. This research was performed in part at the Jet Propulsion Laboratory, California Institute of Technology, under contract to NASA.

Lister, Matthew L.↗
DOE OSTI2020

The effect of Cu additions in FePt–BN–SiO 2 heat-assisted magnetic recording media

Structural and chemical order impact magnetic properties of solids, which are governed by spin–orbit coupling and exchange interaction. The ordered L1 0 phase of FePt is a key material to heat-assisted magnetic recording; to enable high storage density, a solid understanding is needed of structural and chemical disorder at small length scales, as well as associated modifications of the electronic band structure. Here, we investigate the effect of boron and copper additions (≲6 mol% Cu) on structural and magnetic properties of L1 0 FePt granular media. Two copper-driven mechanisms, although competing, can lead to improvements in both structural and magnetic properties. In particular, the Cu substitution on the Fe-site leads to a degradation of magnetic properties due to the delocalized electron orbitals originating from a larger Cu d -orbital occupancy. At the same time, Cu substitution leads to an enhanced crystallographic order and consequently magneto-crystalline anisotropy, which offsets the former effect to a large extent. Our study is based on magnetometry, x-ray absorption spectroscopy, ab-initio calculations and a phenomenological theory of disordered FePt granular media. We do not observe a sizable modification to Fe moments and electronic configuration; Cu reveals two different resonances associated with the presence and absence of Cu–B bonds that vary with total Cu concentration.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2023

Effect of a guide field on the turbulence like properties of magnetic reconnection

The effect of an external guide field on the turbulence-like properties of magnetic reconnection is studied using five different 2.5D kinetic particle-in-cell (PIC) simulations. The magnetic energy spectrum is found to exhibit a slope of approximately −5/3 in the inertial range, independent of the guide field. On the contrary, the electric field spectrum in the inertial range steepens more with the guide field and approaches a slope of −5/3. In addition, spectral analysis of the different terms of the generalized Ohm's law is performed and found to be consistent with PIC simulations of turbulence and MMS observations. Finally, the guide field effect on the energy transfer behavior is examined using the von Kármán–Howarth (vKH) equation based on incompressible Hall-MHD. The general characteristics of the vKH equation with constant rate of energy transfer in the inertial range are consistent in all the simulations. This suggests that the qualitative behavior of energy spectrum and energy transfer in reconnection are similar to that of turbulence, indicating that reconnection fundamentally involves an energy cascade.

Physics↗
DOE OSTI2020

System and method for measuring fluid properties using magnetic field techniques via magnetic tracer

A method and apparatus for determining a property of a fluid in a vessel. The method uses magnetic tracer particles and an externally applied magnetic field which orients the particles. When the fluid moves, it changes the orientation of the tracer particles, thus changing the magnetic fields. These changes are detected by external magnetic field sensors. By using mathematical models, the property of the fluid in the vessel is determined from the detected magnetic field. In this manner, fluid vorticity, velocity, strain and stress may be estimated.

42 ENGINEERING↗
DOE OSTI2021

Tuning magnetic and optical properties through strain in epitaxial LaCrO 3 thin films

We report on the effect of epitaxial strain on magnetic and optical properties of perovskite LaCrO 3 (LCO) single crystal thin films. Epitaxial LCO thin films are grown by pulsed laser deposition on proper choice of substrates to impose different strain states. A combined experimental and theoretical approach is used to demonstrate the direct correlation between lattice-strain and functional properties. The magnetization results show that the lattice anisotropy plays a critical role in controlling the magnetic behavior of LCO films. The strain induced tetragonality in the film lattice strongly affects the optical transitions and charge transfer gap in LCO. This study opens possibilities to tailor the functional properties of LCO and related materials by strain engineering in epitaxial growth.

36 MATERIALS SCIENCE↗