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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 613 records · Page 34

Influence of Austempering Temperature and Time on the Microstructure and Mechanical Properties of Ductile Iron Weldment Using Developed Coated Electrode

Sound welded joints of ductile iron were first made by developing coated electrodes as well as weld procedure. The weldments were then austenitized at 900 °C for 2-h holding time followed by austempering at 300 and 350 °C for three different holding times (1.5, 2 and 2.5 h) at each austempering temperature. The influence of austempering temperature and time on the microstructural and mechanical properties was studied. Microstructural characterization, phase analysis, microhardness and mechanical properties were performed to understand the effect of austempering heat treatment on microstructure, austempering kinetics and mechanical properties of welded joints. In spite of significant variation in microstructures among all the three zones of DI weldment before austempering, the response of both weld metal and HAZ to austempering heat treatment similar to a base metal was noted. However, a significant variation in matrix structures (bainitic ferrite, retained austenite) as well as graphite nodules among the three zones was observed with changing the austempering temperature and holding time. Also, 100% joint efficiency of the welded joints was achieved at both 300 and 350 °C for 2-h holding time. Hardness and charpy impact toughness mostly depended on the volume fraction of retained austenite and carbon content. Based on the results of tensile and charpy impact testing, 350 °C and 2-h holding time could be considered as an optimum austempering condition for ADI weldment.

36 MATERIALS SCIENCE↗

Phase 1-2 Study of Stereotactic Ablative Radiotherapy Including Regional Lymph Node Irradiation in Patients With High-Risk Prostate Cancer (SATURN): Early Toxicity and Quality of Life

Five-fraction stereotactic ablative radiation therapy appears to be gaining popularity in treatment of prostate cancer, but it has not been extensively tested in the context of pelvic radiation. The objective of this prospective prostate and pelvic SABR study is to report the acute toxicity, late toxicity, and quality of life (QoL) after study completion.

62 RADIOLOGY AND NUCLEAR MEDICINE↗

Regulating phase behavior of nanoparticle assemblies through engineering of DNA-mediated isotropic interactions

Self-assembly of isotropically interacting particles into desired crystal structures could allow for creating designed functional materials via simple synthetic means. However, the ability to use isotropic particles to assemble different crystal types remains challenging, especially for generating low-coordinated crystal structures. Here, we demonstrate that isotropic pairwise interparticle interactions can be rationally tuned through the design of DNA shells in a range that allows transition from common, high-coordinated FCC-CuAu and BCC-CsCl lattices, to more exotic symmetries for spherical particles such as the SC-NaCl lattice and to low-coordinated crystal structures (i.e., cubic diamond, open honeycomb). The combination of computational and experimental approaches reveals such a design strategy using DNA-functionalized nanoparticles and successfully demonstrates the realization of BCC-CsCl, SC-NaCl, and a weakly ordered cubic diamond phase. The study reveals the phase behavior of isotropic nanoparticles for DNA–shell tunable interaction, which, due to the ease of synthesis is promising for the practical realization of non-close-packed lattices.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

Beam test performance studies of CMS Phase-2 Outer Tracker module prototypes

A new tracking detector will be installed as part of thePhase-2 upgrade of the CMS detector for the high-luminosity LHC era.This tracking detector includes the Inner Tracker, equipped withsilicon pixel sensor modules, and the Outer Tracker, consisting ofmodules with two parallel stacked silicon sensors. The Outer Trackerfront-end ASICs will be able to correlate hits from chargedparticles in these two sensors to perform on-module discriminationof transverse momenta (p$_{T}$). The p$_{T}$information is generated at a frequency of 40 MHz and will be usedin the Level-1 trigger decision of CMS. Prototypes of theso-called 2S modules were tested at the Test Beam Facility at DESYHamburg between 2019 and 2020. These modules use the finalfront-end ASIC, the CMS Binary Chip (CBC), and for the firsttime the Concentrator Integrated Circuit (CIC), optical readoutand on-module power conversion. In total, seven modules were tested,one of which was assembled with sensors irradiated with protons. Animportant aspect was to show that it is possible to read out modulessynchronously. A cluster hit efficiency of about 99.75 % wasachieved for all modules. The CBC p$_{T}$ discriminationmechanism has been verified to work together with the CIC andoptical readout. The measured module performance meets therequirements for operation in the upgraded CMS tracking detector.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Adjuvant Hepatic Arterial Infusion Pump Chemotherapy After Resection of Colorectal Liver Metastases: Results of a Safety and Feasibility Study in The Netherlands

Background: The 10-year overall survival with adjuvant hepatic arterial infusion pump (HAIP) chemotherapy after resection of colorectal liver metastases (CRLMs) was 61% in clinical trials from Memorial Sloan Kettering Cancer Center. A pilot study was performed to evaluate the safety and feasibility of adjuvant HAIP chemotherapy in patients with resectable CRLMs. Study Design: A phase II study was performed in two centers in The Netherlands. Patients with resectable CRLM without extrahepatic disease were eligible. All patients underwent complete resection and/or ablation of CRLMs and pump implantation. Safety was determined by the 90-day HAIP-related postoperative complications from the day of pump placement (Clavien–Dindo classification, grade III or higher) and feasibility by the successful administration of the first cycle of HAIP chemotherapy. Results: A total of 20 patients, with a median age of 57 years (interquartile range [IQR] 51–64) were included. Grade III or higher HAIP-related postoperative complications were found in two patients (10%), both of whom had a reoperation (without laparotomy) to replace a pump with a slow flow rate or to reposition a flipped pump. No arterial bleeding, arterial dissection, arterial thrombosis, extrahepatic perfusion, pump pocket hematoma, or pump pocket infections were found within 90 days after surgery. After a median of 43 days (IQR 29–52) following surgery, all patients received the first dose of HAIP chemotherapy, which was completed uneventfully in all patients. Conclusion: Pump implantation is safe, and administration of HAIP chemotherapy is feasible, in patients with resectable CRLMs, after training of a dedicated multidisciplinary team.

62 RADIOLOGY AND NUCLEAR MEDICINE↗

Chemical Composition Analysis and Product Consistency Tests of the ORP Phase 6 Nepheline Study Glasses

In this report, Savannah River National Laboratory (SRNL) provides chemical analyses and Product Consistency Test (PCT) results for a series of simulated high-level waste (HLW) glass compositions fabricated at Pacific Northwest National Laboratory (PNNL). The results of this effort will improve the ability to predict the impacts of glass composition and nepheline crystallization on the durability of HLW glasses. Chemical analyses were performed on a representative sample of each of the quenched glasses to allow for comparisons with the targeted compositions. A review of the individual glass composition measurements identified no analytical issues of concern. Minor differences between the targeted and measured concentrations of some of the baseline glass components were noted, including some high values for Fe 2 O 3 , and some low values for Al 2 O 3 , Li 2 O, Na 2 O and P 2 O 5 . The PCT Method-A was performed in triplicate on each of the quenched and canister centerline cooled (CCC) versions of the glasses to assess chemical durability. A review of the leachate analyses and standard solution data identified no issues with the analytical methods. Some of the CCC versions of the study glasses have normalized concentration for boron (NC B ) values that are higher than the Environmental Assessment glass benchmark NC B value of 16.695 g/L. For some of the study glasses, the NC B values were higher after the CCC heat treatment. The normalized concentrations for lithium and sodium (NC Li and NC Na ) followed this same trend. For many of these glasses, the changes in the normalized concentration for silicon (NC Si ) values were not congruent with the changes in NC B , NC Li , and NC Na values. It may be valuable for PNNL to perform a more complete review of the influence of composition and heat treatment on the PCT responses of the glasses described in this report to draw further conclusions, including any potential correlations with the methods used in selecting these glass compositions for study.

36 MATERIALS SCIENCE↗

Hydrogen Based Energy Storage System for Integration with Dispatchable Power Generator (Phase I Feasibility Study)

This project examined the feasibility of integrating hydrogen generation, storage, and use as a means to decarbonize campus activities while retaining the ability to utilize the existing natural gas fired combined heat and power system installed at the campus of the University of California @ Irvine. Analysis of specific potential sites for the integrated system identified a location adjacent to the existing central plant which resulted in minimization of interconnections. A strategy based on use of commercial electrolyzers and gas storage was identified. Primary technology advancements are required for the gas turbine to accommodate higher levels of hydrogen and the integrated controls. The project indicated challenges for adopting the proposed strategy with the present rates and constraints. The availability of a relatively low-cost biogas resource by the campus already decarbonizes the gas turbine to some extent. In the absence of this resource, procurement of electricity directly from large scale renewable operations could facilitate lower electricity costs. Additional solar resources on campus could also help in this regard. The gas turbine cannot be operated below 50% capacity due to air permit constraints. Using the otherwise curtailed gas turbine operation to generate hydrogen via electrolysis by consuming natural gas is not highly efficient and therefore leads to relatively high costs of electricity returned. Several scenarios demonstrate potential for effective decarbonization, yet most involve lower and lower capacity factor for the legacy gas turbine which is not a good use of the asset. A small gas turbine output with higher efficiency operation would help. As would ability to export electricity to the grid. Certainly current rate structures and operational scenarios are less attractive than other possible future structures which should be pushed for in the future.

03 NATURAL GAS↗