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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 613 records · Page 34
All sourcesNASA NTRSDOE OSTI
NASA NTRS2011

Size Optimization for Mirror Segments for X-Ray Optics

The flight mirror assemblies (FMA) for X-ray telescopes similar to that of the International X-ray Observatory (IXO) concept consist of several thousands of individual mirror segments. The size, shape, and location of these mirrors affect many characteristics of the telescope design. Mission requirements among other factors in turn restrict mirror segment parameters such as thickness, axial- length, azimuthal span, and mass density. This paper provides an overview of the critical relationships relating to mirror segment size and configuration throughout the design and analysis of an X-ray mirror assembly. A computational analysis is presented in the form of ray tracing pairs of thin X-ray mirror segments of varying sizes aligned in gravity and supported using kinematic constraints with corresponding self weight distortions calculated using finite element analysis (FEA). The work in this paper may be used as a starting point for determining mirror segment sizes for X-ray missions like that of IXO and beyond.

Biskach, Michael P.↗
DOE OSTI2024

Automated Gold Nanorod Spectral Morphology Analysis Pipeline

The development of a colloidal synthesis procedure to produce nanomaterials with high shape and size purity is often a time-consuming, iterative process. This is often due to quantitative uncertainties in the required reaction conditions and the time, resources, and expertise intensive characterization methods required for quantitative determination of nanomaterial size and shape. Absorption spectroscopy is often the easiest method for colloidal nanomaterial characterization. However, due to the lack of a reliable method to extract nanoparticle shapes from absorption spectroscopy, it is generally treated as a more qualitative measure for metal nanoparticles. This work demonstrates a gold nanorod (AuNR) spectral morphology analysis tool, called AuNR-SMA, which is a fast and accurate method to extract quantitative structural information from colloidal AuNR absorption spectra. To demonstrate the practical utility of this model, we apply it to three distinct applications. First, we demonstrate this model's utility as an automated analysis tool in a high-throughput AuNR synthesis procedure by generating quantitative size information from optical spectra. Second, we use the predictions generated by this model to train a machine learning model to predict the resulting AuNR size distributions under specified reaction conditions. Third, we apply this model to spectra extracted from the literature where no size distributions are reported and impute unreported quantitative information on AuNR synthesis. This approach can potentially be extended to any other nanocrystal system where absorption spectra are size dependent, and accurate numerical simulation of absorption spectra is possible. In addition, this pipeline could be integrated into automated synthesis apparatuses to provide interpretable data from simple measurements, help explore the synthesis science of nanoparticles in a rational manner, or facilitate closed-loop workflows.

36 MATERIALS SCIENCE↗
NASA NTRS1984

An approach for automated analysis of particle holograms

A simple method for analyzing droplet holograms is proposed that is readily adaptable to automation using modern image digitizers and analyzers for determination of the number, location, and size distributions of spherical or nearly spherical droplets. The method determines these parameters by finding the spatial location of best focus of the droplet images. With this location known, the particle size may be determined by direct measurement of image area in the focal plane. Particle velocity and trajectory may be determined by comparison of image locations at different instants in time. The method is tested by analyzing digitized images from a reconstructed in-line hologram, and the results show that the method is more accurate than a time-consuming plane-by-plane search for sharpest focus.

Stanton, A. C.↗
NASA NTRS1977

Sizes and albedos of the larger asteroids

The purpose of the present paper is to review all asteroid diameter measurements, current through mid-1976, and to combine them in a consistent way to give the best available estimates for a sample totalling 187 objects. From these diameters it is possible to determine the size-distributions of minor planets down to diameters of 50 km in the inner belt and 100 km in the outer belt. The associated albedos further indicate the distribution of objects of the C, S, and M classes throughout the belt.

Morrison, D.↗
DOE OSTI2023

Functionalized porous organic polymers as uranium nano-traps for efficient uranium extraction

Compositions are provided for efficient uranium extraction, for example from wastewater, seawater, or other water sources. The compositions can include a functionalized porous organic polymer functionalized with one or more uranium binding moieties, e.g. having a plurality of amidoxime or amidrazone groups covalently attached thereto. The compositions can include covalent organic frameworks, porous aromatic frameworks, and various porous organic polymers, especially those having a hierarchical pore size distribution over a range of pore sizes. The compositions can have functional groups such as amidoxime or an amidrazone covalently attached thereto. The hierarchical pore size distribution can be determined based upon at least 60% of the pore sizes in the range of pore sizes having a pore volume of at least 0.01 cm 3 g −1 in the pore size distribution at 77 K. Methods of making the compositions and methods of using the compositions are also provided.

Ma, Shengqian↗
NASA NTRS1978

Elemental characteristics of aerosols emitted from a coal-fired heating plant

Size differentiated aerosols were collected downstream from a heating plant fueled with eastern coal and analyzed using particle induced X-ray emission technique. Based on aerosol masses collected in various size ranges, the aerosol size distribution is determined to be trimodal, with the three peaks centered at 0.54 microns, 4.0 microns, and 11.0 microns, respectively. Of the various trace elements present in the aerosols, sulphur is the only element that shows very strong concentration in the smallest size group. Iron is strongly concentrated in the 4.0 micron group. Potassium, calcium, and titanium also exhibit stronger concentration in the 4.0 micron group than any other group. Other trace elements - vanadium, chromium, manganese, nickel, copper, and barium - are equally divided between the 0.54 microns and the 4.0 microns groups. Apparently, all of the trace elements - except S - enter aerosols during the initial formation and subsequent condensation phases in the combustion process. Excess concentration of sulphur in the 0.54 microns group can only be accounted for by recondensation of sulphur vapors on the combustion aerosols and gas-to-particle phase conversion of sulfate vapors at the stack top.

Singh, J. J.↗
NASA NTRS1987

Centrifuge impact cratering experiments: Scaling laws for non-porous targets

A geotechnical centrifuge was used to investigate large body impacts onto planetary surfaces. At elevated gravity, it is possible to match various dimensionless similarity parameters which were shown to govern large scale impacts. Observations of crater growth and target flow fields have provided detailed and critical tests of a complete and unified scaling theory for impact cratering. Scaling estimates were determined for nonporous targets. Scaling estimates for large scale cratering in rock proposed previously by others have assumed that the crater radius is proportional to powers of the impactor energy and gravity, with no additional dependence on impact velocity. The size scaling laws determined from ongoing centrifuge experiments differ from earlier ones in three respects. First, a distinct dependence of impact velocity is recognized, even for constant impactor energy. Second, the present energy exponent for low porosity targets, like competent rock, is lower than earlier estimates. Third, the gravity exponent is recognized here as being related to both the energy and the velocity exponents.

Schmidt, Robert M.↗
NASA NTRS1972

The determination and optimization of (rutile) pigment particle size distributions

A light scattering particle size test which can be used with materials having a broad particle size distribution is described. This test is useful for pigments. The relation between the particle size distribution of a rutile pigment and its optical performance in a gray tint test at low pigment concentration is calculated and compared with experimental data.

Richards, L. W.↗
NASA NTRS1980

Determination of the complex refractive index and size distribution of atmospheric particulates from bistatic-monostatic lidar and solar radiometer measurements

A method is presented for inferring both the size distribution and the complex refractive index of atmospheric particulates from combined bistatic-monostatic lidar and solar radiometer observations. The basic input measurements are spectral optical depths at several visible and near-infrared wavelengths as obtained with a solar radiometer and backscatter and angular scatter coefficients as obtained from a biostatic-monostatic lidar. The spectral optical depth measurements obtained from the radiometer are mathematically inverted to infer a columnar particulate size distribution. Advantage is taken of the fact that the shape of the size distribution obtained by inverting the particulate optical depth is relatively insensitive to the particle refractive index assumed in the inversion. Bistatic-monostatic angular scatter and backscatter lidar data are then processed to extract an optimum value for the particle refractive index subject to the constraint that the shape of the particulate size distribution be the same as that inferred from the solar radiometer data. Specifically, the scattering parameters obtained from the bistatic-monostatic lidar data are compared with corresponding theoretical computations made for various assumed refractive index values. That value which yields best agreement, in a weighted least squares sense, is selected as the optimal refractive index estimate. The results of this procedure applied to a set of simulated measurements as well as to measurements collected on two separate days are presented and discussed.

Reagan, J. A.↗
NASA NTRS1985

Determination of Mineral Type, Abundance, and Grain Size with Remotely Obtained Reflectance Spectra

To derive the abundances of minerals in a surface composed of more then one mineral in an intimate mixture, the bidirectional reflectance spectrum must be measured at several angles of incidence and emission. From these measurements, the scattering parameters may be derived, and the effective single scattering albedo can be computed from the models. If the scattering parameters are not derived, and the particles scatter anisotropically, then the computed effective single scattering albedo has been computed, the solution to the model is a nonlinear least squares problem with three unknowns per particle type. The solution is feasible when the complex indices of refraction and the densities of each mineral component are known. The unknowns are: the grain size of each particle type, the mass fraction of each particle type, and a grain internal scattering coefficient that describes grain imperfections.

Clark, R. N.↗
NASA NTRS1975

Comparisons of ground-based monitor data with Pioneers 8, 9, 10 and 11 observations in 1968-1974

The paper examines ground-based neutron monitor data and the counting rates in different energy channels on the Pioneer 8, 9, 10 and 11 spacecraft to determine the scale size of the transient cosmic-ray variations (Forbush decreases) and the relationship of these variations to changes in the interplanetary magnetic field. Since the Pioneer spacecraft sampled the inner modulating region extensively, the spatial extent of Forbush decreases (Fd's) can be determined. In some cases the Fd modulating region was co-rotating and in others radially expanding. The azimuthal extent of the Fd region was variable but was typically about 45 deg in extent. These observations will be interpreted in terms of models proposed for Fds.

Lockwood, J. A.↗
NASA NTRS1970

Design problems of small turbomachinery

Advanced design and testing techniques developed at NASA Lewis to achieve high efficiency in small turbomachines are described. Small radial and axial turbines and compressors were built for space power systems and associated studies at the Lewis Research Center. A six stage axial compressor of 3.5 inches diameter and axial turbines of 5 and 8.5 inches diameter were included. Radial turbines and compressors ranged from 3.5 to 6 inches. Topics discussed include maximum efficiency as a function of speed, the effect of compressibility on passage size, the use of quasi-orthogonals to calculate cross-channel velocity gradients, a design point velocity diagram study for axial turbines, and estimating off-design performance. Special turbine instruments and calibration procedures were developed to test compressors and turbines, to determine Reynolds and size number effects clearance, specific speed effects, and compressor performance. Laboratory tests conducted to study system operation and shaft and bearing motions are also reviewed.

Rohlik, H. E.↗
NASA NTRS2009

Residual Stresses and Critical Initial Flaw Size Analyses of Welds

An independent assessment was conducted to determine the critical initial flaw size (CIFS) for the flange-to-skin weld in the Ares I-X Upper Stage Simulator (USS). A series of weld analyses are performed to determine the residual stresses in a critical region of the USS. Weld residual stresses both increase constraint and mean stress thereby having an important effect on the fatigue life. The purpose of the weld analyses was to model the weld process using a variety of sequences to determine the 'best' sequence in terms of weld residual stresses and distortions. The many factors examined in this study include weld design (single-V, double-V groove), weld sequence, boundary conditions, and material properties, among others. The results of this weld analysis are included with service loads to perform a fatigue and critical initial flaw size evaluation.

Brust, Frederick W.↗
DOE OSTI2021

Magnetic properties of the Shastry-Sutherland lattice material BaNd 2 ZnO 5

We investigate the physical properties of the Shastry-Sutherland lattice material BaNd 2 ZnO 5 . Neutron diffraction, magnetic susceptibility, and specific heat measurements reveal antiferromagnetic order below 1.65 K. The magnetic order is found to be a 2–Q magnetic structure with the magnetic moments lying in the Shastry-Sutherland lattice planes comprising the tetragonal crystal structure of BaNd 2 ZnO 5 . The ordered moment for this structure is 1.9(1) μB per Nd ion. Inelastic neutron scattering measurements reveal that the crystal field ground state doublet is well separated from the first excited state at 8 meV. The crystal field Hamiltonian is determined through simultaneous refinement of models with both the LS coupling and intermediate coupling approximations to the inelastic neutron scattering and magnetic susceptibility data. The ground state doublet indicates that the magnetic moments lie primarily in the basal plane with magnitude consistent with the size of the determined ordered moment.

36 MATERIALS SCIENCE↗
NASA NTRS1977

Simulation model of erosion and deposition on a barchan dune

Erosion and deposition over a barchan dune near the Salton Sea, California, are modeled by bookkeeping the quantity of sand in saltation following streamlines of transport. Field observations of near surface wind velocity and direction plus supplemental measurements of the velocity distribution over a scale model of the dune are combined as input to Bagnold type sand transport formulas corrected for slope effects. A unidirectional wind is assumed. The resulting patterns of erosion and deposition compare closely with those observed in the field and those predicted by the assumption of equilibrium (downwind translation of the dune without change in size or geometry). Discrepancies between the simulated results and the observed or predicted erosional patterns appear to be largely due to natural fluctuations in the wind direction. The shape of barchan dunes is a function of grain size, velocity, degree of saturation of the oncoming flow, and the variability in the direction of the oncoming wind. The size of the barchans may be controlled by natural atmospheric scales, by the age of the dunes, or by the upwind roughness. The upwind roughness can be controlled by fixed elements or by sand in the saltation. In the latter case, dune scale is determined by grain size and wind velocity.

Howard, A. D.↗
DOE OSTI2021

Temperature and salt controlled tuning of protein clusters

The formation of molecular assemblies in protein solutions is of strong interest both from a fundamental viewpoint and for biomedical applications. While ordered and desired protein assemblies are indispensable for some biological functions, undesired protein condensation can induce serious diseases. As a common cofactor, the presence of salt ions is essential for some biological processes involving proteins, and in aqueous suspensions of proteins can also give rise to complex phase diagrams including homogeneous solutions, large aggregates, and dissolution regimes. Here, we systematically study the cluster formation approaching the phase separation in aqueous solutions of the globular protein BSA as a function of temperature (T), the protein concentration (c p ) and the concentrations of the trivalent salts YCl 3 and LaCl 3 (c s ). As an important complement to structural, i.e. time-averaged, techniques we employ a dynamical technique that can detect clusters even when they are transient on the order of a few nanoseconds. By employing incoherent neutron spectroscopy, we unambiguously determine the short-time self-diffusion of the protein clusters depending on c p , c s and T. We determine the cluster size in terms of effective hydrodynamic radii as manifested by the cluster center-of-mass diffusion coefficients D. For both salts, we find a simple functional form D(c p , c s , T) in the parameter range explored. The calculated inter-particle attraction strength, determined from the microscopic and short-time diffusive properties of the samples, increases with salt concentration and temperature in the regime investigated and can be linked to the macroscopic behavior of the samples.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2023

Optimal Sizing and Dispatch of Solar Power with Storage

Designers of utility-scale solar plants with storage, seeking to maximize some aspect of plant performance, face multiple challenges. In many geographic locations, there is significant penetration of photovoltaic generation, which depresses energy prices during the hours of solar availability. An energy storage system affords the opportunity to dispatch during higher-priced time periods, but complicates plant design and dispatch decisions. Solar resource variability compounds these challenges, because determining optimal system sizes requires simultaneously considering how the plant will be operated under the imposed market and weather conditions. We develop an approach to analyze the economic performance of hybrid and single-technology solar power plants, which incorporates optimal dispatch, and considers the expected electricity market and weather conditions. We utilize the System Advisor Model software package to simulate the operation of multiple renewable generation and energy storage technologies, in conjunction with hourly-fidelity generation decisions determined by a revenue-maximizing, mixed-integer linear program. We show that, under our assumed market and weather conditions, the lifetime benefit-to-cost ratio can be improved by 6 to 19 percent, relative to a baseline design without optimizing, and that a concentrating solar power with thermal energy storage design produces significantly more energy per year, but is less profitable under our cost assumptions.

black-box optimization↗
NASA NTRS1983

Pressure investigation of NASA leading edge vortex flaps on a 60 deg Delta wing

Pressure distributions on a 60 deg Delta Wing with NASA designed leading edge vortex flaps (LEVF) were found in order to provide more pressure data for LEVF and to help verify NASA computer codes used in designing these flaps. These flaps were intended to be optimized designs based on these computer codes. However, the pressure distributions show that the flaps wre not optimum for the size and deflection specified. A second drag-producing vortex forming over the wing indicated that the flap was too large for the specified deflection. Also, it became apparent that flap thickness has a possible effect on the reattachment location of the vortex. Research is continuing to determine proper flap size and deflection relationships that provide well-behaved flowfields and acceptable hinge-moment characteristics.

Marchman, J. F., III↗