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All sourcesNASA NTRSDOE OSTI
NASA NTRS2016

Ionomer-Membrane Water Processing Apparatus

This disclosure provides water processing apparatuses, systems, and methods for recovering water from wastewater such as urine. The water processing apparatuses, systems, and methods can utilize membrane technology for extracting purified water in a single step. A containment unit can include an ionomer membrane, such as Nafion(Registered Trademark), over a hydrophobic microporous membrane, such as polytetrafluoroethylene (PTFE). The containment unit can be filled with wastewater, and the hydrophobic microporous membrane can be impermeable to liquids and solids of the wastewater but permeable to gases and vapors of the wastewater, and the ionomer membrane can be permeable to water vapor but impermeable to one or more contaminants of the gases and vapors. The containment unit can be exposed to a dry purge gas to maintain a water vapor partial pressure differential to drive permeation of the water vapor, and the water vapor can be collected and processed into potable water.

MacCallum, Taber K.↗
NASA NTRSDate not supplied

A METHOD TO REDUCE BIOBURDEN IN ASTROMATERIALS CURATION FACILITIES WITHOUT INTRODUCING UNWANTED CONTAMINATION

Introduction: NASA curates its Astromaterials collections in cleanrooms that are carefully monitored for particulate, inorganic and trace metal contamination. Current sample collections are not particularly susceptible to organic contamination or biological alteration. However, new collections like those from the OSIRIS-REx and Hayabusa2 missions will have organic contamination requirements and are susceptible to biodegradation. It will be necessary sterilize or at least disinfect curation labs, as well as tools and equipment in a manner that does not introduce additional contamination and does not affect the samples 1. Current curation cleaning procedures utilize isopropyl alcohol which offers some bioburden reduction, but is not effective against spore-forming bacteria or fungal spores 2. We present a modified disinfection method that uses ultrapure hydrogen peroxide to reduce bioburden inside curation labs and glove boxes without introducing contamination or damaging curation equipment. We tested this method in the meteorite processing lab as well as on a glovebox being cleaned for use in processing ANGSA (Apollo Next Generation Sample Analysis) samples and present the results of those tests. We discuss the limitations of this method and describe potential situations in which it will not be applicable. The CDC guidelines for disinfection andsterilization in healthcare facilities discusses over 15different methods for reducing bioburden in hospitalsettings 3. The most common method, steamsterilization, is well suited to sterilizing curationprocessing tools but cannot easily be used to sterilizecleanroom surfaces or large equipment likegloveboxes. Chemical sterilization with bleach(NaOCl) is also a common strategy in healthcare andpharmaceutical settings that presents materialcompatibility issues as well as serious inorganiccontamination concerns for curation facilities.Introducing a new source of Na and Cl into curationlabs is not acceptable. Other chemical methods likeethylene oxide, formaldehyde, iodophors andquaternary ammonium compounds could introduceorganic and inorganic contamination. We chose tofocus on hydrogen peroxide because it is generallycompatible with commonly used curation materialslike stainless steel, aluminum and Teflon and becauseit decomposes to oxygen and water. The CDCguidelines for hydrogen peroxide specify using a 7.5wt% solution at 25 ̊C with a contact time of 30 minutesfor high level disinfection and 6 hours for sterilization.High level disinfection is defined as a technique thatwill kill all microorganisms except large numbers ofbacterial spores 3. Methods: We prepared a solution of 7.5 wt%hydrogen peroxide from a stock solution of ultrapure30 wt% peroxide (JT Baker) and curation gradeultrapure water. This ultrapure water is already used incuration cleaning procedures and thus is not consideredand additional source of contamination. We conducteda materials compatibility test by exposing unanodizedand anodized 6061 T6 Al alloy to the peroxide solutionfor up to six hours and periodically inspecting thesurfaces for visible defects. We used this peroxide todisinfect the floor of the meteorite processing lab andthe interior of a curation glovebox by exposing thesesurfaces to the peroxide solution for 30 min. Thesurfaces were swabbed with a dry macrofoam swabbefore (Puritan Brand 2518051PFRNDFD) and afterperoxide treatment to collect microbes present on thesurfaces. Microbes were extracted by sonication fromthe swab into 15 ml of PBS (phosphate buffered saline)and inoculated onto the following media: TSA (trypticsoy agar) BA (blood agar), R2A (Reasoners 2 agar),Potato Dextrose Agar, Saboraud Dextrose Agar andSaboraud Dextrose Agar with 0.1 mg/ mlchloramphenicol. Four TSA plates and two BA plateswere inoculated with 0.1 ml of PBS each andincubated at 35 and 37 for 48 hours. Two R2A°C°Cplates (0.1 ml of PBS each) were incubated at 25 .°CThe remaining plates were inoculated with 0.2ml ofPBS and incubated at 30 ̊C for seven days. Afterincubation bacterial and fungal isolates were countedand transferred to new plates for identification usingthe VITEK24 automated system or by sequencing aportion of the barcode gene (16S rRNA for bacteria,small subunit gene for fungi) on an ABI 3500 Sangersequencer. Negative controls consisted of swabs thatwere opened in the sampling environment andanalyzed alongside the experimental samples.Results: A 6 hour exposure to hydrogen peroxideresulted in visible pitting on un-anodized 6061 Al, butnot on anodized surfaces. No visible pitting occurredafter a 30 minute exposure. Therefore, we decided tolimit our experimental tests to 30 min. exposures. 17bacterial CFU (colony forming units) representing 4distinct organisms were isolated from the meteorite processing lab floor prior to hydrogen peroxidetreatment. We were unable culture any organisms afterperoxide treatment. In the glovebox we were able toculture three bacterial CFU representing three distinctspecies, including a spore forming bacterium prior todisinfection with peroxide. After the peroxidetreatment we were unable to culture any organisms.Routine monitoring of the meteorite processing lab andthe glovebox did not indicate any increase in unwantedinorganic contamination after these peroxidetreatments. Discussion: A 30 minute treatment with 7.5 wt%peroxide appears to be an effective method forreducing bioburden on typical cleanroom surfaces. Themethod does not introduce unwanted organic orinorganic contamination and is compatible withcommonly used curation materials like stainless steel,Teflon and anodized aluminum alloys. Special careshould be taken with un-anodized aluminum.Prolonged exposure to hydrogen peroxide can causepitting on this material. We recommend using thismethod to disinfect curation labs and equipment whenbiological alteration is a concern. This method iseffective at room temperature and cannot be used todisinfect labs and equipment where the ambienttemperature is < 0 ̊C. Astromaterials samples shouldbe removed from the area where disinfection is tooccur. Hydrogen peroxide is a powerful oxidizingagent and will react with any organic carbon present inthe sample. References: [1.] Mccubbin, F. M. et al.Sp. Sci Rev(2019) doi:10.1007/s11214-019-0615-9. [2.] Mogul, R.et al.Astrobiology 18, ast.2017.1814 (2018). [3.]Rutala, W. A. & Weber, D. J. Guideline for Disinfection and Sterilization in Healthcare Facilities, 2008. [4.] Pincus, D. H. in Encyclopedia of Rapid Microbiological Methods (2005).

A. B. Regberg↗
DOE OSTI2026

Influence of Air and Ethanol Dehydration on Structure, Behavior, and Function of Type I Collagen Scaffolds

Ethanol dehydration is a common step in both scaffold manufacturing and tissue processing, yet the influence of ethanol on collagen is not well understood. This study examined the effects of dehydration, via ethanol treatment and air drying, on collagen structure, behavior, mechanics, and rehydration capacity. Multiple material characterization methods were used including Fourier Transform infrared spectroscopy (FTIR), Raman spectroscopy, scanning electron microscopy, thermogravimetric analysis, small/medium angle x‐ray scattering, volumetric swelling analysis, and tensile testing. Ethanol dehydration removed bulk water from scaffolds, making them stronger and stiffer, but also showed loss of molecular water. This molecular water appears to act as a collagen stabilizer, resulting in less thermally stable scaffolds. The loss of molecular water is also evident in the molecular d‐spacing. Secondary structure of scaffolds was also altered by ethanol, resulting in significantly enhanced rehydration capacity. Bulk water, both before and after rehydration, largely determined mechanical properties, which did not correlate with other structural measures such as FTIR. While rehydration largely returned collagen spacing to pre‐ethanol treated state, structural alterations seen in FTIR cannot be recovered. These results have implications for not only collagen scaffolds, but in many tissue engineering and processing applications.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
NASA NTRSDate not supplied

Automated Ply-By-Ply Lamination and in-Situ Consolidation of Dry Carbon Fiber Non-Crimp Fabrics for High-Rate Aircraft Manufacturing of Structural Aircraft Components

NASA’s Hi-Rate Composites Aircraft Manufacturing (HiCAM) program addresses market needs to advance structural aircraft composite manufacturing technologies to significantly increase production rates. Dry, non-crimp fabric (NCF) carbon materials infused with advanced resin systems offer a promising solution to these manufacturing demands. Northrop Grumman’s Automated Stiffener Forming (ASF) technology has been adapted for ply-by-ply, in-situ processing of NCF materials. The modular ASF process accommodates flexibility in the laminate stacking, while allowing for ply drops, ply additions, and yaw, pitch, and roll in the laminate geometry. To adapt the ASF process for NCF materials, heating technologies and roller compaction processes were designed and tested on representative structural aircraft part geometries. Key success criteria for the ASF process with NCF materials is forming quality and preform compaction. Trials were performed with multiple NCF materials: unidirectional up to quad-axial formats. The NCF constituents, veils, stitching, and binders, were evaluated with the ASF process. The material performance in the ASF process and the resulting preform quality are presented.

dry carbon fiber materials↗
DOE OSTI2025

Conceptual Model Testing Related to SDU 6 Drainwell Observations

From its inception in the early 1950s through the end of the Cold War in the early 1990s, the Savannah River Site (SRS) produced nuclear materials for national defense in five reactors. Additionally, irradiated reactor fuel and target tubes were dissolved in nitric acid to recover plutonium and uranium using the PUREX (Plutonium Uranium Reduction EXtraction) process. Liquid waste from these chemical separations processes was then stored onsite in 51 underground tanks. Eight waste storage tanks have been operationally closed (i.e. cleaned and grouted) and the remaining tanks hold a mixture of liquids, insoluble solids, and precipitated salts (SRMC-LWP-2022-00001), the latter generated by evaporating water from the liquid waste. Waste is currently being retrieved from tanks and separated into 1) high-radioactivity, low-volume, and 2) low-radioactivity, high-volume components, principally through the Salt Waste Processing Facility (SWPF) (SRMC-LWP-2023-00001). The former waste stream is vitrified in the Defense Waste Processing Facility (DWPF), stored onsite, and destined for offsite disposal in a deep geologic repository. The latter stream is mixed with dry cementitious materials in the Saltstone Production Facility (SPF) and the wet slurry placed in onsite Saltstone Disposal Units (SDUs) within the Saltstone Disposal Facility (SDF), where it hardens into a cement waste form termed saltstone. A low-infiltration surface cover system will be placed over the SDF at closure, where SDUs will then be in the subsurface post-closure (SRR-CWDA-2019-00001).

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
NASA NTRS1975

Forced-flow once-through boilers

A compilation and review of NASA-sponsored research on boilers for use in spacecraft electrical power generation systems is presented. Emphasis is on the heat-transfer and fluid-flow problems. In addition to space applications, much of the boiler technology is applicable to terrestrial and marine uses such as vehicular power, electrical power generation, vapor generation, and heating and cooling. Related research areas are discussed such as condensation, cavitation, line and boiler dynamics, the SNAP-8 project (Mercury-Rankine cycle), and conventional terrestrial boilers (either supercritical or gravity-assisted liquid-vapor separation types). The research effort was directed at developing the technology for once-through compact boilers with high heat fluxes to generate dry vapor stably, without utilizing gravity for phase separations. A background section that discusses, tutorially, the complex aspects of the boiling process is presented. Discussions of tests on alkali metals are interspersed with those on water and other fluids on a phenomenological basis.

Stone, J. R.↗
NASA NTRS1976

Relative humidity from psychrometric data

Analytical equation for computing relative humidity as function of wet bulb temperature, dry bulb temperature, and atmospheric pressure is suitable for use with calculator or computer. Analytical expressions may be useful for chemical process control systems and building environmental control systems.

Putnam, T. W.↗
NASA NTRS1978

Formation of the imidazolides of dinucleotides under potentially prebiotic conditions

Imidazolides of dinucleotides such as ImpApA can be formed from the corresponding dinucleotides in a two-stage process, which gives up to 15% yields under potentially prebiotic conditions. First a solution of the dinucleotide and sodium trimetaphosphate is dried out at constant temperature and humidity. This produces polyphosphates such as p(n)ApA in excellent yield (greater than or equal to 80%). The products are dissolved in water, imidazole is added, and the solution is dried out again. This yields the 5'-phosphorimidazolides.

Sleeper, H. L.↗
NASA NTRS1992

Preliminary results of polarization signatures for glacial moraines in the Mono Basin, Eastern Sierra Nevada

The valleys of the Mono Basin contain several sets of lateral and terminal moraines representing multiple stages of glaciation. The semi-arid climate with slow weathering rates preserved sequences of nested younger moraines within older ones. There is a well established relative chronology and recently exposure dating provided a new set of numerical dates. The moraines span the late Wisconsin (11-25 ka) to the Illinoian (130-190 ka) glaciations. The Mono Basin area was used as a 'calibration site' to establish remote dating techniques for eventual transfer to the more inaccessible but geomorphically and climatically similar moraines of the South American Andes Mountains. Planned polarimetric synthetic aperture radar (SAR) imagery acquired by JPL AIRSAR (South American Campaign) and SIR-C (Andes super-site) are analyzed to establish chronologies of previously undated moraine sequences in a study of Pleistocene climatic change in the Southern Hemisphere. The dry climate and sparse vegetation is also favorable for correlation of ground surface roughness with radar polarization signature. The slow weathering processes acting over thousands of years reduce the size, frequency, and angularity of surface boulders while increasing soil development on the moraines. Field observations based on this hypothesis result in relative ages consistent with those inferred from nested position within the valley. Younger moraines, therefore, will appear rougher than the older smoother moraines at scales measurable at AIRSAR wavelengths. Previously documented effects of ground surface roughness on polarization signatures suggest that analysis of moraine polarization signatures can be useful for relative dating. The technique may be extended to predict numerical ages. The data set reported were acquired on 8 Sep. 1989 with the JPL Airborne SAR (AIRSAR) collecting polarimetric imagery at C- (5.6 cm), L- (24 cm), and P-band (68 cm) with a flight-line parallel to the strike of the mountains. Phase calibration was performed on the analyzed scene by setting the co-phase of a smooth lake to zero as described. Absolute amplitude calibration was not possible because corner reflectors were not deployed.

Forster, Richard R.↗
NASA NTRS2004

Comparison of Local Scale Measured and Modeled Brightness Temperatures and Snow Parameters from the CLPX 2003 by Means of a Dense Medium Radiative Transfer Theory Model

Microwave remote sensing offers distinct advantages for observing the cryosphere. Solar illumination is not required, and spatial and temporal coverage are excellent from polar-orbiting satellites. Passive microwave measurements are sensitive to the two most useful physical quantities for many hydrological applications: physical temperature and water content/state. Sensitivity to the latter is a direct result of the microwave sensitivity to the dielectric properties of natural media, including snow, ice, soil (frozen or thawed), and vegetation. These considerations are factors motivating the development of future cryospheric satellite remote sensing missions, continuing and improving on a 26-year microwave measurement legacy. Perhaps the biggest issues regarding the use of such satellite measurements involve how to relate parameter values at spatial scales as small as a hectare to observations with sensor footprints that may be up to 25 x 25 km. The NASA Cold-land Processes Field Experiment (CLPX) generated a dataset designed to enhance understanding of such scaling issues. CLPX observations were made in February (dry snow) and March (wet snow), 2003 in Colorado, USA, at scales ranging from plot scale to 25 x 25 km satellite footprints. Of interest here are passive microwave observations from ground-based, airborne, and satellite sensors, as well as meteorological and snowpack measurements that will enable studies of the effects of spatial heterogeneity of surface conditions on the observations. Prior to performing such scaling studies, an evaluation of snowpack forward modelling at the plot scale (least heterogeneous scale) is in order. This is the focus of this paper. Many forward models of snow signatures (brightness temperatures) have been developed over the years. It is now recognized that a dense medium radiative transfer (DMRT) treatment represents a high degree of physical fidelity for snow modeling, yet dense medium models are particularly sensitive to snowpack structural parameters such as grain size, density, and depth---parameters that may vary substantially within a snowpack. Microwave radiometric data and snow pit measurements collected at the Local-Scale Observation Site (LSOS) during the third Intensive Observation Period (IOP3) of the CLPX have been used to test the capabilities of a DMRT model using the Quasi Crystalline Approximation with Coherent Potential (QCA-CP). The radiometric measurements were made by the University of Tokyo s Ground Based Microwave Radiometer-7 (GBMR-7) system. We evaluate the degree to which a DMRT-based model can accurately reproduce the GBMR-7 brightness temperatures at different frequencies and incidence angles.

Tedescol, Marco↗
NASA NTRS2012

Seasonally Active Slipface Avalanches in the North Polar Sand Sea of Mars: Evidence for a Wind-Related Origin

Meter-scale MRO/HiRISE camera images of dune slipfaces in the north polar sand sea of Mars reveal the presence of deep alcoves above depositional fans. These features are apparently active under current climatic conditions, because they form between observations taken in subsequent Mars years. Recently, other workers have hypothesized that the alcoves form due to destabilization and mass-wasting during sublimation of CO2 frost in the spring. While there is evidence for springtime modification of these features, our analysis of early springtime images reveals that over 80% of the new alcoves are visible underneath the CO2 frost. Thus, we present an alternative hypothesis that formation of new alcoves and fans occurs prior to CO2 deposition. We propose that fans and alcoves form primarily by aeolian processes in the mid- to late summer, through a sequence of aeolian deposition on the slipface, over-steepening, failure, and dry granular flow. An aeolian origin is supported by the orientations of the alcoves, which are consistent with recent wind directions. Furthermore, morphologically similar but much smaller alcoves form on terrestrial dune slipfaces, and the size differences between the terrestrial and Martian features may reflect cohesion in the near-subsurface of the Martian features. The size and preservation of the largest alcoves on the Martian slipfaces also support the presence of an indurated surface layer; thus, new alcoves might be sites of early spring CO2 sublimation and secondary mass-wasting because they act as a window to looser, less indurated materials that warm up more quickly in the spring.

Horgan, Briony H. N.↗
NASA NTRS2017

Virtual Design of a Four-Bed Molecular Sieve for Exploration

Aboard the International Space Station, CO2 is removed from the cabin atmosphere by a four-bed molecular sieve (4BMS) process called the Carbon Dioxide Removal Assembly (CDRA).1 This 4BMS process operates by passing the CO2-laden air through a desiccant bed to remove any humidity and then passing the dried air through a sorbent bed to remove the CO2. While one pair of beds is in use, the other pair is thermally regenerated to allow for continuous CO2 removal.

Giesy, T. J.↗
NASA NTRS2020

Twenty‐First Century Drought Projections in the CMIP6 Forcing Scenarios

There is strong evidence climate change will increase drought risk and severity, but these conclusions depend on the regions, seasons, and drought metrics being considered. We analyze changes in drought across the hydrologic cycle (precipitation, soil moisture, and runoff) in projections from Phase Six of the Coupled Model Intercomparison Project (CMIP6). The multi‐model ensemble shows robust drying in the mean state across many regions and metrics by the end of the 21st century, even following the more aggressive mitigation pathways (SSP1‐2.6 and SSP2‐4.5). Regional hotspots with strong drying include western North America, Central America, Europe and the Mediterranean, the Amazon, southern Africa, China, Southeast Asia, and Australia. Compared to SSP3‐7.0 and SSP5‐8.5, however, the severity of drying in the lower warming scenarios is substantially reduced and further precipitation declines in many regions are avoided. Along with drying in the mean state, the risk of the historically most extreme drought events also increases with warming, by 200–300% in some regions. Soil moisture and runoff drying in CMIP6 is more robust, spatially extensive, and severe than precipitation, indicating an important role for other temperature‐sensitive drought processes, including evapotranspiration and snow. Given the similarity in drought responses between CMIP5 and CMIP6, we speculate both generations of models are subject to similar uncertainties, including vegetation processes, model representations of precipitation, and the degree to which model responses to warming are consistent with observations. These topics should be further explored to evaluate whether CMIP6 models offer reasons to have increased confidence in drought projections.

drought↗
NASA NTRS2022

Trash-to-Gas: Trash Preparation and Feed Mechanism

One method of reducing the mass and volume of astronaut waste items during future exploration missions is a process called Trash-to-Gas (TtG), which uses thermal degradation to convert various astronaut waste items into a gas that can either be repurposed onboard or safely vented overboard. This project aims to determine which methods for pre-processing waste may enhance the gasification efficiency within a microgravity TtG reactor. Preparation methods that were investigated include mixing, pre-drying, shredding, compacting, and raw unprocessed waste. Each of these preparation methods was tested within the state-of-the-art subscale TtG system, known as the Orbital Syngas/Commodity Augmentation Reactor (OSCAR), and the resulting solid-to-gas conversion and burn durations were compared. Full-scale CAD models of these various preparation methods in conjunction with a projected full-scale TtG reactor were created using Creo Parametric. An Equivalent System Mass (ESM) analysis was then performed to trade the benefits of improved solid-to-gas performance with the costs associated with implementing the additional components that would increase system mass, power, volume, and design complexity. The results of this ESM analysis will be leveraged for future full-scale TtG system development to help reduce the overall mass, power, and volume of the system while ensuring effective reactor performance.

Ray Pitts↗
DOE OSTI2024

Opening pathways for the conversion of woody biomass into sustainable aviation fuel via catalytic fast pyrolysis and hydrotreating

Meeting aggressive decarbonization targets set by the International Civil Aviation Organization (ICAO) will require the rapid development of technologies to produce sustainable aviation fuel (SAF). Catalytic fast pyrolysis (CFP) can support these efforts by opening pathways for the conversion of woody biomass into an upgraded biogenic oil that can be further processed to SAF and other fuels. However, the absence of end-to-end experimental data for the process leads to uncertainty in the yield, product quality, costs, and sustainability of the pathway. The research presented here serves to address these needs through a series of integrated experimental campaigns in which real biomass feedstocks are converted to a final SAF product using large bench-scale continuous reactor systems. For these campaigns, the degree of catalytic upgrading during CFP was varied to produce CFP-oils with oxygen contents of 17 and 20 wt% on a dry basis. The CFP-oils were then hydrotreated and distilled into gasoline, diesel, and SAF fractions. Detailed yield and compositional data were obtained for each step of the process to inform technoeconomic and lifecycle analyses, and the fuel properties of the SAF fraction were evaluated to provide first-of-its-kind insight into the quality of the final product. This research reveals opportunities to optimize process carbon efficiency by tuning the degree of catalytic upgrading during the CFP step and highlights routes to produce a high-quality cycloalkane-rich SAF with 85–92% reduction in greenhouse gas emissions compared to fossil-based pathways.

09 BIOMASS FUELS↗
DOE OSTI2025

Techno-economic evaluation of emission control configurations for AMP/PZ-based post-combustion CO 2 capture

Minimizing the environmental impacts of amine-based post-combustion carbon capture technologies is essential for regulatory compliance and public acceptance. Experimental campaigns at RWE's CO 2 capture pilot plant in Niederaussem using CESAR1 demonstrated that combining existing emission abatement technologies can substantially reduce the concentration of amines and degradation products in the CO 2 -depleted flue gas to below the detection limit of an infrared spectrometer. The campaign confirmed that a proprietary dry bed technology (OEASE aerozone™) or a second water wash can reduce AMP and PZ emissions to below 1 mg/Nm 3 . However, an acid or chemically active wash downstream of the water wash is necessary to reduce NH 3 emissions to very low levels (<2 mg/Nm 3 ). Combining a dry bed with an acid wash significantly reduces both the required acid solution and the resulting acid waste. The techno-economic analysis indicates that implementing emission mitigation technologies provides substantial environmental benefits for the CESAR1 process, with only a marginal increase (<1 €/tCO 2 ) in both the carbon capture cost (CCC) and CO 2 avoidance cost (CAC). The additional capital cost associated with extra column packing is offset by operational cost savings from reduced solvent losses. For stringent emission permits targeting NH 3 , a configuration combining a dry bed upstream of the water wash followed by an acid wash achieves the best balance between emission control and cost efficiency. This configuration results in a Levelized Cost of Electricity (LCOE) of 143 €/MWh, a CCC of 45.4 €/tCO 2 , and a CAC of 88.4 €/tCO 2 .

AMP↗
NASA NTRS2013

Fabrication Methods for Adaptive Deformable Mirrors

Previously, it was difficult to fabricate deformable mirrors made by piezoelectric actuators. This is because numerous actuators need to be precisely assembled to control the surface shape of the mirror. Two approaches have been developed. Both approaches begin by depositing a stack of piezoelectric films and electrodes over a silicon wafer substrate. In the first approach, the silicon wafer is removed initially by plasmabased reactive ion etching (RIE), and non-plasma dry etching with xenon difluoride (XeF2). In the second approach, the actuator film stack is immersed in a liquid such as deionized water. The adhesion between the actuator film stack and the substrate is relatively weak. Simply by seeping liquid between the film and the substrate, the actuator film stack is gently released from the substrate. The deformable mirror contains multiple piezoelectric membrane layers as well as multiple electrode layers (some are patterned and some are unpatterned). At the piezolectric layer, polyvinylidene fluoride (PVDF), or its co-polymer, poly(vinylidene fluoride trifluoroethylene P(VDF-TrFE) is used. The surface of the mirror is coated with a reflective coating. The actuator film stack is fabricated on silicon, or silicon on insulator (SOI) substrate, by repeatedly spin-coating the PVDF or P(VDFTrFE) solution and patterned metal (electrode) deposition. In the first approach, the actuator film stack is prepared on SOI substrate. Then, the thick silicon (typically 500-micron thick and called handle silicon) of the SOI wafer is etched by a deep reactive ion etching process tool (SF6-based plasma etching). This deep RIE stops at the middle SiO2 layer. The middle SiO2 layer is etched by either HF-based wet etching or dry plasma etch. The thin silicon layer (generally called a device layer) of SOI is removed by XeF2 dry etch. This XeF2 etch is very gentle and extremely selective, so the released mirror membrane is not damaged. It is possible to replace SOI with silicon substrate, but this will require tighter DRIE process control as well as generally longer and less efficient XeF2 etch. In the second approach, the actuator film stack is first constructed on a silicon wafer. It helps to use a polyimide intermediate layer such as Kapton because the adhesion between the polyimide and silicon is generally weak. A mirror mount ring is attached by using adhesive. Then, the assembly is partially submerged in liquid water. The water tends to seep between the actuator film stack and silicon substrate. As a result, the actuator membrane can be gently released from the silicon substrate. The actuator membrane is very flat because it is fixed to the mirror mount prior to the release. Deformable mirrors require extremely good surface optical quality. In the technology described here, the deformable mirror is fabricated on pristine substrates such as prime-grade silicon wafers. The deformable mirror is released by selectively removing the substrate. Therefore, the released deformable mirror surface replicates the optical quality of the underlying pristine substrate.

Toda, Risaku↗
NASA NTRS1977

Dry air entrainment into convective clouds

A systematic approach to the study of atmospheric turbulent motion is discussed in terms of weather modification. The background of cloud physics, and the mixing process are described. A zero-g study is proposed to enable the basic experimental data to be collected so that theory may be developed to generalize results for practical applications.

Telford, J. W.↗