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At least 613 records · Page 34
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

Debris-induced consequences on turbulence and vorticity in solar photovoltaic module-generated array wakes

Particle-laden flows in solar photovoltaic (PV) systems are inevitable, where wind-swept debris in open environments are carried by high winds and turbulence, coating panel surfaces or damaging structures. Particle deposition, or soiling, is a well-known issue for large-scale plants which rely on uninhibited solar rays for optimal production. But understanding the mechanisms leading to soiling requires a physical and fluid dynamics-centered focus, since turbulence dominates PV panel wakes and is also known to alter particle concentration and trajectories. This study presents an experimental campaign toward consequences of particle-laden flow between two model PV panels using time-resolved particle image velocimetry. The model array was subjected to varied particle volume fractions, including a tracer particle case and a water droplet case. Characterization of mean velocity, turbulence statistics, and mean kinetic energy within the single phase and, separately, particle phase flows showed modified features due to particle inertia. Images captured at a frequency of 1 kHz in the near wake of the upstream panel allow for a first experimental look at vorticity and convective velocity of vortex structures for single-phase and particle-phase flows which are crucial to debris transport and soiling in PV environments.

Energy & Fuels↗
NASA NTRS1990

A novel electron tunneling infrared detector

The pneumatic infrared detector, originally developed by Golay in the late 1940s, uses the thermal expansion of one cm(exp 3) of xenon at room temperature to detect the heat deposited by infrared radiation. This detector was limited by thermal fluctuations within a 10 Hz bandwidth, but suffered from long thermal time constants and a fragile structure. Nevertheless, it represents the most sensitive room temperature detector currently available in the long wavelength infrared (LWIR). Fabrication of this type of detector on smaller scales has been limited by the lack of a suitably sensitive transducer. Researchers designed a detector based on this principle, but which is constructed entirely from micromachined silicon, and uses a vacuum tunneling transducer to detect the expansion of the trapped gas. Because this detector is fabricated using micromachining techniques, miniaturization and integration into one and two-dimensional arrays is feasible. The extreme sensitivity of vacuum tunneling to changes in electrode separation will allow a prototype of this detector to operate in the limit of thermal fluctuations over a 10 kHz bandwidth. A calculation of the predicted response and noise of the prototype is presented with the general formalism of thermal detectors. At present, most of the components of the prototype have been fabricated and tested independently. In particular, a characterization of the micromachined electron tunneling transducer has been carried out. The measured noise in the tunnel current is within a decade of the limit imposed by shot noise, and well below the requirements for the operation of an infrared detector with the predicted sensitivity. Assembly and characterization of the prototype infrared detector will be carried out promptly.

Kenny, T. W.↗
NASA NTRS1992

Coronal density and temperature structure from coordinated observations associated with the total solar eclipse of 1988 March 18

This paper explores and compares diagnostics for temperature and density within large-scale structures of the inner corona based on cospatial and cotemporal spectrophotometric observations made at the time of the total solar eclipse of 1988 March 17/18. In the analysis a determination of plasma temperature T can be derived unambiguously from the intensity ratios Fe XIV/XUV or Fe XIV/Fe X since all the emission lines come from the ionized state of Fe and the ratios are only weakly dependent on density. These temperatures and the densities found in well-defined large-scale coronal structures are discussed. The emission-line temperature is found to be high (local maxima) in the coronal structures with enhanced white-light emission and associated with new cycle high-latitude magnetic fields separated from the old cycle polar field of opposite polarity. Also the average of the ratio of scale-height temperature/temperature over the entire range of position angle is roughly unity although the ratio is higher than unity (1.3-1.6) in the three most prominent streamers.

Guhathakurta, M.↗
NASA NTRS2012

Multiscale Dynamics of Solar Magnetic Structures

Multiscale topological complexity of the solar magnetic field is among the primary factors controlling energy release in the corona, including associated processes in the photospheric and chromospheric boundaries.We present a new approach for analyzing multiscale behavior of the photospheric magnetic flux underlying these dynamics as depicted by a sequence of high-resolution solar magnetograms. The approach involves two basic processing steps: (1) identification of timing and location of magnetic flux origin and demise events (as defined by DeForest et al.) by tracking spatiotemporal evolution of unipolar and bipolar photospheric regions, and (2) analysis of collective behavior of the detected magnetic events using a generalized version of the Grassberger-Procaccia correlation integral algorithm. The scale-free nature of the developed algorithms makes it possible to characterize the dynamics of the photospheric network across a wide range of distances and relaxation times. Three types of photospheric conditions are considered to test the method: a quiet photosphere, a solar active region (NOAA 10365) in a quiescent non-flaring state, and the same active region during a period of M-class flares. The results obtained show (1) the presence of a topologically complex asymmetrically fragmented magnetic network in the quiet photosphere driven by meso- and supergranulation, (2) the formation of non-potential magnetic structures with complex polarity separation lines inside the active region, and (3) statistical signatures of canceling bipolar magnetic structures coinciding with flaring activity in the active region. Each of these effects can represent an unstable magnetic configuration acting as an energy source for coronal dissipation and heating.

Magnetic fields↗
NASA NTRS1983

Observations of a hard X-ray component in the spectrum of Nova Ophiuchi

The spectrum and time variation of Nova Ophiuchi (H1705-25) in the 10-200 keV range as measured by the UCSD/MIT instruments aboard HEAO 1 during the period 1977 August 25 to September 28 are reported. The composite curve is best fitted by a kT = 2 keV thin thermal bremsstrahlung model below 10 keV and a separate hard X-ray component fitted equally well by a power-law component with photon index 2.19 + or - 0.06 or a kT = 32.1 + or - 2.4 keV thermal bremsstrahlung model. This is the first observation of a hard tail in the spectrum of a transient X-ray source with sufficient statistical significance to allow a detailed study of its spectral and temporal variability. It is found that the intensity variations of the high-energy X-rays are consistent with the variability at lower energies (3-6 keV), but no hard X-ray spectral index variability is found on time scales from 2 days to 2 weeks. The results can be interpreted as due to accretion onto a neutron star (or possibly onto a black hole) that may also be surrounded by an extended corona.

Wilson, C. K.↗
NASA NTRS1984

The lower main sequence and the nature of secondary stars in ultracompact binaries

The possible nature of the secondary stars in ultracompact binary stellar systems (with orbital periods of less than about 1 hr) are systematically investigated. Using a simplified stellar evolution code, which assumes isentropic stellar models, nearly 3000 separate models for hydrogen-burning main-sequence stars with masses less than 0.3 solar mass are generated. The effects of the (homogeneous) chemical composition on the properties of such stars and in, particular, on the minimum main-sequence mass are explored in detail. It is found that this minimum mass is a sensitive function of the hydrogen content and can be as small as 0.035 solar mass. The properties of fully degenerate low-mass stars, as well as low-mass stars that are not in thermal equilibrium are also studied. In particular, it is shown that the thermal time scale of such nonequilibrium stars may exceed 10 billion yr. The results also confirm the existence of a second branch of the main sequence and shed new light on the thermal instability of this branch. The available observational information on the three known ultracompact binary systems (4U 1626-67, G61-29, 4U 1916-05) is summarized, and the results of the stellar model calculations are combined with the empirical results to place constraints on the properties of the secondary stars.

Rappaport, S.↗
NASA NTRS1988

Demixing kinetics of phase separated polymer solutions in microgravity

Phase separated solutions of two neutral polymers in buffer provide a useful and versatile medium for the partition separation of biological cells. However, the efficiency of such separations is orders of magnitude lower than the thermodynamic limit. To test the hypothesis that this inefficiency is at least partially due to the convection and sedimentation that occur during the gravity driven demixing that follows introduction of cells to the systems, a series of experiments were begun aimed at performing cell partition in a low g environment. Demixing of isopycnic three polymer solvent systems was studied, experiments were performed on KC-135 aircraft and one shuttle middeck experiment was completed. Analysis of the results of these experiments and comparisons with the predictions of scaling relations for the dependence of phase domain size on time, derived for a number of possible demixing mechanisms, are presented.

Brooks, D. E.↗
NASA NTRS2002

Dynamical Models of the Solar System Formation and Evolution

Mark Lewis has extended his them is work by completing a series of N-body simulations of a narrow ring that: is in the location of Saturn's F-ring and is perturbed by a single satellite comparable to Prometheus, but on a circular orbit. We had previously shown how the satellite perturbations can cause a broadly distributed sparse population of ring particles to become concentrated into narrow rings that can be maintained outside of any resonance location. For low optical depths, the collisions between ring particles are highly localized in the peaks of the satellite wakes. The inelastic collisions therefore occur at a particular orbital phase angle so as to damp the azimuthal component of the relative velocities. Since particle positions are not changed by collisions, the semimajor axes of the particles are shifted toward the actual particle positions where the collisions occur. Thus, negative radial diffusion can occur while conserving orbital angular momentum so long as the forced eccentricity is continually re-excited by the satellite. We speculated that the separation between the final ringlets was largely determined by the magnitude of the forced eccentricities induced by the satellite at closest approach. We carried out a series of simulations with a variety of different satellite masses in order to vary the magnitude of the forced eccentricity. We found that indeed the final spacing of the ringlets does increase with the magnitude of the forced eccentricity (Lewis and Stewart 2002). This occurs because neighboring eccentric ringlets drift out of phase with one another due to Keplerian shear and eventually collide with one another, leading to a smaller number of more widely spaced ringlets, The time scale required to form narrow ringlets in these simulations is much shorter than one would expect from standard theories based upon the orbit-averaged torque produced by multiple passes by the satellite. We find that the initial ringlets form in less than two synodic periods and the final state is typically reached in 10 to 20 synodic periods. These studies move us closer to understanding the significantly more complex system of Saturn's F ring, where the perturbation magnitude varies over short temporal and spatial time scales due to the orbital eccentricities of the perturbing satellite. We are currently extending the simulation to allow for an eccentric orbit of the satellite.

Stewart, Glen R.↗
NASA NTRS2008

Active Management of Flap-Edge Trailing Vortices

The vortex hazard produced by large airliners and increasingly larger airliners entering service, combined with projected rapid increases in the demand for air transportation, is expected to act as a major impediment to increased air traffic capacity. Significant reduction in the vortex hazard is possible, however, by employing active vortex alleviation techniques that reduce the wake severity by dynamically modifying its vortex characteristics, providing that the techniques do not degrade performance or compromise safety and ride quality. With this as background, a series of experiments were performed, initially at NASA Langley Research Center and subsequently at the Berlin University of Technology in collaboration with the German Aerospace Center. The investigations demonstrated the basic mechanism for managing trailing vortices using retrofitted devices that are decoupled from conventional control surfaces. The basic premise for managing vortices advanced here is rooted in the erstwhile forgotten hypothesis of Albert Betz, as extended and verified ingeniously by Coleman duPont Donaldson and his collaborators. Using these devices, vortices may be perturbed at arbitrarily long wavelengths down to wavelengths less than a typical airliner wingspan and the oscillatory loads on the wings, and hence the vehicle, are small. Significant flexibility in the specific device has been demonstrated using local passive and active separation control as well as local circulation control via Gurney flaps. The method is now in a position to be tested in a wind tunnel with a longer test section on a scaled airliner configuration. Alternatively, the method can be tested directly in a towing tank, on a model aircraft, a light aircraft or a full-scale airliner. The authors believed that this method will have significant appeal from an industry perspective due to its retrofit potential with little to no impact on cruise (devices tucked away in the cove or retracted); low operating power requirements; small lift oscillations when deployed in a time-dependent manner; and significant flexibility with respect to the specific devices selected.

Greenblatt, David↗
NASA NTRS2018

Violation of Field Line Conservation and Associated Spatial Scales in Particle-In-Cell Simulations and MMS Data

For the first time, space flight technology exists to detect, in situ, violation of magnetic field line conservation. The violation of magnetic line conservation on scales smaller than the system size is a necessary and sufficient condition for finite magnetic field reconnection. We demonstrate that violation of line conservation produces a detectable, structured signature both in particle-in-cell simulations of reconnection and in data from the Magnetospheric Multi-Scale mission. In particle-in-cell simulations of asymmetric reconnection, the quantity-which we call M-that identifies this violation achieves significant values in electron skin depth-scale layers that extend away from the separator, with higher values emerging on the low-density, high-magnetic-field side of the current sheet. At the separator, M owes largely to perpendicular gradients in the parallel electric field, while it attains its highest values away from the separator in dispersed, layered structures associated with gradients in the perpendicular nonideal electric field and electron transport. Sub-ion scale bipolar forms of the quantity also appear further from the separator. In two MMS burst data intervals detecting the electron diffusion region, we find that M exceeds measurement uncertainties both at the separator and near the separatrices. One interval has highly sheared reconnecting fields and the other a stronger guide field. For one event, we determine the location and scale of M and the inner electron diffusion region relative to electron outflows and the magnetic separatrices. The measure can therefore serve as a potent diagnostic for magnetic reconnection in space measurements.

Wendel, Deirdre E.↗
NASA NTRS2021

Perseverance’s Scanning Habitable Environments with Raman and Luminescence for Organics and Chemicals (SHERLOC) Investigation

The Scanning Habitable Environments with Raman and Luminescence for Organics and Chemicals (SHERLOC) is a robotic arm-mounted instrument on NASA’s Perseverance rover. SHERLOC has two primary boresights. The Spectroscopy boresight generates spatially resolved chemical maps using fluorescence and Raman spectroscopy coupled to microscopic images (10.1 μm/pixel). The second boresight is a Wide Angle Topographic Sensor for Operations and eNgineering (WATSON); a copy of the Mars Science Laboratory (MSL) Mars Hand Lens Imager (MAHLI) that obtains color images from microscopic scales (∼13 μm/pixel) to infinity. SHERLOC Spectroscopy focuses a 40 μs pulsed deep UV neon-copper laser (248.6 nm), to a ∼100 μm spot on a target at a working distance of ∼48 mm. Fluorescence emissions from organics, and Raman scattered photons from organics and minerals, are spectrally resolved with a single diffractive grating spectrograph with a spectral range of 250 to ∼370 nm. Because the fluorescence and Raman regions are naturally separated with deep UV excitation (<250 nm), the Raman region ∼ 800 – 4000 cm−1 (250 to 273 nm) and the fluorescence region (274 to ∼370 nm) are acquired simultaneously without time gating or additional mechanisms. SHERLOC science begins by using an Autofocus Context Imager (ACI) to obtain target focus and acquire 10.1 μm/pixel greyscale images. Chemical maps of organic and mineral signatures are acquired by the orchestration of an internal scanning mirror that moves the focused laser spot across discrete points on the target surface where spectra are captured on the spectrometer detector. ACI images and chemical maps (< 100 μm/mapping pixel) will enable the first Mars in situ view of the spatial distribution and interaction between organics, minerals, and chemicals important to the assessment of potential biogenicity (containing CHNOPS). Single robotic arm placement chemical maps can cover areas up to 7x7 mm in area and, with the < 10 min acquisition time per map, larger mosaics are possible with arm movements. This microscopic view of the organic geochemistry of a target at the Perseverance field site, when combined with the other instruments, such as Mastcam-Z, PIXL, and SuperCam, will enable unprecedented analysis of geological materials for both scientific research and determination of which samples to collect and cache for Mars sample return.

Rohit Bhartia↗
DOE OSTI2025

An In Situ , Automated High-Explosives Aging Method Utilizing Two-Dimensional Gas Chromatography–Mass Spectrometry

Understanding chemical changes that occur in high explosives as they age is of great importance to the safe employment and storage of these compounds. Traditional methods of aging high explosives even under accelerated aging conditions are time intensive with durations on the order of months to years. The nature of traditional aging analyses reduces each sample to a snapshot data point often separated widely in time, requiring many assumptions as to how the degradation products develop. Further complicating matters, several analytical techniques are typically employed for each sample analysis in order to ascertain an entire picture of the decomposition pathways. To address these shortcomings with existing methods, a new method of accelerated aging of high explosives utilizing comprehensive two-dimensional gas chromatography coupled to high-resolution mass spectrometry (GC × GC-HRMS) was developed using 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazaisowurtzitane (CL-20) as a model compound for method development. This in situ automated method reduces the time scale of aging to a matter of hours using the inlet of the GC × GC as the aging vessel. GC × GC in combination with HRMS allowed for the collection of both evolved gases and other decomposition products produced during the entire aging process in real time with HRMS providing far greater certainty in identification of explosives aging products. Additionally, this method allowed for a higher throughput of samples with greatly simplified sample preparation. Chemometric analysis of the GC × GC-HRMS data set via the alteration analysis (ALA) enabled discovery of statistically significant chemical changes providing insight into the variation of decomposition pathways with varying aging temperatures.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS2000

The 3-Dimensional Inner and Outer Structure of Ejecta Around Eta Carinae as Detected by the STIS

The HST/STIS instrument was used successfully to perform a complete mapping of the Homunculus nebula at two wavelength ranges including H-alpha and H-beta with a spectral resolving power of about 5000 and a spatial resolution of 0.1". The individual spectra were merged to synthesize three-dimensional data cubes that contain a set of images of Eta Car with spatial resolution of 0.10 to 0.251, sliced at velocity increment of 10 -- 30 km/s. For the first time this unique method allows us to diagnose the origin of intrinsic narrow emission structure of the nebula with high spatial and velocity resolution. Our initial analysis revealed the inner emission structure appeared to trace an elongated bipolar shell (possibly other shells as well) with a scale size of an arcsecond (i.e., "little homunculus in the Homunculus"). Furthermore, the mapping data cube revealed that the "fan" or "paddle" -- often referred as the source of peculiar blue-shifted intrinsic emissions including the Strontium cloud -- is not the source of intrinsic emissions. The fan is not even a part of the equatorial disk, but is spatially separated from the peculiar emission structure. Indeed we suggest that the fan is a surface of the Northwest lobe, possibly revealed by a blowout of the equatorial disk. We will use a number of visualization techniques (tomographic animations and simple 3-D models) to show these structures. These new results have strong impact upon future numerical modelings of the Homunculus nebula and of understanding of the evolution of the ejecta powered by the central source(s).

Ishibashi, Kazunori↗
DOE OSTI2025

Spherical and sessile droplet dynamics by fluctuating hydrodynamics

We simulate the mesoscopic dynamics of droplets formed by phase-separated fluids at nanometer scales where thermal fluctuations are significant. Both spherical droplets fully immersed in a second fluid and sessile droplets which are also in contact with a solid surface are studied. Our model combines a Cahn–Hilliard formulation with incompressible fluctuating hydrodynamics; for sessile droplets, the fluid–solid contact angle is specified as a boundary condition. Deterministic simulations with an applied body force are used to measure the droplets' mobility from which a diffusion coefficient is obtained using the Einstein relation. Stochastic simulations are independently used to obtain a diffusion coefficient from a linear fit of the variance of a droplet's position with time. In some scenarios, these two measurements give the same value but not in the case of a spherical droplet initialized near a slip wall or in the case of sessile droplets with large contact angles (≥90°) on both slip and no-slip surfaces.

Bell, John B↗
NASA NTRS2020

A Summary Of: Collecting Sleep, Circadian, Fatigue, and Performance Data in Complex Operational Environments

Sleep loss and circadian misalignment contribute to a meaningful proportion of operational accidents and incidents. Countermeasures and work scheduling designs aimed at mitigating fatigue are typically evaluated in controlled laboratory environments, but the effectiveness of translating such strategies to operational environments can be challenging to assess. This manuscript summarizes an approach for collecting sleep, circadian, fatigue, and performance data in a complex operational environment. We studied 44 airline pilots over 34 days while they flew a fixed schedule, which included a baseline data collection with 5 days of mid-morning flights, four early flights, four high-workload mid-day flights, and four late flights that landed after midnight. Each work block was separated by 3-4 days of rest. To assess sleep, participants wore a wrist-worn research-validated activity monitor continuously and completed daily sleep diaries. To assess the circadian phase, pilots were asked to collect all urine produced in four or eight hourly bins during the 24 h after each duty block for the assessment of 6-sulfatoxymelatonin (aMT6s), which is a biomarker of the circadian rhythm. To assess subjective fatigue and objective performance, participants were provided with a touchscreen device used to complete the Samn-Perelli Fatigue Scale and Psychomotor Vigilance Task (PVT) during and after each flight, and at wake-time, mid-day, and bedtime. Using these methods, it was found that sleep duration was reduced during early starts and late finishes relative to baseline. Circadian phase shifted according to duty schedule, but there was a wide range in the aMT6s peak between individuals on each schedule. PVT performance was worse on the early, high-workload, and late schedules relative to baseline. Overall, the combination of these methods was practical and effective for assessing the influence of sleep loss and circadian phase on fatigue and performance in a complex operational environment.

Arsintescu, Lucica↗
NASA NTRS2011

An Estimate of Low-Cloud Feedbacks from Variations of Cloud Radiative and Physical Properties with Sea Surface Temperature on Interannual Time Scales

Simulations of climate change have yet to reach a consensus on the sign and magnitude of the changes in physical properties of marine boundary layer clouds. In this study, the authors analyze how cloud and radiative properties vary with SST anomaly in low-cloud regions, based on five years (March 2000 - February 2005) of Clouds and the Earth s Radiant Energy System (CERES) -- Terra monthly gridded data and matched European Centre for Medium-Range Weather Forecasts (ECMWF) meteorological reanalaysis data. In particular, this study focuses on the changes in cloud radiative effect, cloud fraction, and cloud optical depth with SST anomaly. The major findings are as follows. First, the low-cloud amount (-1.9% to -3.4% /K) and the logarithm of low-cloud optical depth (-0.085 to -0.100/K) tend to decrease while the net cloud radiative effect (3.86 W/m(exp 2)/ K) becomes less negative as SST anomalies increase. These results are broadly consistent with previous observational studies. Second, after the changes in cloud and radiative properties with SST anomaly are separated into dynamic, thermodynamic, and residual components, changes in the dynamic component (taken as the vertical velocity at 700 hPa) have relatively little effect on cloud and radiative properties. However, the estimated inversion strength decreases with increasing SST, accounting for a large portion of the measured decreases in cloud fraction and cloud optical depth. The residual positive change in net cloud radiative effect (1.48 W/m(exp 2)/ K) and small changes in low-cloud amount (-0.81% to 0.22% /K) and decrease in the logarithm of optical depth (-0.035 to -0.046/ K) with SST are interpreted as a positive cloud feedback, with cloud optical depth feedback being the dominant contributor. Last, the magnitudes of the residual changes differ greatly among the six low-cloud regions examined in this study, with the largest positive feedbacks (approximately 4 W/m(exp 2)/ K) in the southeast and northeast Atlantic regions and a slightly negative feedback (-0.2 W/m(exp 2)/ K) in the south-central Pacific region. Because the retrievals of cloud optical depth and/or cloud fraction are difficult in the presence of aerosols, the transport of heavy African continental aerosols may contribute to the large magnitudes of estimated cloud feedback in the two Atlantic regions.

Eitzen, Zachary A.↗
NASA NTRS1973

Synthetic carbohydrate: An aid to nutrition in the future

The synthetic production of carbohydrate on a large scale is discussed. Three possible nonagricultural methods of making starch are presented in detail and discussed. The simplest of these, the hydrolysis of cellulose wastes to glucose followed by polymerization to starch, appears a reasonable and economic supplement to agriculture at the present time. The conversion of fossil fuels to starch was found to be not competitive with agriculture at the present time, but tractable enough to allow a reasonable plant design to be made. A reconstruction of the photosynthetic process using isolated enzyme systems proved technically much more difficult than either of the other two processes. Particular difficulties relate to the replacement of expensive energy carrying compounds, separation of similar materials, and processing of large reactant volumes. Problem areas were pinpointed, and technological progress necessary to permit such a system to become practical is described.

Berman, G. A.↗
DOE OSTI2024

Comprehensive characterization of the structure of Zr-based metallic glasses

Structure of metallic glasses fascinates as the generic amorphous structural template for ubiquitous systems. Its specification necessitates determination of the complete hierarchical structure, starting from short-range-order (SRO) → medium-range-order (MRO) → bulk structure and free volume (FV) distribution. This link has largely remained elusive since previous investigations adopted one-technique-at-a-time approach, focusing on limited aspects of any one domain. Reconstruction of structure from experimental data inversion is non-unique for many of these techniques. As a result, complete and precise structural understanding of glass has not emerged yet. In this work, we demonstrate the first experimental pathway for reconstruction of the integrated structure, for and glasses. Our strategy engages diverse (×7) multi-scale techniques [XAFS, 3D-APT, ABED/NBED, FEM, XRD, PAS, FHREM] on the same glass. This strategy complemented mutual limitations of techniques and corroborated common parameters to generate complete, self-consistent and precise parameters. Further, MRO domain size and inter-void separation were correlated to identify the presence of FV at MRO boundaries. This enabled the first experimental reconstruction of hierarchical subset: SRO → MRO → FV → bulk structure. The first ever image of intermediate region between MRO domains emerged from this link. We clarify that determination of all subsets is not our objective; the essence and novelty of this work lies in directing the pathway towards finite solution, in the most logical and unambiguous way.

36 MATERIALS SCIENCE↗