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DOE OSTI2018

Modeling the He II Transverse Proximity Effect: Constraints on Quasar Lifetime and Obscuration

The He II transverse proximity effect - enhanced He II Lyα transmission in a background sightline caused by the ionizing radiation of a foreground quasar - offers a unique opportunity to probe the emission properties of quasars, in particular the emission geometry (obscuration, beaming) and the quasar lifetime. Building on the foreground quasar survey published in Schmidt et al., we present a detailed model of the He II transverse proximity effect, specifically designed to include light travel time effects, finite quasar ages, and quasar obscuration. Here, we post-process outputs from a cosmological hydrodynamical simulation with a fluctuating He ii ultraviolet background model, with the added effect of the radiation from a single bright foreground quasar. We vary the age t age and obscured sky fractions Ω obsc of the foreground quasar, and explore the resulting effect on the He ii transverse proximity effect signal. Fluctuations in intergalactic medium density and the ultraviolet background, as well as the unknown orientation of the foreground quasar, result in a large variance of the He II Lyα transmission along the background sightline. We develop a fully Bayesian statistical formalism to compare far-ultraviolet He ii Lyα transmission spectra of the background quasars to our models, and extract joint constraints on t age and Ω obsc for the six Schmidt et al. foreground quasars with the highest implied He II photoionization rates. Our analysis suggests a bimodal distribution of quasar emission properties, whereby one foreground quasar, associated with a strong He II transmission spike, is relatively old (22 Myr) and unobscured (Ω obsc < 35%), whereas three others are either younger than 10 Myr or highly obscured (Ω obsc > 70%).

79 ASTRONOMY AND ASTROPHYSICS↗

NASA NTRS1994

X-ray sources in regions of star formation. 5: The low mass stars of the Upper Scorpius association

We report followup investigations of Einstein x-ray observations of the Upper Scorpius OB association. We identify 28 low mass pre-main sequence stars as counterparts of x-ray sources in the approximately = 7 square degrees of the OB association observed. Based on kinematics and lithium abundances, these stars are low mass members of the OB association. We use optical spectra and optical and near-IR photometry to determine the stellar luminosities, effective temperatures, masses, and ages. We show that the bolometric corrections and effective temperatures of the G and K stars are consistent with those of subgiants. The low mass stars have isochronal ages of 1-2 Myr, depending on the choice of evolutionary models, with very small dispersion (sigma approximately = 1 Myr). This age is significantly younger than the 5-6 Myr found for the more massive B stars. The small dispersion in stellar ages, less than 10% the sound-crossing time of the association, suggests that star formation was triggered. We present two scenarios for star formation in this association. In the two-episode scenario, formation of the low mass stars was triggered by a supernova explosion, and the low mass stars form quickly, with high efficiency. Alternatively, high and low mass star formation was all initiated at the same time, some 5-6 Myr ago, and the apparent systematic age difference is an artifact of how the isochrones are dated. The effect of the supernova is to terminate mass accretion and yield an apparently coeval population. We show that the incompleteness in the x-ray sampling is about 65%, and is strongly dependent on stellar mass. After correction for incompleteness, we estimate there are about 2000 low mass members (stellar mass less than 2 solar mass) of this association. The mass function in this association is indistinguishable from that of the field. The ratio of naked to classical T Tauri stars is much larger than in Tau-Aur, and may be attributable to the local environment. We also present observations of eight ROX sources associated with the rho Oph cloud, and observations of non-pre-main sequence (PMS) stars in our fields.

Walter, Frederick M.↗

NASA NTRS1991

Lithium in halo stars - Constraining the effects of helium diffusion on globular cluster ages and cosmology

Stellar evolutionary models with diffusion are used to show that observations of lithium in extreme halo stars provide crucial constraints on the magnitude of the effects of helium diffusion. The flatness of the observed Li-T(eff) relation severely constrains diffusion Li isochrones, which tend to curve downward toward higher T(eff). It is argued that Li observations at the hot edge of the plateau are particularly important in constraining the effects of helium diffusion; yet, they are currently few in number. It is proposed that additional observations are required there, as well as below 5500 K, to define more securely the morphology of the halo Li abundances. Implications for the primordial Li abundance are considered. It is suggested that a conservative upper limit to the initial Li abundance, due to diffusive effects alone, is 2.35.

Deliyannis, Constantine P.↗

NASA NTRS1975

Investigation of organic adhesives for hybrid microcircuits

The properties of organic adhesives were investigated to acquire information for a guideline document regarding the selection of adhesives for use in high reliability hybrid microcircuits. Specifically, investigations were made of (1) alternate methods for determining the outgassing of cured adhesives, (2) effects of long term aging at 150 C on the electrical properties of conductive adhesives, (3) effects of shelf life age on adhesive characteristics, (4) bond strengths of electrically conductive adhesives on thick film gold metallization, (5) a copper filled adhesive, (6) effects of products outgassed from cured adhesives on device electrical parameters, (7) metal migration from electrically conductive adhesives, and (8) ionic content of electrically insulative adhesives. The tests performed during these investigations are described, and the results obtained are discussed.

Perkins, K. L.↗

DOE OSTI2021

Thermo-Oxidation Analysis of Structural Adhesives: An Experimental Study

Abstract Cross-linked polymers play an important role in structural applications as adhesives. In this article, we performed an experimental study to understand the effects of high temperature i.e. thermo-oxidative aging on the mechanical behavior of polymers. Subsequently, the constitutive behavior, i.e. stress-strain relation of these adhesives before and after the accelerated aging tests were studied on samples aged at different temperature and different time durations at zero humidity. The aging conditions and periods selected for the tests have been specifically designed to simulate the effects of aging under the working conditions that the materials will be subjected to in their standard applications. The focus of this study is on the investigation of the effects of aging on the polymeric adhesives used in automotive applications. Consequently, four different polymeric adhesives (one silicone-based, two polyurethane-based, and one acrylic type), which are being used extensively in these applications, have been chosen. The quasi-static tensile loading was used on these four adhesives and the changes in the constitutive behavior were measured. The failure tensile tests as well as the cyclic tensile tests were performed in our lab using a Test-Resources tensile testing machine. The temperatures that were used in this work are 60, 80 and 95°C for varying aging periods of 24hrs, 240hrs, and 720hrs. Then, all the data was collected and consequently analyzed, and the resulting behavior was compared to that of the unaged material, showing varying results depending on the material, temperature, and aging period. Different behaviors have been observed after aging. The polymers’ behavior was expanding from no effect to significant damage caused by aging conditions. This work provides the core understanding required for modeling the material behavior during aging and lays down the groundwork for further data-infused model-free approaches.

Alazhary, Sharif↗

DOE OSTI2018

Effect of in-situ (TiC-TiB2) reinforcement on aging and mechanical behavior of AZ91 magnesium matrix composite

Highlights: • Effect of TiC-TiB{sub 2} particles on precipitation behavior of in-situ composite was studied. • The age-hardening rate of in-situ composites is faster than that of alloy. • Faster age hardening rate is due to the presence of high dislocation density in composite. • Post aging treatment improved the mechanical properties of both base and composite. - Abstract: In the present work, influence of in-situ TiC-TiB{sub 2} reinforcement on age hardening behavior and mechanical properties of TiC-TiB{sub 2}/AZ91 composite was investigated. The base and in-situ composite materials were solution treated at 400 °C for 24 h and then aged at different temperatures up to 100 h. The kinetics of age hardening results revealed that the addition of in-situ TiC-TiB{sub 2} reinforcement increase the age hardening kinetics of the composite as compared to AZ91 magnesium alloy. The improvement in age hardening kinetics is attributed to the presence of high dislocation density resulted from the mismatch of coefficients of thermal expansion between in-situ TiC-TiB{sub 2} reinforcement and magnesium matrix. The precipitation behavior of Mg{sub 17}Al{sub 12} phase in both AZ91 alloy and TiC-TiB{sub 2}/AZ91 composites were established. After age hardening, base and in-situ composite materials show significant improvement in ultimate tensile strength by 47.72% and 66.49% respectively as compared with the base monolithic alloy. The enhancement of mechanical properties in the base and in-situ composites is explained in detail by analyzing their fractographs and microstructures.

36 MATERIALS SCIENCE↗

DOE OSTI2023

Effect of heat treatment paths on the aging and rejuvenation of metallic glasses

Here, this study explores the influence of heat treatment paths on the structural relaxation of metallic glasses (MGs) in the regime of fast dynamics. We create MG samples using various quenching rates, from 10 9 to 10 11 K/s, and expose these samples to near-T g heat treatments with assorted combinations of heating/cooling rates, from 5×10 10 to 5×10 12 K/s, and annealing durations, from 10 ps to 10 ns. Results show that the effect of the heating rate is intricately tied to the initial structure of the MG, while a decrease in the cooling rate invariably intensifies the aging process. Extending the annealing duration may induce either aging or rejuvenation, subject to the specific thermal history. To interpret these findings, we hypothesize that the memory effect, governed by the activation and annihilation of reversible and irreversible flow units, underpins the rejuvenation-aging competition in MGs. Moreover, we suggest viewing the cooling stage as an annealing phase controlled by gradient temperature and fine-tuning its rate to achieve the targeted active flow unit distributions. This study illuminates the role of fast dynamics during the glass relaxation process and offers practical strategies for tailoring heat treatments to optimize MG structures and mechanical performance.

36 MATERIALS SCIENCE↗

DOE OSTI2021

The Impact of Stand Age and Fertilization on the Soil Microbiome of Miscanthus × giganteus

Yield of the perennial grass Miscanthus × giganteus has shown an inconsistent and unpredictable response to nitrogen (N) fertilizer, yet fertilization underpins the crop’s environmental and economic sustainability. The interactions among soil microbial communities, N availability, and Miscanthus × giganteus and management may explain changes in plant productivity. In this study, soil samples from different stand ages of Miscanthus × giganteus in a replicated chronosequence field trial were used to investigate the effects of stand age and N fertilizer rates on microbial community structure. We hypothesized that there is a definable Miscanthus × giganteus soil microbiome and that this community varies significantly with stand age and fertilization. Our results showed that the main phyla in soil microbial communities, regardless of plant age, are similar but microbial community structures are significantly different. The variation in observed microbial communities generally decreases with older stand ages. The amount of N fertilizer applied also affected the microbial community structure associated with different aged Miscanthus × giganteus. Specifically, the relative abundance of Proteobacteria (Alphaproteobacteria and Gammaproteobacteria) and Acidobacteria (subgroup Gp1) increased shortly after fertilization and was more associated with younger Miscanthus × giganteus. Furthermore, our results show a significant relationship between bacterial α diversity and fertilization rates and that this response is also affected by stand age. Overall, our results emphasize linkages between microbial community structure, plant age, and fertilization in Miscanthus × giganteus.

59 BASIC BIOLOGICAL SCIENCES↗

NASA NTRS1992

Thermomechanical deformation behavior of a dynamic strain aging alloy, Hastelloy X

An experimental study was performed to identify the effects of dynamic strain aging (solute drag) and metallurgical instabilities under thermomechanical loading conditions. The study involved a series of closely controlled thermomechanical deformation tests on the solid-solution-strenghened nickel-base superalloy, Hastelloy X. This alloy exhibits a strong isothermal strain aging peak at approximately 600 C, promoted by the effects of solute drag and precipitation hardening. Macroscopic thermomechanical hardening trends are correlated with microstructural characteristics through the use of transmission electron microscopy. These observations are compared and contrasted with isothermal conditions. Thermomechanical behavior unique to the isothermal database is identified and discussed. The microstructural characteristics were shown to be dominated by effects associated with the highest temperature of the thermomechanical cycle. Results indicate that the deformation behavior of Hastelloy X is thermomechanically path dependent. In addition, guidance is given pertaining to deformation modeling in the context of macroscopic unified theory. An internal state variable is formulated to qualitatively reflect the isotropic hardening trends identified in the TMD experiments.

Castelli, Michael G.↗

DOE OSTI2018

Effect of Air and Argon Sintering Atmospheres on Properties and Hydrothermal Aging Resistance of Y-TZP Ceramics

In this work, we investigated the role of sintering atmosphere and temperature on low-temperature degradation of 3 mol.% yttria tetragonal zirconia polycrystals ceramics. Green compacts were prepared by die-pressing followed by cold isostatic pressing at 200 MPa. The green bodies were sintered between the temperature range of 1250 and 1500 °C in air and argon gas atmosphere. Sintered samples were tested to determine bulk density, Young’s modulus, Vickers hardness and fracture toughness. The results revealed that the mechanical properties of air-sintered samples were better than that of argon-sintered samples sintered at 1400 °C and below while the argon sintering marginally improves the fracture toughness and hardness when sintered at 1450 °C and above. FESEM images showed that the tetragonal grain size was similar when sintered in argon atmosphere. However, regardless of sintering atmosphere, grain growth was inevitable as the sintering temperature was increased. Hydrothermal aging test in superheated steam was performed in an autoclave at temperature of 180 °C and 10 bar pressure up to 12 h. Effect of aging on tetragonal-to-monoclinic phase transformation was measured by using x-ray diffraction. The phase transformation was found to be strongly influenced by the sintering temperature and sintering atmosphere. The sample sintered at 1500 °C in argon atmosphere exhibited rapid phase transformation compared to air atmosphere, while the samples sintered at or below 1400 °C in argon showed no phase transformation after 12-h exposure in steam environment.

36 MATERIALS SCIENCE↗

NASA NTRS1979

Initial results on 5 MHz quartz oscillators equipped with BVA resonators

The techniques of fabricating BVA resonators are discussed in terms of aging, amplitude-frequency effect, and acceleration sensitivity. Results on 5 MHz resonators concerning aging versus drive level, reduced amplitude-frequency effect, frequency and phase stability performance, and frequency retrace following power interruption are presented. It is indicated that a zero aging rate is possible at a drive level which depends on the qaurtz material used. For natural AT quartz, a level of 70 to 90 micro W appears to be optimum, and for SC quartz approximately 160 micro W.

Besson, R. J.↗

NASA NTRS1989

The age of the Galactic disk - Inflow, chemical evolution, astration, and radioactivity

Theoretical models of Galactic evolution and observational data on the age of the Galaxy are compared, with a focus on recent results. Topics addressed include the infall of material and its effects on the age-metallicity relation, the distribution of metallicity, the present gas fraction and metallicity, and the age spectrum of interstellar nuclei; the chemical evolution of the solar neighborhood; the key results of nuclear cosmochronology; and astration effects on Galactic age. It is found that both nuclear cosmochronology and detailed stellar and Galactic evolution models tend to support an age of 12-16 Gyr.

Clayton, Donald D.↗

DOE OSTI2019

The Microstructure, and Mechanical and Corrosion Properties of As-Cast and As-Extruded Mg-2%Zn-x%Cu Alloys After Solution and Aging Heat Treatments

The effects of different Cu concentrations and heat treatment on the microstructure, mechanical and corrosion properties of the as-cast and hot-extruded Mg-2%Zn alloys were studied. The results showed that T6 heat treatment led to the dissolution of intermetallics and breaking the continuous networks of intermetallics. Also, the grain size of the base alloy decreased with further Cu additions after solution and aging heat treatments. Microstructural characterization indicated that Mg(Zn,Cu) and Mg(Zn,Cu){sub 2} intermetallics were formed which their volume fractions increased with exceeding Cu additions. Moreover, the addition of 3 wt.% Cu and T6 heat treatment increased the Brinell hardness of both as-cast and hot-extruded specimens reached to 94 HBN and 116 HBN, respectively. The optimum amounts of the ultimate tensile strength and elongation values obtained from 0.1 wt.% Cu addition for both conditions after T6 treatment which were 253 MPa, 11.5% and 263 MPa, 14.7%, respectively. However, more Cu addition (> 0.5 wt.%) deteriorated the tensile properties of the alloy due to the high volume fraction of intermetallics. The yield tensile strength increased continuously with different Cu additions for the cast and extruded alloys after solution and aging heat treatments. After T6 heat treatment, extruded alloys showed better anti-corrosion properties than those of the cast alloys, while the extruded Mg-2%Zn-0.1%Cu alloy exhibited the best anti-corrosion property. Further Cu addition increased the volume fraction of intermetallics and enhanced the corrosion rate which was due to the galvanic couple effect.

36 MATERIALS SCIENCE↗

DOE OSTI2025

Computer-Based Procedures Among Older Adults: Findings from the Rancor Microworld Simulator

As with many industries worldwide, nuclear energy is experiencing an aging workforce; older than other energy sources and the national average. For example, while almost one in three nuclear industry professionals are 55+ years, for oil and gas that number is one in five. The challenges brought about by an aging workforce are one of the industry’s top concerns. However, the industry lacks for empirical research that examines the effects of developmental aging in older workers, as well as the interactions between aging and new digital technologies. We present the results of an experiment that tested three different computer-based procedures in a sample of 30 older adults (55+ years). While the industry has traditionally relied on paper-based procedures, these are being modernized by digital technology. Participants were randomly assigned to one of three procedure-types that varied by the level of digitalization, based on the IEEE Standard-1786. Type 1 essentially represents a digital representation of a paper-based procedure, Type 2 adds embedded indicators, and Type 3 adds soft controls. Participants performed two different operational scenarios (startup and loss of feedwater) on a simplified nuclear power plant simulator. Results revealed a weak signal that Type 2 may produce lower workload and lower completion times in some instances. However, there were no significant effects of procedure-type across any other outcomes, including simulator log data, situation awareness, and preference ratings. We discuss our findings in terms of optimal levels of digitalization/automation for an aging nuclear workforce and suggest pathways for future directions.

46 - INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AN↗

DOE OSTI2017

Association of UV radiation with Parkinson disease incidence: A nationwide French ecologic study

Background: Vitamin D is thought to contribute to brain health, but it is unclear whether low vitamin D levels are associated with increased incidence of Parkinson's disease (PD). Using ultraviolet B (UV-B) as a surrogate for vitamin D levels, we conducted a nationwide ecologic study in France in order to examine the association of UV-B with PD incidence. Methods: We used French national drug claims databases to identify PD cases using a validated algorithm. UV-B data from the solar radiation database were derived from satellite images. We estimated PD incidence (2010–2012) at the canton level (small administrative French unit) and used multilevel Poisson regression to examine its association with UV-B (2005 annual average), after adjustment for age, sex, deprivation index, density of neurologists, smoking, proportion of agricultural land, and vitamin D supplementation. Results: Analyses are based on 69,010 incident PD patients. The association between UV-B and PD incidence was quadratic (P<0.001) and modified by age (P<0.001). Below 70y, incidence was higher in the bottom quintile (relative risk, RR{sub Q1:45-49y}=1.18, 95% CI=1.08–1.29) compared with the middle UV-B quintile, and lower in the top quintile (RR{sub Q5:45-49y}=0.85 [0.77–0.94]). An opposite pattern was observed in older subjects (RR{sub Q1:85-89y}=0.92 [0.89–0.96]; RR{sub Q5:85-89y}=1.06 [1.02–1.11]). Analysis based on continuous UV-B yielded similar conclusions. Conclusions: In this nationwide study, there was an age-dependent quadratic association between UV-B and PD incidence. This study suggests that reasonable UV-B exposure is associated with lower PD risk in younger persons and that future studies should examine dose-response relations and take age into account. - Highlights: • There is an age-dependent quadratic association between UV-B and PD incidence. • Reasonable UV-B exposure is beneficial in younger persons for the risk of PD. • Our findings are consistent with a role of vitamin D in PD, especially at younger ages. • Future studies should examine dose-effect relations and take age into account.

54 ENVIRONMENTAL SCIENCES↗

NASA NTRS1969

Experiences with physical conditioning programs in middle-aged men

Long term effects of physical exercise and conditioning in the prevention and treatment of coronary heart disease are studied. Some aspects of the problem are outlined and difficulties encountered in a group of middle aged business executives using a carefully prescribed, but non-regimented and loosely supervised conditioning program employing commonly used forms of exercise (bicycling and jogging), are described.

Schuster, B.↗

DOE OSTI2018

Aging Management Considerations for Dry Cask Storage Canisters - 18472

Dry cask storage systems (DCSSs) are used to store used nuclear fuel (UNF) at independent spent fuel storage installations (ISFSIs) prior to final geologic storage or reprocessing. As storage durations increase beyond the twenty-year period commonly implemented for licensing the storage sites, it is important to consider aging related degradation issues for DCSS components. A large portion of the DCSS designs used throughout the world employ a ventilated concrete overpack with a welded stainless steel canister that confines the UNF. This paper explores key issues related to aging management for these canister components, including: (1) canister environment, (2) inspection limitations, and (3) aging management program guidance and requirements. While the austenitic stainless steel used for the canisters are generally resistant to most forms of environmental attack, it is possible for conditions to arise that lead to pitting and even stress corrosion cracking of the canister systems. A large number of studies related to canister degradation have been performed by industry groups and government researchers, both in the US and worldwide. These advances in the collective knowledge provide insight into risk factors for DCSS. Such information is beneficial to improve ISFSI siting decisions and ensure successful relicensing of existing ISFSIs. This paper highlights relevant research and also discusses applicability to degradation of other equipment and containers used to process and isolate UNF and other nuclear waste streams from the public and the environment. Inspection of the canister surface is an important tool to investigate and evaluate the potential for degradation. Existing DCSS designs typically do not offer ready access to the canister surface in order to perform the inspection. Further complicating inspection efforts are the surface conditions present on the sheltered canisters after extended storage times, including atmospheric debris such as dust and pollen. Given ongoing development efforts, inspection capabilities and associated limitations should be assessed at multiple points in time over the course of an aging management program to incorporate new advances in the field. This paper explores the limitations of currently available capabilities in inspection and delivery, and provides insight into the gaps remaining to be filled to permit an effective inspection program. Recommendations and requirements related to programs for aging management of canisters have been published or are in progress from a variety of groups, including industry groups, regulatory authorities, and Codes and Standards. An effective aging management program should consider the technical bases of these various inputs and maintain compliance with requirements. Given multiple sources, decisions will be required when considering conflicting guidance, and this paper will include discussion of the relative merits of the various approaches. (author)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

NASA NTRS1999

Computer Analysis of Spectrum Anomaly in 32-GHz Traveling-Wave Tube for Cassini Mission

Computer modeling of the 32-GHz traveling-wave tube (TWT) for the Cassini Mission was conducted to explain the anomaly observed in the spectrum analysis of one of the flight-model tubes. The analysis indicated that the effect, manifested as a weak signal in the neighborhood of 35 GHz, was an intermodulation product of the 32-GHz drive signal with a 66.9-GHz oscillation induced by coupling to the second harmonic'signal. The oscillation occurred only at low- radiofrequency (RF) drive power levels that are not expected during the Cassini Mission. The conclusion was that the anomaly was caused by a generic defect inadvertently incorporated in the geometric design of the slow-wave circuit and that it would not change as the TWT aged. The most probable effect of aging on tube performance would be a reduction in the electron beam current. The computer modeling indicated that although not likely to occur within the mission lifetime, a reduction in beam current would reduce or eliminate the anomaly but would do so at the cost of reduced RF output power.

Dayton, James A., Jr.↗